Provided are a quality inspection method and a quality inspection system for unvulcanized rubber material. A final dielectric constant measurement device detects the dielectric constant of a final rubber material in which a compounding agent of predetermined type is mixed with unvulcanized rubber, and a calculator calculates a compounding ratio of the compounding agent to the final rubber material based on the detected dielectric constant, determines whether or not the calculated compounding ratio is in a preset compounding reference range, displays a determination result on a monitor, and adjusts a ratio of the compounding agent fed into an extruder to the unvulcanized rubber such that the calculated compounding ratio is within the compounding reference range.

A material is provided which comprises cellulose fine fibers and which is capable of suitably acting on resin or rubber uniformly on a high level, and of generating superior action when added to a resin composition. As such a material, cellulose xanthate fine fibers are contained in a resin composition or a resin dispersion.

The disclosure relates to methods for producing poly(cyclohexadiene) homopolymers (PCHD). The PCHD is formed by polymerizing a 1,3-cyclohexadiene monomer in the presence of a catalyst, in a hydrocarbon solvent, and at a temperature of −100° C. to 120° C. The catalyst is selected from the group consisting of a Bronsted acid, a Lewis acid, and combinations thereof. PCHD produced under these conditions has good solubility in non-polar solvents, and a number average molecular weight of 300 to 5,000 Dalton; a weight average molecular weight of 5,000 to 15,000 Delton; and a polydispersity index of 3.0 to 8.0. The PCHD is useful for producing crosslinked materials having good physical properties. The crosslinked materials can be combined with a rubbery polymer to produce compositions valuable for further downstream uses.

Disclosed herein are copolymers formed by cationic polymerfization of one or more cyclic dienes and a comonomer selected from the group consisting of a monoterpene, a branched styrene, and combinations thereof, in the presence of a catalyst. Random copolymers having repeat units derived from a cyclic conjugated diene, such as 1,3-cyclohexadiene, and a comonomer such as a monoterpene, can be prepared as soluble products in hydrocarbon solvents. The copolymers can be crosslinked with various crosslinking agents to form materials having good oxidative stability and fire retardancy. The uncrosslinked and crosslinked copolymers have useful properties such as a low dissipation factor, low dielectric constants, and a good balance of thermomechanical and electrical properties that make them valuable in electronic applications.

Provided are a quality inspection method and a quality inspection system for unvulcanized rubber material. A final dielectric constant measurement device detects the dielectric constant of a final rubber material in which a compounding agent of predetermined type is mixed with unvulcanized rubber, and a calculator calculates a compounding ratio of the compounding agent to the final rubber material based on the detected dielectric constant, determines whether or not the calculated compounding ratio is in a preset compounding reference range, displays a determination result on a monitor, and adjusts a ratio of the compounding agent fed into an extruder to the unvulcanized rubber such that the calculated compounding ratio is within the compounding reference range.

A material is provided which comprises cellulose fine fibers and which is capable of suitably acting on resin or rubber uniformly on a high level, and of generating superior action when added to a resin composition. As such a material, cellulose xanthate fine fibers are contained in a resin composition or a resin dispersion.

The disclosure relates to methods for producing poly(cyclohexadiene) homopolymers (PCHD). The PCHD is formed by polymerizing a 1,3-cyclohexadiene monomer in the presence of a catalyst, in a hydrocarbon solvent, and at a temperature of 100 C. to 120 C. The catalyst is selected from the group consisting of a Bronsted acid, a Lewis acid, and combinations thereof. PCHD produced under these conditions has good solubility in non-polar solvents, and a number average molecular weight of 300 to 5,000 Dalton; a weight average molecular weight of 5,000 to 15,000 Delton; and a polydispersity index of 3.0 to 8.0. The PCHD is useful for producing crosslinked materials having good physical properties. The crosslinked materials can be combined with a rubbery polymer to produce compositions valuable for further downstream uses.

A process for manufacturing an ultra-high thermally conductive graphene curing bladder includes the following steps: (1) pre-mixing an ultra-high thermally conductive graphene with rubber to obtain a pre-dispersed graphene master batch, performing a granulation process or a cutting process on the pre-dispersed graphene master batch to obtain a granular solid or a sheet solid, mixing the solid in a rubber mixing mill to obtain an ultra-high thermally conductive graphene rubber compound; (2) extruding, by an extruding machine, the ultra-high thermally conductive graphene rubber compound into a rubber strip of a desirable size; weighing and fixed-length processing the rubber strip of the ultra-high thermally conductive graphene rubber compound to obtain a rubber blank, placing the rubber blank into a pressing type curing bladder mold, closing the mold, pressurizing, heating and curing to obtain a finished product of the ultra-high thermally conductive graphene curing bladder.

A process for manufacturing an ultra-high thermally conductive graphene curing bladder includes the following steps: (1) pre-mixing an ultra-high thermally conductive graphene with rubber to obtain a pre-dispersed graphene master batch, performing a granulation process or a cutting process on the pre-dispersed graphene master batch to obtain a granular solid or a sheet solid, mixing the solid in a rubber mixing mill to obtain an ultra-high thermally conductive graphene rubber compound; (2) extruding, by an extruding machine, the ultra-high thermally conductive graphene rubber compound into a rubber strip of a desirable size; weighing and fixed-length processing the rubber strip of the ultra-high thermally conductive graphene rubber compound to obtain a rubber blank, placing the rubber blank into a pressing type curing bladder mold, closing the mold, pressurizing, heating and curing to obtain a finished product of the ultra-high thermally conductive graphene curing bladder.

A resin infusion method that includes: (a) heating a mixture of solid amine compounds until all amine compounds are melted; (b) cooling the mixture of melted amine compounds to a temperature of 35 C. or lower to form an amine blend (A); (c) combining the amine blend (A) with a thermosettable resin (B), which includess one or more epoxy monomers, at a temperature effective for forming a liquid resin composition; and (d) infusing a fibrous preform with the liquid resin composition. The amine blend (A) contains an aromatic diamine represented by Structure 1 or 2:

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