It is an object of the present invention to provide a grease composition, for an outer ring rotation type rolling bearing, which is capable of satisfying all of high-temperature durability, low-temperature property, peeling resistance, and rust-preventive property. A grease composition (7) to be enclosed in the outer rig rotation type rolling bearing for use in automotive electric auxiliary machines contains base oil, a thickener, a peeling-resistant additive, a wear-resistant additive, and a rust-preventive agent. The base oil is mixed oil of trimellitic acid ester oil and synthetic hydrocarbon oil mixed therewith in a mass ratio of (70:30) to (90:10). The thickener consists of a diurea compound shown by a formula (1).
R.sup.1NHCONHR.sup.2NHCONHR.sup.1(1)
wherein a reference symbol R.sup.2 denotes a divalent aromatic hydrocarbon group having a carbon number of 6 to 15, and a reference symbol R.sup.1 denotes a cyclohexyl group.

A lubricating oil composition including greater than 50 wt. % of a base oil, from 100 ppm to less than 1800 ppm by weight of total metal from metal-containing detergent(s) including an overbased calcium detergent and a magnesium containing detergent. The composition has a total nitrogen of 900 ppm to less than 1600 ppm by weight, and a ratio of total metal from the detergent(s) in ppm to the total nitrogen in ppm of less than 1.9. The composition also includes a borated compound to provide greater than 50 ppm by weight to 1000 ppm by weight of boron, and a ppm ratio of metal from the detergent(s) in ppm to the total boron is less than 7.5 and a molybdenum compound to provide greater than 80 ppm to 1200 ppm by weight molybdenum and a ppm ratio of total metal from the detergent(s) to the molybdenum is less than 23.8.

Methods of making antidegradant compounds are disclosed in which a p-phenylenediamine is reacted with a dicarbonyl to thereby obtain a diimine, which is reduced to obtain mixtures comprising the antidegradant compound.

A lubricating oil additive composition containing a polymer-based compound may be excellent in solubility in a mineral oil and wear resistance, and favorable as a friction modifier. A lubricating oil composition may contain the additive composition. Such a lubricating oil additive composition may contain a copolymer (X) containing: (a) a structural unit derived from a monomer (A) having a (meth)acryloyl group and a linear or branched alkyl group having 6 to 24 carbon atoms; (b) a structural unit derived from a monomer (B) having a (meth)acryloyl group and a polar group; and (c) a structural unit derived from a monomer (C) having a polymerizable functional group and a cyclic structure group. The copolymer (X) may have a content of the structural unit (a) of 43% by mol or more based on the total structural units of the copolymer (X), and a mass average molecular weight (Mw) of 5,000 to 90,000.

A lubricating oil composition and method of operating a boosted internal combustion engine. The lubricating oil composition is formulated to be resistant to turbocharger deposit formation in the boosted internal combustion engine, as shown by its ability to ensure a TCO Temperature Increase of less than 9.0% as measured using the 2015 version of the General Motors Dexos1 Turbocharger Coking Test. The lubricating oil composition may also have a low NOACK volatility, as measured by the method of ASTM D-5800 at 250 C.

A lubricating oil composition and method of operating a boosted internal combustion engine. The lubricating oil composition includes greater than 50 wt. % of a base oil, one or more overbased calcium sulfonate detergent(s) and one or more overbased calcium phenate detergent(s). The calcium, boron, nitrogen, and amount of soap are maintained within certain ratios, and the total base number contribution from all detergents to the lubricating oil composition is less than 4.2 mg KOH/g of the lubricating oil composition, as measured by the method of ASTM D-2896. The lubricating oil composition and method may be effective to reduce low-speed pre-ignition events in a boosted internal combustion engine lubricated with the lubricating oil composition relative to capable lubricating oil compositions.

A lubricating oil composition prepared by blending a base oil (A) containing a compound (A1) that is an ester or ether and has two or more aromatic rings, with a polyalkylene glycol (B) is provided. The lubricating oil composition has a high density (i.e., a high bulk modulus), a high viscosity index, and excellent shear stability.

The present invention relates to non-flammable compositions comprising chlorotrifluoropropene with reduced risk of flammability which are useful as refrigerants, heat transfer fluids, solvents, cleaners, blowing agents, aerosols, extraction fluids, and the like.

A method of increasing the spreading of a lubricant on the liner surface after it's delivery, wherein the method comprises preparing the lubricant compositions comprising copolymers of monomers (A) selected from C6-C10 alkyl methacrylate monomers, and monomers (B) selected from C10-C18 alkyl methacrylate monomers, and a base oil or comprising a copolymer obtained by combining at least monomers (A) selected from C6-C10 alkyl methacrylate monomers, and monomers (B) selected from C10-C18 alkyl methacrylate monomers in a mixture and co-polymerizing the monomers for increasing the spreading and/or the self-spreading of the lubricant on the cylinder liner surface after its delivery.

A method for preventing or reducing low speed pre-ignition in an engine lubricated with a lubricating oil by using as the lubricating oil a formulated oil. The formulated oil has a composition including a lubricating oil base stock as a major component, and at least one lubricating oil additive, as a minor component. The lubricating oil contains at least one metal or metalloid in an amount sufficient that, in thermogravimetric measurements of the lubricating oil by a Thermogravimetric Engine Oil Simulation Test, carbon black decomposition temperature is increased as compared to the carbon black decomposition temperature in a lubricating oil containing calcium or magnesium. A lubricating oil useful for preventing or reducing low speed pre-ignition in an engine lubricated with the lubricating oil. The lubricating oils of this disclosure are particularly advantageous as passenger vehicle engine oil (PVEO) products.