A method for preparing supercritical fluid by deep-sea pressure is provided and belongs to the technical field of supercritical fluid preparation. The method includes the following steps of: placing low-pressure fluid in a closed flexible container, sending the closed flexible container down to a location of a sea at a depth where a seawater pressure meets a requirement by using a powered or unpowered traction device, leaving the flexible container standing still until a volume of the flexible container does not change, wrapping the closed flexible container with a rigid pressure-bearing container, transferring the closed flexible container to the sea surface by the powered or unpowered traction device, and taking out the fluid in the flexible container as supercritical fluid. Then the supercritical fluid is produced. Therefore, the process of preparing supercritical (high pressure) liquid in deep-sea is safer and more stable than the preparation way on land.

Processes for reducing shutdown time of a sub-system/ reactor component in an LDPE process. The process includes closing one or more pairs of upstream lock-out valves, each pair of upstream lock-out valves being located in an inlet stream upstream of the reactor component and configured to cease fluid flow into the reactor component through said inlet stream when said pair of upstream lock-out valves is closed; closing one or more pairs of downstream lock-out valves, each pair of downstream lock-out valves being located in an outlet stream downstream of the reactor component and configured to cease fluid flow out of the reactor component through said outlet stream when said pair of downstream lock-out valves is closed; depressurizing the reactor component; introducing purge gas comprising N.sub.2 into the reactor component at and withdrawing the purge gas from the reactor component.

The present disclosure belongs to the technical field of clean and efficient mining of deep unconventional or conventional resources, and discloses a pilot-scale supercritical water oxidation oil and hydrogen production system capable of realizing long-distance multi-stage heating of organic rock. The system comprises a supercritical water generator, a supercritical water pyrolysis reaction system for organic rock, an oxygen injection system and an oil-gas condensation and collection system, wherein the supercritical water generator mainly comprises a water injection system, a front-section preheating reaction system, a second-stage heating system and a third-stage heating system. The reaction system can carry out a pilot-scale simulation process of supercritical water pyrolysis for organic rock, a multi-stage heating function is realized, the maximum reaction distance is 8 m or more, and the release characteristics of oil-gas products under different reaction distances are explained. Meanwhile, the parameters of high-temperature residual carbon oxygenation hydrogen production are obtained, and the supercritical water oxidation oil and hydrogen production process of long-distance multi-stage heating of organic rock is completely simulated.

Disclosed is a hydrothermal synthesis device for continuously preparing an inorganic slurry using a hydrothermal method. The hydrothermal synthesis device includes a mixer to mix at least one precursor solution for preparing an inorganic material, injected via at least one supply tube, to prepare an intermediate slurry, a connection tube provided at a side of the mixer, continuously discharging the prepared intermediate slurry to a reactor, and having a hydrophobic coating on an inner surface of a portion thereof adjacent to the reactor, and the reactor performing hydrothermal reaction of the intermediate slurry supplied from the connection tube by receiving a liquid stream heated to supercritical or subcritical conditions using a heat exchanger and connected to the connection tube into which the intermediate slurry prepared from the mixer is introduced and to at least one injection tube into which the heated liquid stream is injected.

A vacuum chamber may include an ambient side and a vacuum side. The vacuum chamber may be configured to carry a feedthrough that may include a hollow tube, a first O-ring captured by a first recess within the hollow tube and a rod extending through the hollow tube. The outer circumference of the rod may be configured to contact an entirety of an inner circumference of the first O-ring. A vacuum fitting having an inner circumference may be fixedly secured to the hollow tube. The rod may be operable to be linearly movable within the hollow tube and may be rotatably movable about an axis within the hollow tube. An object may be secured to the rod and may be linearly and rotatably moved within the vacuum chamber.

The invention concerns a continuous flow process for manufacturing surface modified metal oxide nanoparticles by supercritical solvothermal synthesis in an reaction medium flowing within a continuous flow chamber, said continuous flow chamber containing a hydrolysis area and a supercritical area, said process comprising the introduction of a flow of metal oxide precursor into the continuous flow chamber at a point P located in the hydrolysis area or in the supercritical area, and the introduction of a flow of is located downstream of P1 with respect to the flow direction, as well as the device for carrying out this process.

A feedthrough for use in a vacuum chamber is provided and includes a hollow tube having a length, an inner circumference, and a first recess located within the inner circumference. The feedthrough also includes a first O-ring captured by the first recess within the hollow tube. The feedthrough further includes a rod extending through an entirety of the length of the hollow tube. An outer circumference of the rod is configured to contact an entirety of an inner circumference of the first O-ring, and a vacuum fitting is fixedly secured to the hollow tube.

The present disclosure provides a reaction method with homogeneous-phase supercritical fluid, including: preparing a supercritical fluid and a solute; supplying the supercritical fluid and the solute into a molecular sieve component to uniformly mix the supercritical fluid and the solute in the molecular sieve component, forming a homogeneous-phase supercritical fluid; and supplying the homogeneous-phase supercritical fluid into a reaction chamber for conducting a reaction. The present disclosure further provides an apparatus for homogeneous-phase supercritical fluid reaction, which can be utilized with the reaction method with homogeneous-phase supercritical fluid

An autoclave system comprises an autoclave vessel 210, for performing a leaching operation on sacrificial ceramic cores (not shown) and a storage vessel 220 for containing caustic leaching fluid 230. Interposed in a fluid flow path between the vessel 210 and the tank 220 is a heat exchange unit 240, comprising a body 250 containing a thermal exchange medium, in the form of water 260, and first and second thermal exchange conduits represented at 270 and 280. A thermal exchange medium inlet pipe 290a and a thermal exchange medium outlet pipe 290b are provided to the body so that the medium 260 can be replenished, preferably substantially continuously, to optimize thermal transfer efficiency.

A SCWO reactor fouling prevention and mitigation system that includes at least one feedstock tee which provides a feedstock to the SCWO reactor, at least one feedstock tee pressure sensor, such that each of the at least one feedstock tee has one of the at least one feedstock tee pressure sensor, at least one pressure sensor proximate a SCWO reactor inlet, and at least one pressure sensor proximate a SCWO reactor outlet. Also included is a controller which triggers a Clean In Place (CIP) procedure when there is a pressure difference between any two of the following, the SCWO reactor inlet, the at least one feedstock tee, and the SCWO reactor outlet. The CIP procedure includes washing a portion of the SCWO reactor with a fluid supplied through the at least one feedstock tee.