C07G99/00

MAGNESIUM SULFONATE SYNTHESIS

An overbased magnesium sulfonate detergent is made by (A) preparing a mixture of a sulfonic acid or salt with a magnesium oxide, water, a C.sub.1-C.sub.5 alkanol, a hydrocarbon solvent, and a combination of a polyisobutene succinic anhydride of molecular weight (M.sub.w) 500 to 1500 g mol.sup.1 and a salicylic acid as first and second promoters; and (B) carbonating the mixture with an acidic gas to form the overbased magnesium sulfonate.

Metal detergent and preparation method thereof and lubricant oil containing metal detergent

A metal detergent and a preparation method thereof and a lubricant oil containing the metal detergent. The metal detergent is sulfurized calcium alkyl phenolate, the method for preparing the metal detergent includes the following steps: a) mixing alkyl phenol, a calcium source and base oil to obtain a mixed solution; b) mixing the mixed solution, ethylene glycol and a sulfur source to carry out sulfurization reaction to obtain a sulfurization reaction solution; c) implementing carbonation reaction between the sulfurization reaction solution and CO.sub.2 to obtain a carbonation reaction solution; and d) extracting the carbonation reaction solution with a solvent, upon refining, to obtain sulfurized calcium alkyl phenolate; wherein the solvent includes solvent oil, water and oxygenous derivative of hydrocarbon. Experimental results show that the content of free alkyl phenol is below 1.5 wt % in the sulfurized calcium alkyl phenolate prepared using the preparation method provided by the present application.

ULTRASONIC REACTION FOR HIGH-YIELD PRODUCTION OF HUMIC ACIDS FROM COAL-LIGNITE, OXIDIZED COALS, AND RESIDUAL FEEDSTOCKS

Processes are disclosed for the ultrasonic functionalization and extraction of humic acids from carbonaceous feedstocks, in the presence of an oxidant in an alkaline extraction media. Humate fertilizers are provided by these processes, comprising potassium and nitrogen modified humic acids.

ULTRASONIC REACTION FOR HIGH-YIELD PRODUCTION OF HUMIC ACIDS FROM COAL-LIGNITE, OXIDIZED COALS, AND RESIDUAL FEEDSTOCKS

Processes are disclosed for the ultrasonic functionalization and extraction of humic acids from carbonaceous feedstocks, in the presence of an oxidant in an alkaline extraction media. Humate fertilizers are provided by these processes, comprising potassium and nitrogen modified humic acids.

Control of phytopathogenic microorganisms with Pseudomonas sp. and substances and compositions derived therefrom

Provided are compounds and compositions derived from Pseudomonas sp., particularly, Pseudomonas fluorescens or Pseudomonas protegens and more particularly strain having the identifying characteristics of Pseudomonas ATCC 55799 having antimicrobial properties and particularly, antibacterial properties.

Control of phytopathogenic microorganisms with Pseudomonas sp. and substances and compositions derived therefrom

Provided are compounds and compositions derived from Pseudomonas sp., particularly, Pseudomonas fluorescens or Pseudomonas protegens and more particularly strain having the identifying characteristics of Pseudomonas ATCC 55799 having antimicrobial properties and particularly, antibacterial properties.

Heterologous Hosts

This invention is related to bacterial engineering and the heterologous expression of useful compounds. In particular, the invention relates to a heterologous host that has been engineered for expression of a gene which is capable of polyketide or non-ribosomal peptide synthesis. Methods of treating cancer are also disclosed.

Heterologous Hosts

This invention is related to bacterial engineering and the heterologous expression of useful compounds. In particular, the invention relates to a heterologous host that has been engineered for expression of a gene which is capable of polyketide or non-ribosomal peptide synthesis. Methods of treating cancer are also disclosed.

Method for preparing a sulfurized alkaline earth metal dodecylphenate

A sulfurized alkaline earth metal (e.g., calcium) dodecylphenate is prepared by reacting (i) dodecylphenol with (ii) calcium hydroxide or calcium oxide in an amount of about 0.3 to about 0.7 moles per mole of dodecylphenol charged and (iii) an alkylene glycol in an amount of about 0.13 to about 0.6 moles per mole of dodecylphenol charged; and reacting the product of the first step with sulfur in an amount of about 1.6 to about 3 moles per mole of dodecylphenol charged; and thereafter optionally reacting the product with additional calcium hydroxide or calcium oxide and with carbon dioxide so as to form an overbased phenate. The product thus prepared has reduced levels of monomeric dodecylphenol.

Method for preparing a sulfurized alkaline earth metal dodecylphenate

A sulfurized alkaline earth metal (e.g., calcium) dodecylphenate is prepared by reacting (i) dodecylphenol with (ii) calcium hydroxide or calcium oxide in an amount of about 0.3 to about 0.7 moles per mole of dodecylphenol charged and (iii) an alkylene glycol in an amount of about 0.13 to about 0.6 moles per mole of dodecylphenol charged; and reacting the product of the first step with sulfur in an amount of about 1.6 to about 3 moles per mole of dodecylphenol charged; and thereafter optionally reacting the product with additional calcium hydroxide or calcium oxide and with carbon dioxide so as to form an overbased phenate. The product thus prepared has reduced levels of monomeric dodecylphenol.