B01J49/00

Urea sulfate and sodium chloride blend for regeneration of cation exchange resins

Methods and systems for an integrated acid regeneration of ion exchange resins are disclosed for use in cleaning applications. Acid resins designed for use in a variety of cleaning application using a treated, softened, acidic water source are disclosed. Various methods of using the softened acidic water generated by acid regenerate-able ion exchange resins within a cleaning application, e.g. ware wash machine, are disclosed to beneficially reduce spotting, filming and scale buildup on treated surfaces, reduce and/or eliminate the need for polymers, threshold reagents and/or rinse aids, and using protons generated in the acidic water effluent for triggering events useful in various cleaning applications.

Process for regeneration of spent zirconium phosphate for reuse in sorbent treatments

A method is provided for regenerating spent zirconium phosphate for reuse in sorbent dialysis treatments or other re-uses as a sorbent material. The method includes contacting spent zirconium phosphate with an aqueous disinfectant solution having at least one antimicrobial agent, and treating the resulting disinfected zirconium phosphate with an acidic solution to provide a treated zirconium phosphate that can be re-used as a sorbent material. Sorbent cartridge products containing the regenerated spent zirconium phosphate are also provided. Methods and systems for sorbent dialysis which re-use the regenerated zirconium phosphate such as part of sorbent cartridges, additionally are provided.

Turbidity sensing filter apparatus, systems, and methods thereof

A filter press having a plurality of stackable filter plate assemblies comprises at least one turbidity sensing module [20, 220, 320, 420] coupled to a first filter plate assembly [1] within the plurality of stackable filter plate assemblies. The turbidity sensing module [20, 220, 320, 420] is generally positioned between a filtrate drain opening [8a-d] communicating with a filter chamber [14], and either a filtrate port [7, 13] or filtrate discharge tube [4g, 15], in order to determine a level of turbidity of filtrate [50] exiting said first filter plate assembly. Turbidity levels may be determined independently of turbidity levels of filtrate [50] exiting other filter plate assemblies [1] within the filter press. When turbidity levels reach a predetermined threshold, and alarm [80] is activated, which informs an operator of the need to replace a filter cloth associated with the affected filter plate assembly [1].

Processes for the recovery of uranium from industrial phosphoric acid using dual or single cycle continuous ion exchange approaches

In alternative embodiments, the invention provides processes and methods for the recovery, removal or extracting of, and subsequent purification of uranium from a wet-process phosphoric acid using a continuous ion exchange processing approach, where the uranium is recovered from a phosphoric acid, or a phos-acid feedstock using either a dual or a single stage extraction methodology. In both cases an intermediate ammonium uranyl-tricarbonate solution is formed. In alternative embodiments, in the dual cycle approach, this solution is contacted in a second continuous ion exchange system with a strong anion exchange resin then subsequently recovered as an acidic uranyl solution that is further treated to produce an intermediate uranyl peroxide compound which is ultimately calcined to produce the final uranium oxide product. In alternative embodiments, in the single cycle case, the intermediate ammonium uranyl-tricarbonate solution is evaporated to decompose the ammonium carbonate and produce an intermediate uranium carbonate/oxide solid material. These solids are digested in an acid medium, and then processed in the same manner as the secondary regeneration solution from the dual cycle process to produce an intermediate uranyl peroxide that is calcined to produce a final uranium oxide product.

Processes for the recovery of uranium from industrial phosphoric acid using dual or single cycle continuous ion exchange approaches

In alternative embodiments, the invention provides processes and methods for the recovery, removal or extracting of, and subsequent purification of uranium from a wet-process phosphoric acid using a continuous ion exchange processing approach, where the uranium is recovered from a phosphoric acid, or a phos-acid feedstock using either a dual or a single stage extraction methodology. In both cases an intermediate ammonium uranyl-tricarbonate solution is formed. In alternative embodiments, in the dual cycle approach, this solution is contacted in a second continuous ion exchange system with a strong anion exchange resin then subsequently recovered as an acidic uranyl solution that is further treated to produce an intermediate uranyl peroxide compound which is ultimately calcined to produce the final uranium oxide product. In alternative embodiments, in the single cycle case, the intermediate ammonium uranyl-tricarbonate solution is evaporated to decompose the ammonium carbonate and produce an intermediate uranium carbonate/oxide solid material. These solids are digested in an acid medium, and then processed in the same manner as the secondary regeneration solution from the dual cycle process to produce an intermediate uranyl peroxide that is calcined to produce a final uranium oxide product.

Water softening compositions, and related systems and methods
09700884 · 2017-07-11 · ·

Water softening compositions, and related systems and methods are disclosed. The present disclosure involves a composition for the regeneration of cation exchange media. The regenerant composition includes an alkali metal formate salt (and optionally a metal halide salt). The present disclosure also involves a systems and methods for treating a cation exchange medium in a water softener to replace hardness cations therefrom with alkali metal cations (such as Na.sup.+ and K.sup.+. The method includes contacting the media with a regenerant including an alkali metal formate salt (and optionally an alkali metal halide salt). The method also includes contacting the media with the regenerant in an amount sufficient to regenerant the ion exchange medium. According to the method, the hardness cations coupled to the cation exchange media are replaced with the alkali metal cations.

Removal of components from a starting material

The present invention relates to a process and, more specifically, to a process for the removal of components from a starting material. Optionally, the process is used for the removal of contaminants from ion exchange regenerant material.

Nanoporous silica polyamine composites with surface-bound zirconium (IV) and methods of use

Silica polyamine composites (SPC) made from silanized amorphous nano-porous silica gel and poly(allylamine) (BP-1) were functionalized with phosphorus acid using the Mannich reaction, resulting in a phosphonic acid modified composite (BPAP). Zirconium (IV) was immobilized on BPAP. Arsenate anions strongly adsorbed on the ZrBPAP composite in the pH range 2 to 8, while arsenite only adsorbed well at pH 10. Regeneration of the resin was carried out successfully for As(V) and As(III) using 2M-H.sub.2SO.sub.4. Four adsorption/desorption cycles were performed for As(V) at pH 4 without significant decrease in the uptake performance. ZrBPAP capture capacity and kinetics for arsenate were tested for longevity over 1000 cycles with only a marginal loss of performance.

Method for purifying silane compound or chlorosilane compound, method for producing polycrystalline silicon, and method for regenerating weakly basic ion-exchange resin

The present invention provides a technique which allows stable use of an ion-exchange resin for removing boron impurities over a long period of time in the purification step of a silane compound or a chlorosilane compound. In the present invention, a weakly basic ion-exchange resin used for the purification of a silane compound and a chlorosilane compound is cleaned with a gas containing hydrogen chloride. When this cleaning treatment is used for the initial activation of the weakly basic ion-exchange resin, a higher impurity-adsorbing capacity can be obtained. Further, use of the cleaning treatment for the regeneration of the weakly basic ion-exchange resin allows stable use of the ion-exchange resin for a long time. This allows reduction in the amount of the resin used in a long-term operation and reduction in the cost of used resin disposal.

Process for nitrate reduction from water
09670075 · 2017-06-06 ·

A system and process for nitrate reduction from a water source. The process includes the steps of passing nitrate contaminated water through a strong acid cation exchange resin to reduce cations. The effluent is thereafter passed through a weak base anion exchange resin in order to reduce nitrate content. The strong acid cation exchange resin is regenerated, and the weak base anion exchange resin is also regenerated.