B01J14/00

Conversion of a hydrogen fluoride alkylation unit to a sulfuric acid alkylation unit and apparatus utilized therein

This disclosure relates to methods of converting an HF alkylation unit which utilizes HF as a reaction catalyst to a sulfuric acid alkylation unit which utilizes sulfuric acid as a reaction catalyst. This disclosure also relates to a segmented sulfuric acid settler for separating a sulfuric acid phase from a hydrocarbon phase. This disclosure also relates to methods of converting a vertical HF acid settler to a segmented sulfuric acid settler. This disclosure also relates to converted sulfuric acid alkylation units and alkylation processes performed in the converted sulfuric acid alkylation units.

METHOD AND APPARATUS FOR CONTROLLED PRODUCTION OF A FLUID REACTION PRODUCT
20210187506 · 2021-06-24 ·

A device and method for producing a fluid product, such as a fluid reaction product, are provided. The device includes a reaction chamber and a reception chamber and a control unit configured to control the flow of fluid into the reaction chamber through the one or more fluid connections. The device also includes a first and second amount sensor arranged to determine an amount of fluidic component(s) of the reaction chamber and reception chamber continuously or at least quasi-continuously at least during the introduction of fluidic component(s).

PRODUCTION OF LINEAR ALPHA OLEFINS FROM ORGANIC SULFIDES

Embodiments of the disclosure provide a system and method for producing a linear alpha olefin. A disulfide, a hydrogen donating compound, and water are combined to produce a mixture. The mixture is introduced to a reactor operated at a pressure equal to or greater than 22.06 MPa and a temperature equal to or greater than 374 deg. C to produce an effluent stream. The effluent stream is separated to produce a product stream including the linear alpha olefin. The disulfide can be a compound of formula R—S—S—R′ where R is a first alkyl group having carbon atoms ranging from 1 to 12 and R′ is a second alkyl group having carbon atoms ranging from 5 to 12. The hydrogen donating compound can include a partially hydrogenated multi-ring aromatic compound.

PRODUCTION OF LINEAR ALPHA OLEFINS FROM ORGANIC SULFIDES

Embodiments of the disclosure provide a system and method for producing a linear alpha olefin. A disulfide, a hydrogen donating compound, and water are combined to produce a mixture. The mixture is introduced to a reactor operated at a pressure equal to or greater than 22.06 MPa and a temperature equal to or greater than 374 deg. C to produce an effluent stream. The effluent stream is separated to produce a product stream including the linear alpha olefin. The disulfide can be a compound of formula R—S—S—R′ where R is a first alkyl group having carbon atoms ranging from 1 to 12 and R′ is a second alkyl group having carbon atoms ranging from 5 to 12. The hydrogen donating compound can include a partially hydrogenated multi-ring aromatic compound.

Production of linear alpha olefins from organic sulfides

Embodiments of the disclosure provide a system and method for producing a linear alpha olefin. A disulfide, a hydrogen donating compound, and water are combined to produce a mixture. The mixture is introduced to a reactor operated at a pressure equal to or greater than 22.06 MPa and a temperature equal to or greater than 374 deg. C. to produce an effluent stream. The effluent stream is separated to produce a product stream including the linear alpha olefin. The disulfide can be a compound of formula R—S—S—R′ where R is a first alkyl group having carbon atoms ranging from 1 to 12 and R′ is a second alkyl group having carbon atoms ranging from 5 to 12. The hydrogen donating compound can include a partially hydrogenated multi-ring aromatic compound.

Production of linear alpha olefins from organic sulfides

Embodiments of the disclosure provide a system and method for producing a linear alpha olefin. A disulfide, a hydrogen donating compound, and water are combined to produce a mixture. The mixture is introduced to a reactor operated at a pressure equal to or greater than 22.06 MPa and a temperature equal to or greater than 374 deg. C. to produce an effluent stream. The effluent stream is separated to produce a product stream including the linear alpha olefin. The disulfide can be a compound of formula R—S—S—R′ where R is a first alkyl group having carbon atoms ranging from 1 to 12 and R′ is a second alkyl group having carbon atoms ranging from 5 to 12. The hydrogen donating compound can include a partially hydrogenated multi-ring aromatic compound.

PERFORMIC ACID PRODUCTION SYSTEMS AND METHODS

Systems for producing performic acid and methods for producing performic acid. The systems may include two or more reactor units, two or more servient programmable logic controllers, a control panel, and a master programmable logic controller. The system may modify the production of performic acid in at least one of the two or more reactor units upon and/or after the occurrence of a disruptive event in order to maintain a desired level of performic acid production and/or a desired level of disinfection.

PERFORMIC ACID PRODUCTION SYSTEMS AND METHODS

Systems for producing performic acid and methods for producing performic acid. The systems may include two or more reactor units, two or more servient programmable logic controllers, a control panel, and a master programmable logic controller. The system may modify the production of performic acid in at least one of the two or more reactor units upon and/or after the occurrence of a disruptive event in order to maintain a desired level of performic acid production and/or a desired level of disinfection.

SULFURIC ACID ALKYLATION REACTOR SYSTEM AND CONVERSION OF A HYDROGEN FLUORIDE ALKYLATION UNIT TO A SULFURIC ACID ALKYLATION UNIT

This disclosure relates to SA alkylation reactor systems. The reactor system involves a closed reactor vessel comprising a shell, a vapor outlet, and an emulsion outlet. The reactor system also involves a distributor located at the lower portion of the reactor vessel, a mixer fluidly connected with the distributor, and an emulsion pump fluidly connected with the mixer and the emulsion outlet, wherein the emulsion pump is located outside the reactor vessel. This disclosure also relates to a split SA alkylation reactor system wherein a single horizontal reactor vessel is divided to accommodate two reactor systems. This disclosure also relates to alkylation processes using the reactor systems. This disclosure also relates to methods of converting an HF alkylation unit to a SA alkylation unit. This disclosure also relates to converted SA alkylation units and alkylation processes performed in the converted SA alkylation units.

SULFURIC ACID ALKYLATION REACTOR SYSTEM AND CONVERSION OF A HYDROGEN FLUORIDE ALKYLATION UNIT TO A SULFURIC ACID ALKYLATION UNIT

This disclosure relates to SA alkylation reactor systems. The reactor system involves a closed reactor vessel comprising a shell, a vapor outlet, and an emulsion outlet. The reactor system also involves a distributor located at the lower portion of the reactor vessel, a mixer fluidly connected with the distributor, and an emulsion pump fluidly connected with the mixer and the emulsion outlet, wherein the emulsion pump is located outside the reactor vessel. This disclosure also relates to a split SA alkylation reactor system wherein a single horizontal reactor vessel is divided to accommodate two reactor systems. This disclosure also relates to alkylation processes using the reactor systems. This disclosure also relates to methods of converting an HF alkylation unit to a SA alkylation unit. This disclosure also relates to converted SA alkylation units and alkylation processes performed in the converted SA alkylation units.