C07C51/00

METHODS OF SYNTHESIZING CANNABIGERGOL, CANNABIGEROLIC ACID, AND ANALOGS THEREOF

Disclosed are methods for preparing cannabigerol (CBG) or a CBG analog, embodiments of the method comprising providing a compound (I); combining the compound (I) with geraniol and a solvent to form a reaction mixture; and combining the reaction mixture with an acid catalyst to form a product mixture comprising the CBG or the CBG homolog. The method may further comprise separating the CBG or the CBG analog from the product mixture and may further comprise purifying the CBG or CBG analog. Methods for preparing cannabigerolic acid (CBGA) or a cannabigerolic acid analog are also disclosed. The present disclosure also provides highly purity CBG, CBGA, and analogs thereof.

METHODS OF SYNTHESIZING CANNABIGERGOL, CANNABIGEROLIC ACID, AND ANALOGS THEREOF

Disclosed are methods for preparing cannabigerol (CBG) or a CBG analog, embodiments of the method comprising providing a compound (I); combining the compound (I) with geraniol and a solvent to form a reaction mixture; and combining the reaction mixture with an acid catalyst to form a product mixture comprising the CBG or the CBG homolog. The method may further comprise separating the CBG or the CBG analog from the product mixture and may further comprise purifying the CBG or CBG analog. Methods for preparing cannabigerolic acid (CBGA) or a cannabigerolic acid analog are also disclosed. The present disclosure also provides highly purity CBG, CBGA, and analogs thereof.

METHOD FOR SIMULTANEOUS CONVERSION OF HYDROGEN SOURCE AND A CARBON DIOXIDE SOURCE INTO FORMATE WITH IMPROVED YIELD

Proposed is a high-yield simultaneous conversion method for a hydrogen source and a carbon dioxide source. The method significantly increases a yield of a formate through conversion of carbon dioxide. To this end, a carbon dioxide source and a hydrocarbon containing one or more hydroxy groups undergo a simultaneous conversion reaction in the presence of a solvent containing one or more alcohols and having a pH of 10 to 14.

METHOD FOR SIMULTANEOUS CONVERSION OF HYDROGEN SOURCE AND A CARBON DIOXIDE SOURCE INTO FORMATE WITH IMPROVED YIELD

Proposed is a high-yield simultaneous conversion method for a hydrogen source and a carbon dioxide source. The method significantly increases a yield of a formate through conversion of carbon dioxide. To this end, a carbon dioxide source and a hydrocarbon containing one or more hydroxy groups undergo a simultaneous conversion reaction in the presence of a solvent containing one or more alcohols and having a pH of 10 to 14.

Hemicellulose processing method

A method of processing an aqueous hemicellulosic stream containing lignin, comprising: (a) contacting an aqueous hemicellulosic stream containing lignin with a C.sub.3-8 alkyl alcohol at elevated temperature and acidic pH; (b) separating the reaction mixture obtained from step (a) into an aqueous phase containing hemicellulose-derived monosaccharide and an organic phase containing C.sub.3-8 alkyl alcohol; (c) concentrating the organic phase obtained from step (b) to remove at least some C.sub.3-8 alkyl alcohol; (d) treating the residue from step (c) with water or an aqueous medium having an alkaline pH; and (e) recovering C.sub.3-8 alkyl alcohol from the product of step (d).

Hemicellulose processing method

A method of processing an aqueous hemicellulosic stream containing lignin, comprising: (a) contacting an aqueous hemicellulosic stream containing lignin with a C.sub.3-8 alkyl alcohol at elevated temperature and acidic pH; (b) separating the reaction mixture obtained from step (a) into an aqueous phase containing hemicellulose-derived monosaccharide and an organic phase containing C.sub.3-8 alkyl alcohol; (c) concentrating the organic phase obtained from step (b) to remove at least some C.sub.3-8 alkyl alcohol; (d) treating the residue from step (c) with water or an aqueous medium having an alkaline pH; and (e) recovering C.sub.3-8 alkyl alcohol from the product of step (d).

Hemicellulose processing method

A method of processing an aqueous hemicellulosic stream containing lignin, comprising: (a) contacting an aqueous hemicellulosic stream containing lignin with a C.sub.3-8 alkyl alcohol at elevated temperature and acidic pH; (b) separating the reaction mixture obtained from step (a) into an aqueous phase containing hemicellulose-derived monosaccharide and an organic phase containing C.sub.3-8 alkyl alcohol; (c) concentrating the organic phase obtained from step (b) to remove at least some C.sub.3-8 alkyl alcohol; (d) treating the residue from step (c) with water or an aqueous medium having an alkaline pH; and (e) recovering C.sub.3-8 alkyl alcohol from the product of step (d).

Method and Apparatus for Producing Carbon Monoxide
20230061199 · 2023-03-02 ·

A method for producing carbon monoxide includes decomposing formic acid, in the presence of water, by hydrothermal reaction under conditions with a temperature T of 350° C. or less and a pressure P being equal to or more than the saturated vapor pressure of water at the temperature T.

Method and Apparatus for Producing Carbon Monoxide
20230061199 · 2023-03-02 ·

A method for producing carbon monoxide includes decomposing formic acid, in the presence of water, by hydrothermal reaction under conditions with a temperature T of 350° C. or less and a pressure P being equal to or more than the saturated vapor pressure of water at the temperature T.

FORMATE PRODUCTION METHOD AND FORMATE PRODUCTION SYSTEM
20230147963 · 2023-05-11 ·

The present invention relates to a formate production method including: a first step of producing a formate by causing a reaction between carbon dioxide and hydrogen in a solution containing a solvent, a catalyst dissolved in the solvent, and a metal salt or an organic salt; and a second step of separating, by a separation membrane, the catalyst from a reaction solution obtained in the first step, in which the catalyst contains at least one metal element selected from the group consisting of metal elements belonging to Group 8, Group 9, and Group 10 of a periodic table.