C01F11/00

Modification of layered double hydroxides
10131548 · 2018-11-20 · ·

The present invention relates to a process for modifying a layered double hydroxide (LDH), the process comprising, a. providing a material comprising a layered double hydroxide of formula: [M.sup.z+.sub.1-xM.sup.y+.sub.x(OH).sub.2].sup.q+(X.sup.n).sub.q/n.bH.sub.2O wherein M and M are metal cations, z is 1 or 2, x is 0.1 to 1, b is 0 to 5, y is 3 or 4, X is an anion, n is 1 to 3 and q is determined by x, y and z, b. optionally washing the material at least once with a mixture of water and a mixing solvent miscible with water, and c. washing the material obtained in step a or b at least once with at least one first solvent, the first solvent being miscible with water and having a solvent polarity P.

Carbon-based clathrate compounds

The present invention provides carbon-based clathrate compounds, including a carbon-based clathrate compound that includes a clathrate lattice with atoms of at least one element selected from the group consisting of carbon and boron as a host cage structure; guest atoms encapsulated within the clathrate lattice; and, substitution atoms that may be substituted for at least one portion of the carbon and boron atoms that constitute the clathrate lattice. In one embodiment, the invention provides a carbon-based clathrate compound of the formula LaB.sub.3C.sub.3.

Carbon-based clathrate compounds

The present invention provides carbon-based clathrate compounds, including a carbon-based clathrate compound that includes a clathrate lattice with atoms of at least one element selected from the group consisting of carbon and boron as a host cage structure; guest atoms encapsulated within the clathrate lattice; and, substitution atoms that may be substituted for at least one portion of the carbon and boron atoms that constitute the clathrate lattice. In one embodiment, the invention provides a carbon-based clathrate compound of the formula LaB.sub.3C.sub.3.

SOLUBLE CALCIUM STABILISED IN AN ANIONIC-CATIONIC POLYMER AND FRUCTANS

The present invention provides processes that promote the solvation of calcium ions in macromolecular matrices. Processes in which the relationship, concentration, physicochemical conditions at each stage and preparation methods allow to obtain a stabilized soluble product, based on calcium salts and polymers. The present invention does not result in the deposition of crystals of the salts used, and exceeds the commercial calcium formulations so they are of great utility for their application in the food, pharmaceutical and/or cosmetic industry.

Cementation Methods

The present invention provides methods for mineral precipitation and/or cementation of permeable or fractured non-porous materials using isolated urease.

Cementation Methods

The present invention provides methods for mineral precipitation and/or cementation of permeable or fractured non-porous materials using isolated urease.

Hematite manufacturing process and hematite manufactured by same

Magnesium oxide produced by a process is used as a neutralizing agent for preliminary neutralization treatment of a leached slurry obtained by leaching a nickel oxide ore at a high temperature and pressure with sulfuric acid added. A neutralizing agent is added to a leachate, obtained by leaching a nickel oxide ore, to separate impurities, and a sulfurizing agent is added to the resulting neutralized solution to obtain nickel and cobalt sulfides, followed by separating the sulfurized solution; discharge waste water, obtained by adding a neutralizing agent to the sulfurized solution to separate aluminum and manganese, is concentrated to precipitate and separate calcium contained in the discharge waste water as calcium sulfate; the resulting solution is concentrated to precipitate magnesium in the solution as magnesium sulfate; the magnesium sulfate is roasted with a reducing agent to obtain magnesium oxide and a sulfurous gas; and the magnesium oxide is washed.

Hematite manufacturing process and hematite manufactured by same

Magnesium oxide produced by a process is used as a neutralizing agent for preliminary neutralization treatment of a leached slurry obtained by leaching a nickel oxide ore at a high temperature and pressure with sulfuric acid added. A neutralizing agent is added to a leachate, obtained by leaching a nickel oxide ore, to separate impurities, and a sulfurizing agent is added to the resulting neutralized solution to obtain nickel and cobalt sulfides, followed by separating the sulfurized solution; discharge waste water, obtained by adding a neutralizing agent to the sulfurized solution to separate aluminum and manganese, is concentrated to precipitate and separate calcium contained in the discharge waste water as calcium sulfate; the resulting solution is concentrated to precipitate magnesium in the solution as magnesium sulfate; the magnesium sulfate is roasted with a reducing agent to obtain magnesium oxide and a sulfurous gas; and the magnesium oxide is washed.

METHOD FOR MANUFACTURING CALCIUM ZINCATE CRYSTALS, AND THE USES THEREOF
20180086646 · 2018-03-29 · ·

Disclosed is a method for manufacturing calcium zincate crystals including: placing calcium hydroxide.sub.2 and zinc oxide, one of the precursors thereof, or one of the water mixtures thereof in a starting suspension, the mass ratio of water to calcium hydroxide and zinc oxide, or one of the precursors or mixtures thereof, being greater than or equal to 1; milling the starting suspension to an ambient temperature less than or equal to 50 C. in a wet-phase three-dimensional micro-ball mill for a residence time less than or equal to 15 minutes and in particular from 5 to 25 seconds; recovering a calcium zincate crystal suspension coming out of the mill; and optionally, concentrating or drying the calcium zincate crystal suspension so as to obtain a calcium zincate crystal powder. Also disclosed are uses associated with the calcium zincate crystals obtained according to the method described above.

METHOD FOR MANUFACTURING CALCIUM ZINCATE CRYSTALS, AND THE USES THEREOF
20180086646 · 2018-03-29 · ·

Disclosed is a method for manufacturing calcium zincate crystals including: placing calcium hydroxide.sub.2 and zinc oxide, one of the precursors thereof, or one of the water mixtures thereof in a starting suspension, the mass ratio of water to calcium hydroxide and zinc oxide, or one of the precursors or mixtures thereof, being greater than or equal to 1; milling the starting suspension to an ambient temperature less than or equal to 50 C. in a wet-phase three-dimensional micro-ball mill for a residence time less than or equal to 15 minutes and in particular from 5 to 25 seconds; recovering a calcium zincate crystal suspension coming out of the mill; and optionally, concentrating or drying the calcium zincate crystal suspension so as to obtain a calcium zincate crystal powder. Also disclosed are uses associated with the calcium zincate crystals obtained according to the method described above.