A high temperature resistant polyimide film and its preparation method. The present invention relates to a polyimide film and its preparation method and solves the problems of honeycomb's and skin panel's core adhesive—polyimide film with insufficient heat resistance, no climbing of bonding core structure and adhesive fillet formation. The high temperature resistant polyimide film is made by polyimide solution, inorganic filler modifier and interface coupling agent by the steps of: under specific temperature and stirring conditions, adding inorganic filler modifier and interface coupling agent to polyimide solution, stirring to obtain the adhesive agent; filtering and degassing the adhesive agent, casting to a stainless steel drum with carrier cloth and release paper to obtain a self-supporting film; then heating and annealing to obtain the final polyimide film. The present invention is applied to high temperature resistant polyimide film and its preparation method.

The present disclosure provides methods for stabilizing a colloidal dispersion during transport for low defect tolerance applications. The methods involve eliminating fluid interfaces within a dispersion, storing the dispersion in an environment of inert gas, and degassing the dispersion. Several bottle closure devices are described which may be ideal for use with these methods, being able to seal a container filled with a dispersion, permit the removal of headspace and rapidly empty the contained dispersion. In one aspect, the device includes a vented cap and semi-permeable membrane, which allows the passage of gas into and out of the container, and a dispenser nozzle integrated with the device to allow a stored dispersion to be dispensed without removing the device from the container. In another aspect, the bottle closure device includes an attachment point for a removable downtube and dispenser nozzle.

The present disclosure provides methods for stabilizing a colloidal dispersion during transport for low defect tolerance applications. The methods involve eliminating fluid interfaces within a dispersion, storing the dispersion in an environment of inert gas, and degassing the dispersion. Several bottle closure devices are described which may be ideal for use with these methods, being able to seal a container filled with a dispersion, permit the removal of headspace and rapidly empty the contained dispersion. In one aspect, the device includes a vented cap and semi-permeable membrane, which allows the passage of gas into and out of the container, and a dispenser nozzle integrated with the device to allow a stored dispersion to be dispensed without removing the device from the container. In another aspect, the bottle closure device includes an attachment point for a removable downtube and dispenser nozzle.

A method of molding a component includes the steps of providing a plurality of fibers, applying the fibers with a low temperature sizing to form a plurality of sized fibers, forming a preform from the plurality of sized fibers, placing the preform in a mold, and de-sizing the preform by heating the mold to an initial temperature that is sufficient to break down the low temperature sizing to a gaseous phase. A molding apparatus is also disclosed.

A method of molding a component includes the steps of providing a plurality of fibers, applying the fibers with a low temperature sizing to form a plurality of sized fibers, forming a preform from the plurality of sized fibers, placing the preform in a mold, and de-sizing the preform by heating the mold to an initial temperature that is sufficient to break down the low temperature sizing to a gaseous phase. A molding apparatus is also disclosed.

Polymers and copolymers, and systems and methods for processing the same. Advantageously, the polymers and copolymers of the present invention have undergone processing in a falling strand devolatilizer and rotary disk finisher such that a low-cost, low-energy, and high-production-rate product is produced.

A method including applying an AC voltage to a mixture of a polymer material and nanoparticles to form a polyolefin-carbon nanomaterial composite. The polyolefin-carbon nanomaterial composite includes electrically conductive pathways that are oriented within the polyolefin-carbon nanomaterial composite. The method forms an electrically conductive polymer-graphene material by a process that includes milling a polyolefin with carbon nanoparticles, then forming a composite plate by press-molding the mixture of polyolefin and graphene while inserting a needle electrode therein. Subsequent application of an AC voltage causes partial dielectric breakdown of the composite thereby forming the electrically conductive pathways.

A molding material supply device and a molding material supply method capable of supplying a degassed molding material to a molding apparatus at a desired timing are desired. According to the molding material supply device and method of the disclosure, a first discharge member is driven to discharge a molding material accommodated in a first accommodation member to a second discharge member through a through hole of a die, and a second discharge member configured by the first accommodation member and the die advances to discharge the molding material having been degassed in the second accommodation member to the molding apparatus from a molding material supply port.

A method for correcting non-rigid thin-walled tubular elements having geometric deficiencies, wherein, following correction, the tubular elements may perform over a wide range of pressure and temperatures, for example as a rocket motor beaker, from about −70 C to about 1000 C. Correction is required to remove asperities, maximize cylindricity, squaring a forward end wall and a rearward end wall, so that the forward end wall of the tube product may be fitted, bonded and sealed to a circular planar element using a labyrinth-joint closure. The method provides uniformity so that both the tubular elements and the circular planar elements are interchangeably uniform in size, shape and performance, and may be readily assembled into non-rigid thin-walled tube products.

A high temperature resistant polyimide film and its preparation method. The present invention relates to a polyimide film and its preparation method and solves the problems of honeycomb's and skin panel's core adhesive—polyimide film with insufficient heat resistance, no climbing of bonding core structure and adhesive fillet formation. The high temperature resistant polyimide film is made by polyimide solution, inorganic filler modifier and interface coupling agent by the steps of: under specific temperature and stirring conditions, adding inorganic filler modifier and interface coupling agent to polyimide solution, stirring to obtain the adhesive agent; filtering and degassing the adhesive agent, casting to a stainless steel drum with carrier cloth and release paper to obtain a self-supporting film; then heating and annealing to obtain the final polyimide film. The present invention is applied to high temperature resistant polyimide film and its preparation method.