B01F17/00

Preparation of Alkylcyclohexanol Polyoxyethylene Ether Emulsifier and Application Thereof
20210087334 · 2021-03-25 ·

The disclosure discloses preparation and application of an alkylcyclohexanol polyoxyethylene ether emulsifier, and belongs to the technical field of surfactants. By performing ethylene oxide adducting on alkylcyclohexanol polyoxyethylene ether (1-3) and using a strong alkaline suspension dispersed in the solvent and alkylcyclohexanol polyoxyethylene ether (1-3) as a catalyst, nonionic surfactants alkylcyclohexanol polyoxyethylene ether (5-17) are synthesized. The products all have good characteristics of nonionic surfactants, and contain lower content of polyethylene. The products such as nonylcyclohexanol ethoxylate (7) and nonylcyclohexanol ethoxylate (9) have emulsifying properties similar to the emulsifying property of nonylphenol ethoxylate (10), and therefore can substitute for nonylphenol ethoxylate (10) as an emulsifier.

Calcium-based Catalyst and Method for Catalytically Synthesizing Alkanolamide Surfactant thereof
20210087136 · 2021-03-25 ·

The present disclosure discloses a calcium-based catalyst and a method for catalytically synthesizing an alkanolamide surfactant thereof, and belongs to the technical field of surfactant synthesis. In the present disclosure, the compounded calcium-based catalyst is prepared, and the calcium-based catalyst is utilized to catalyze reaction of fat and oil or fatty acid ester and alkanol amine to synthesize the alkanolamide surfactant with light color and less free alkanol amine, which facilitates application in daily chemicals. The calcium-based catalyst in the present disclosure has a slow release feature, so that the catalyst still has relatively high catalytic reaction activity in the late reaction period, it is guaranteed that the alkanol amine is converted into the alkanolamide surfactant with a high conversion rate, the conversion rate of the alkanol amine is high, the residual quantity of the alkanol amine in the product is low, and the risk of nitrosamine caused by the residual alkanol amine in the product is greatly lowered. Meanwhile, the speed in the early reaction period is greatly reduced due to control of slow release of the catalyst, and a deepened color of the product caused by poor heat transfer in the synthesis process due to excessively fast reaction in the early period is effectively avoided.

Development of anti-bit balling fluids

Anti-bit balling drilling fluids and methods of making and using drilling fluids are provided. The anti-bit balling drilling fluid contains water, a clay-based component, and at least one of a surfactant having the formula: R(OC.sub.2H.sub.4).sub.xOH, where R is a hydrocarbyl group having from 10 to 20 carbon atoms and x is an integer from 1 and 10, or a polyethylene glycol having the formula: H(OCH.sub.2CH.sub.2).sub.nOH, where n is an integer from 1 to 50. Methods of making and using these drilling fluids are also provided.

Lipid-based ophthalmic emulsion

The present invention is directed to a lipid-based ophthalmic emulsion. The emulsion has an increased amount of a mucoadhesive galactomannan polymer that promotes a long-lasting protection against desiccation and moisture retention.

Surfactant Compositions and Methods for Emulsifying Cannabinoid Extracts as a Nano-Emulsion Material
20210046438 · 2021-02-18 ·

An embodiment of a CBD Nano-Emulsion material and process comprises a formulation comprising at least a lecithin or mixed lecithin, one or more carrier oils, and a Vitamin E TPGS from a sunflower version and a soy version. Among either version, the versions may further comprise mixed tocopherols, and still further comprise at least one of; an LCT oil, an olive oil, and a coconut oil. Any one of the versions may further comprise at least one of; sodium benzoate, potassium sorbate, and sorbic acid; and even yet further comprise purified water. Some embodiments may comprise a Vitamin E acetate.

PROCESS FOR PREPARING TRANSPARENT EMULSIONS

This disclosure provides a process for preparing transparent emulsions, in particular emulsions that are free of solvents such as propylene glycol, for use in producing clear beverages.

SPACER FLUIDS AND CEMENT SLURRIES THAT INCLUDE SURFACTANTS

According to at least one embodiment of the present disclosure, a well bore cementing system may comprise a spacer fluid and a cement slurry. The spacer fluid may be positioned within a well bore, and the spacer fluid may comprise a first surfactant package comprising one or more surfactants. The cement slurry may be positioned within the well bore, and the cement slurry may comprise a second surfactant package comprising one or more surfactants.

Pickering emulsion stabilized by cellulose nanocrystals from ginkgo seed shells and preparation method thereof
20210213405 · 2021-07-15 ·

The disclosure discloses a Pickering emulsion stabilized by cellulose from ginkgo seed shells and a preparation method thereof, and belongs to the fields of preparation methods of biomass materials and food chemical industry. The disclosure uses ginkgo seed shells as a raw material to obtain high-purity cellulose through hot alkali treatment and sodium chlorite bleaching. After the cellulose is dried, the cellulose is hydrolyzed with sulfuric acid to obtain a cellulose nanocrystal suspension. The suspension is mixed with an oil phase, and the Pickering emulsion is obtained through high-speed shearing and homogeneous emulsification. The disclosure can prepare cellulose nanocrystals with different aspect ratios by adjusting the parameters of high-speed shearing and homogeneous emulsification according to actual production needs. Cellulose nanocrystals with high aspect ratio can be used to prepare stable Pickering emulsions with high oil phase and high viscosity, which can be applied to the fields of food, cosmetics and the like; and cellulose nanocrystals with low aspect ratio can be used to prepare Pickering emulsions with low viscosity and high fluidity, which can to be applied to the fields of food and medicine.

Colloidal Particles Functionalized Homogeneously by Biomolecules
20210213410 · 2021-07-15 ·

The present invention relates to a method for producing a colloid comprising functionalised liquid colloidal particles. The invention also relates to such a colloid and to the uses thereof.

Wetting and anti-foaming agent

A wetting agent according to Formula (I): ##STR00001## wherein R.sup.1 is selected from a branched alkyl group or linear alkyl group or a cycloaliphatic group or an aromatic group, each having 6 to 15 carbon atoms; R.sup.2 is selected from hydrogen, methyl, or ethyl; R.sup.3 is selected from hydrogen, methyl, or ethyl; R.sup.4 is selected from hydrogen, methyl, or ethyl; R.sup.5 is selected from methyl or ethyl; x ranges from 0 to 5; y ranges from 0 to 10; z ranges from 1 to 10; with the proviso that when x ranges from 1 to 5, R.sup.2 is different from R.sup.3; and with the proviso that when x=0, R.sup.3 is different from R.sup.4. The wetting agent also imparts anti-foam properties to aqueous solutions while reducing surface tension.