A system for extracting vanadium from a leaching solution containing vanadium chromium silicon and for preparing vanadium pentoxide, and a method therefor, the system comprising, in sequence: an impurity removal system, an extraction system, a reverse-extraction and vanadium precipitation system, a washing system and a calcining system. The method comprises the following steps: removing silicon in a leaching solution by using a silicon removal agent, extracting most of the vanadium to an organic phase by using centrifugal extraction, reverse-extracting the vanadium of a vanadium-rich organic phase by using a mixed solution containing a basic solution and an ammonium salt, and precipitating ammonium metavanadate to obtain an ammonium metavanadate solid, washing and drying, and then calcining at a certain temperature to obtain a low chromium, low silicon, low aluminum and high-purity vanadium pentoxide product.

Disclosed herein are embodiments of low temperature co-fireable dielectric materials which can be used in conjunction with high dielectric materials to form composite structures, in particular for isolators and circulators for radiofrequency components. Embodiments of the low temperature co-fireable dielectric materials can be scheelite or garnet structures, for example, bismuth vanadate. Adhesives and/or glue is not necessary for the formation of the isolators and circulators.

In general, according to one embodiment, there is provided an active material. The active material contains a composite oxide having an orthorhombic crystal structure. The composite oxide is represented by a general formula of Li.sub.2+wNa.sub.2xM1.sub.yTi.sub.6zM2.sub.zO.sub.14+. In the general formula, the M1 is at least one selected from the group consisting of Cs and K; the M2 is at least one selected from the group consisting of Zr, Sn, V, Nb, Ta, Mo, W, Fe, Co, Mn, and Al; and w is within a range of 0w4, x is within a range of 0<x<2, y is within a range of 0y<2, z is within a range of 0<z6, and is within a range of 0.50.5.

The present invention relates to a method of making of hydrocarbon soluble metal composition comprising of one or more metals of group VIB of the periodic table, wherein the metal having 4+ oxidation state predominantly forms highly active metal sulfide catalyst for hydro-conversion of heavy oil feedstocks in liquid phase. More particularly, present invention relates to a hydrocarbon soluble metal composition comprising of reaction products of a metal source, a lipophilic phenolic acid, a surfactant and an organophosphorus compound. The present invention also provides a one-pot process for preparation of the hydrocarbon soluble metal composition comprising reacting a metal source, a lipophilic phenolic acid, a surfactant, an organophosphorus compound and water to obtain a reaction product and drying the reaction product to obtain the hydrocarbon soluble metal composition.

The present invention relates to a method of making of hydrocarbon soluble metal composition comprising of one or more metals of group VIB of the periodic table, wherein the metal having 4+ oxidation state predominantly forms highly active metal sulfide catalyst for hydro-conversion of heavy oil feedstocks in liquid phase. More particularly, present invention relates to a hydrocarbon soluble metal composition comprising of reaction products of a metal source, a lipophilic phenolic acid, a surfactant and an organophosphorus compound. The present invention also provides a one-pot process for preparation of the hydrocarbon soluble metal composition comprising reacting a metal source, a lipophilic phenolic acid, a surfactant, an organophosphorus compound and water to obtain a reaction product and drying the reaction product to obtain the hydrocarbon soluble metal composition.

Methods and systems for removing impurities from electrolyte solutions having three or more valence states. In some embodiments, a method includes electrochemically reducing an electrolyte solution to lower its valence state to a level that causes impurities to precipitate out of the electrolyte solution and then filtering the precipitate(s) out of the electrolyte solution. In embodiments in which the electrolyte solution is desired to be at a valence state higher than the precipitation valence state, a method of the disclosure includes oxidizing the purified electrolyte solution to the target valence.

Methods and systems for removing impurities from electrolyte solutions having three or more valence states. In some embodiments, a method includes electrochemically reducing an electrolyte solution to lower its valence state to a level that causes impurities to precipitate out of the electrolyte solution and then filtering the precipitate(s) out of the electrolyte solution. In embodiments in which the electrolyte solution is desired to be at a valence state higher than the precipitation valence state, a method of the disclosure includes oxidizing the purified electrolyte solution to the target valence.

A method of forming a composite material for use as an isolator or circulator in a radiofrequency device comprises providing a low temperature fireable outer material, the low fireable outer material having a garnet or scheelite structure, inserting a high dielectric constant inner material having a dielectric constant above 30 within an aperture in the low temperature fireable outer material, and co-firing the lower temperature fireable outer material and the high dielectric constant inner material together at temperature between 650-900? C. to shrink the low temperature fireable outer material around an outer surface of the high dielectric constant inner material to form an integrated magnetic/dielectric assembly without the use of adhesive or glue.

A layered double hydroxide is represented by the following formula (I): Ni.sup.2+.sub.1?(x+y+z)Fe.sup.3+.sub.xV.sup.3+.sub.yCo.sup.3+.sub.z(OH).sub.2A.sup.n?.sub.(x+y+z)/n.Math.mH.sub.2O . . . (I). In one embodiment, in the formula (I), (x+y+z) is from 0.2 to 0.5, x represents more than 0 and 0.3 or less, y represents from 0.04 to 0.49, and z represents more than 0 and 0.2 or less.

An electrode comprising a space group Pna2.sub.1 VOPO.sub.4 lattice, capable of electrochemical insertion and release of alkali metal ions, e.g., sodium ions. The VOPO.sub.4 lattice may be formed by solid phase synthesis of KVOPO.sub.4, milled with carbon particles to increase conductivity. A method of forming an electrode is provided, comprising milling a mixture of ammonium metavanadate, ammonium phosphate monobasic, and potassium carbonate; heating the milled mixture to a reaction temperature, and holding the reaction temperature until a solid phase synthesis of KVOPO.sub.4 occurs; milling the KVOPO.sub.4 together with conductive particles to form a conductive mixture of fine particles; and adding binder material to form a conductive cathode. A sodium ion battery is provided having a conductive NaVOPO.sub.4 cathode derived by replacement of potassium in KVOPO.sub.4, a sodium ion donor anode, and a sodium ion transport electrolyte. The VOPO.sub.4, preferably has a volume greater than 90 .sup.3 per VOPO.sub.4.