B01D9/00

DEOILING PROCESS
20230014244 · 2023-01-19 ·

The present disclosure generally relates to methods for deoiling a hydrocarbon feed and to products formed therefrom. In an embodiment is provided a method of deoiling a feed that includes introducing a waxy feed and a deoiling solvent to a dilution chilling zone; mixing the waxy feed and the deoiling solvent in the dilution chilling zone at a temperature of from about 10° F. to about 30° F. to form a slurry; introducing the slurry to a filter zone, the filter zone comprising one or more filter stages, wherein a temperature of the slurry is from about 40° F. to about 75° F.; separating the wax from the oil and the deoiling solvent to form a wax cake in a first filter stage; and washing the wax cake in the first filter stage with the deoiling solvent to obtain a composition comprising a wax. In another embodiment is provided a composition comprising a wax.

CONTAINED PRODUCTION OF PHARMACEUTICALLY PURE CRYSTALS
20230219014 · 2023-07-13 · ·

The present invention relates to means and methods for producing crystals or crystalline substances in a contained vessel. In particular, crystals or crystalline substances, which are useful as pharmaceutical ingredients, can be manufactured.

Method for crystallization of β-ammonium tetramolybdate

A method for crystallization of β-ammonium tetramolybdate includes: performing a stepwise pH-adjusting treatment of an ammonium molybdate solution via zoning to obtain the β-ammonium tetramolybdate. When feeding the ammonium molybdate solution into a reaction system from a first zone and then into second to sixth zones successively, pH.sup.1 of a resultant solution in the first zone is 7.0-6.0; pH.sup.2 of a resultant solution in the second zone is less than 6 and greater than or equal to 4; pH.sup.3 of a resultant solution in the third zone is less than 4 and greater than or equal to 2.5; pH.sup.4 of a crystallized slurry in the fourth zone is less than 2.5 and greater than or equal to 1; pH.sup.5 of a crystallized slurry in the fifth zone is 2.5-4.0; and pH.sup.6 of a crystallized slurry in the sixth zone is less than 2.5 and greater than or equal to 2.0.

Hybrid extraction process for cannabinoids and related methods

The present invention relates to methods for treating cannabis biomass in order to isolate tetrahydrocannabinolic acid (THCA). In another aspect, the present invention relates to a process that involves purification followed by extraction of cannabis biomass to isolate and improve yields of high-purity crystalline extracts.

Stabilized electromagnetic base liquid, formation thereof and application to high-salt wastewater treatment
11691906 · 2023-07-04 · ·

The invention is about a stabilized electromagnetic base liquid, as well as its preparation method and its application in the high-salt wastewater treatment. The raw material components of the electromagnetic base fluid include: 20-30 parts of alkali metal hydroxides(e.g., as sodium hydroxide); 20-30 parts of non-alkali metal (e.g., as silicon or phosphorus); 2-6 parts of ammonia; 31-140 parts of water; after treatment with a direct electrical current the parameters of the stabilized electromagnetic base liquid are: pH value: 12 to 14; oxidation reduction potential value: −1.0 to −1.8 v; with no corrosivity, confirming the presence of stabilized hydrated electrons (e.sub.aq−−). With the stabilized electromagnetic base liquid, the storage problem of the electromagnetic base liquid is solved, and the large-scale application in the industrial field can be realized, thereby achieving a large-scale high-salt wastewater treatment process with low cost, high recovery rate.

Process for production of glycopyrronium tosylate

Provided herein are methods for the production of glycopyrronium tosylate and glycopyrronium tosylate compositions. Also provided herein are compositions useful in the production of glycopyrronium tosylate. Additionally provided herein are glycopyrronium tosylate compositions. Glycopyrronium tosylate is useful for the treatment of, among other conditions, hyperhidrosis.

Process for production of glycopyrronium tosylate

Provided herein are methods for the production of glycopyrronium tosylate and glycopyrronium tosylate compositions. Also provided herein are compositions useful in the production of glycopyrronium tosylate. Additionally provided herein are glycopyrronium tosylate compositions. Glycopyrronium tosylate is useful for the treatment of, among other conditions, hyperhidrosis.

Method of converting delta9-THC to delta10-THC and the purification of the delta10-THC by crystallization
11542243 · 2023-01-03 ·

A method of isomerizing Δ9-tetrahydrocannabinol (“Δ9-THC”) to Δ10-tetrahydrocannabinol (“Δ10-THC”). The method includes the steps of: extracting Δ9-THC from cannabis biomass, which optionally contains one or more of the components found in fire retardant such as PHOS-CHEK®; dewaxing of crude extracts by winterization; pH-adjusting extracts by washing the extracts in heptane solution with aqueous solutions of: citric acid, sodium bicarbonate, and brine; isomerizing Δ9-THC to Δ10-THC by exposure to suitable conditions and in the presence of a catalyst based on the components of fire retardant; vacuum distillation of Δ10-THC at a predetermined temperature range and vacuum level; collecting the distillate and redistilling it up to three times to acquire distillate containing less than 60% Δ10-THC; and purification of the MO-THC to a purity of 99% or greater by crystallization from n-pentane solution.

Process for the synthesis of urea
11535586 · 2022-12-27 · ·

A process for synthesis of urea from CO.sub.2 and NH.sub.3 wherein a steam flow (13) produced in the condenser (3) of a high-pressure synthesis loop is compressed to raise its pressure and temperature before using the steam as a heat source for a downstream step of the process.

Process for the synthesis of urea
11535586 · 2022-12-27 · ·

A process for synthesis of urea from CO.sub.2 and NH.sub.3 wherein a steam flow (13) produced in the condenser (3) of a high-pressure synthesis loop is compressed to raise its pressure and temperature before using the steam as a heat source for a downstream step of the process.