B01J15/00

Rotary reactor for uniform particle coating with thin films

A reactor for coating particles includes one or more motors, a rotary vacuum chamber configured to hold particles to be coated and coupled to the motors, a controller configured to cause the motors to rotate the chamber in a first direction about an axial axis at a rotation speed sufficient to force the particles to be centrifuged against an inner diameter of the chamber, a vacuum port to exhaust gas from the rotary vacuum chamber, a paddle assembly including a rotatable drive shaft extending through the chamber and coupled to the motors and at least one paddle extending radially from the drive shaft, such that rotation of the drive shaft by the motors orbits the paddle about the drive shaft in a second direction, and a chemical delivery system including a gas outlet on the paddle configured inject process gas into the particles.

Reactor packing with preferential flow catalyst

The present invention relates to reactor tubes packed with a catalyst system employed to deliberately bias process gas flow toward the hot tube segment and away from the cold segment in order to reduce the circumferential tube temperature variation.

System and method of dehydrogenative coupling

Embodiments include a system that may include a reactor including a reaction zone and a gas release zone separated by a selectively permeable membrane, wherein the selectively permeable membrane permits hydrogen to pass through the membrane and substantially blocks a substrate and its dehydrogenative coupling product from passing through the membrane. Embodiments further include a method of producing a dehydrogenative coupling product, wherein the method may include exposing a substrate to a catalyst in a reaction zone of a reactor; coupling the substrate to form the dehydrogenative coupling product and hydrogen; and separating the hydrogen from the dehydrogenative coupling product using a selectively permeable membrane and passing the hydrogen to a gas release zone of the reactor.

HYDROGEN PRODUCING APPARATUS, METHOD FOR SEPARATING SOLID PRODUCT AND SYSTEM FOR DISCHARGING AND RECYCLING SOLID PRODUCT
20210246022 · 2021-08-12 ·

To provide an apparatus and a system suitable for continuously and stably producing hydrogen by taking advantage of a direction composition reaction of hydrocarbons as well as a method for separating a solid product.

Provided are a hydrogen producing apparatus using a nickel-based metal structure for the direct decomposition reaction of hydrocarbons and a discharging and recovering system comprising: a depressurization chamber communicating with a lower opening of the reaction chamber of hydrogen producing apparatus 1 via a ventilation hole; a first valve capable of opening and closing said ventilation hole; a collection box communicating with the depressurization chamber via a channel; a second valve capable of opening and closing said depressurization chamber; and a depressurization pump communicating with the collection box.

Systems and methods for making ceramic powders

Systems and methods for making ceramic powders configured with consistent, tailored characteristics and/or properties are provided herein. In some embodiments a system for making ceramic powders, includes: a reactor body having a reaction chamber and configured with a heat source to provide a hot zone along the reaction chamber; a sweep gas inlet configured to direct a sweep gas into the reaction chamber and a sweep gas outlet configured to direct an exhaust gas from the reaction chamber; a plurality of containers, within the reactor body, configured to retain at least one preform, wherein each container is configured to permit the sweep gas to flow therethrough, wherein the preform is configured to permit the sweep gas to flow there through, such that the precursor mixture is reacted in the hot zone to form a ceramic powder product having uniform properties.

SOLAR RECEIVER-REACTOR
20210229988 · 2021-07-29 · ·

The invention relates to a method for producing syngas by means of solar radiation, in which the reactor of a receiver-reactor is periodically heated via an aperture provided in the same for solar radiation by means of the solar radiation to an upper reduction temperature for a reduction process and subsequently cooled to a lower oxidation temperature for an oxidation process in the presence of an oxidation gas, wherein the sunlight is guided through an absorption chamber onto an absorber configured as a reactor, which includes a reducible/oxidizable material, and wherein a gas that absorbs the black-body radiation of the absorber is guided through the absorption chamber and the absorption chamber is configured so that the back radiation of the absorber through the aperture is essentially absorbed by the gas. Radiation losses caused by back radiation of the black-body radiation exiting the optical aperture are thus avoided in accordance with the invention. The heat of the back radiation, however, can be utilized directly in the heat-transporting fluid and is available for a flexible usage. The receiver-reactor has a simple design and is suitable as a low-cost receiver-reactor.

SOLAR RECEIVER-REACTOR
20210229988 · 2021-07-29 · ·

The invention relates to a method for producing syngas by means of solar radiation, in which the reactor of a receiver-reactor is periodically heated via an aperture provided in the same for solar radiation by means of the solar radiation to an upper reduction temperature for a reduction process and subsequently cooled to a lower oxidation temperature for an oxidation process in the presence of an oxidation gas, wherein the sunlight is guided through an absorption chamber onto an absorber configured as a reactor, which includes a reducible/oxidizable material, and wherein a gas that absorbs the black-body radiation of the absorber is guided through the absorption chamber and the absorption chamber is configured so that the back radiation of the absorber through the aperture is essentially absorbed by the gas. Radiation losses caused by back radiation of the black-body radiation exiting the optical aperture are thus avoided in accordance with the invention. The heat of the back radiation, however, can be utilized directly in the heat-transporting fluid and is available for a flexible usage. The receiver-reactor has a simple design and is suitable as a low-cost receiver-reactor.

Halogen generator
11072528 · 2021-07-27 · ·

Disclosed herein are embodiments of a method and system for producing a halogen gas. The method may comprise contacting a solid oxidizing agent with a vapor comprising a halide compound, to produce a gas stream comprising a halogen corresponding to the halide in the halide compound. The halide compound may be an acyl halide, such as an acetyl halide or an oxalyl halide. The oxidizing agent may be any suitable oxidizing agent, and in certain examples, potassium permanganate is used. The method may be performed under a reduced pressure. Also disclosed herein is a system suitable to perform the disclosed method. The system may comprise a reservoir, an oxidizing agent support and a gas stream outlet.

Halogen generator
11072528 · 2021-07-27 · ·

Disclosed herein are embodiments of a method and system for producing a halogen gas. The method may comprise contacting a solid oxidizing agent with a vapor comprising a halide compound, to produce a gas stream comprising a halogen corresponding to the halide in the halide compound. The halide compound may be an acyl halide, such as an acetyl halide or an oxalyl halide. The oxidizing agent may be any suitable oxidizing agent, and in certain examples, potassium permanganate is used. The method may be performed under a reduced pressure. Also disclosed herein is a system suitable to perform the disclosed method. The system may comprise a reservoir, an oxidizing agent support and a gas stream outlet.

HYDROGEN GENERATION SYSTEMS

A system for production of hydrogen includes a steam methane reformer (SMR) including an outer tube, wherein a first end of the outer tube is closed; and an inner tube disposed in the outer tube, wherein a first end of the inner tube is open. An SMR flow channel is defined within the inner tube and an annular space is defined between the outer tube and the inner tube. The flow channel is in fluid communication with the annular space. The SMR includes a foam disposed in the annular space. The system includes a water gas shift reactor comprising a reaction tube, wherein a reaction channel is defined within the reaction tube, and wherein the reaction channel is in fluid communication with the SMR flow channel; a heat transfer material disposed in the reaction channel; and a catalyst disposed in the reaction channel.