The present disclosure is generally directed to methods for purifying cannabinoids from Cannabis plants.

Methods of using silica-zirconia catalysts in processes to reduce an amount of glycidol, glycidyl ester(s), or both glycidol and glycidyl ester(s) from a triglyceride-containing composition, such as edible oils, are disclosed. Silica-zirconia catalysts and methods of making silica-zirconia catalysts are also disclosed.

A method for producing biodiesel using a sulfonated, carbonaceous catalyst produced from rice husk, Moringa seeds, or algae biomass, a method for producing the catalyst, and the catalyst itself.

A system for treating whole stillage includes a stillage tank, a separation system in communication with the stillage tank and configured to separate the whole stillage into a wet cake portion and a thin stillage portion, and a primary filtration system in communication with the separation system. The primary filtration system can be configured to separate the thin stillage into a primary concentrate and a primary permeate. A secondary filtration system in communication with the primary filtration system can be configured to further purify the primary permeate. A water reclamation system in communication with the primary and/or secondary filtration system can remove water from the permeate. An additive can be added to the primary permeate to precipitate phosphorus-containing minerals and corn oil can be advantageously extracted from the primary concentrate. Protein-enriched animal feeds can be generated from dehydration of the primary concentrate.

Remediating hemp oil includes controlling heat and oxygenation levels to reduce the relative weight percentage of THC while mitigating the conversion of other cannabinoids to other compounds. The method may include bubbling air, oxygen, or another oxygen-containing gas into a reactor while maintaining the temperature of the hemp oil.

In an aspect, a method is disclosed that includes contacting a composition with an aqueous solution to yield a mixture, where the composition includes one or more of animal fats, animal oils, plant fats, plant oils, vegetable fats, vegetable oils, greases, and used cooking oil, about 5 wt. % or more of free fatty acids, about 10 wppm or more of total metals, about 8 wppm or more phosphorus, about 20 wppm or more of nitrogen, and the aqueous solution includes ((NH.sub.4).sub.2H.sub.2EDTA, (NH.sub.4).sub.4EDTA, a monoammonium salt of diethylenetriaminepentaacetic acid, a diammonium salt of diethylenetriaminepentaacetic acid, a triammonium salt of diethylenetriaminepentaacetic acid, a tetraammonium salt of diethylenetriaminepentaacetic acid, (NH.sub.4).sub.5DTPA, a combination of citric acid and Na.sub.4EDTA, a combination of citric acid and Na.sub.2H.sub.2EDTA, a combination of citric acid and a monosodium salt of diethylenetriaminepentaacetic acid, a combination of citric acid and a disodium salt of diethylenetriaminepentaacetic acid, a combination of citric acid and a trisodium salt of diethylenetriaminepentaacetic acid, a combination of citric acid and a tetrasodium salt of diethylenetriaminepentaacetic acid, a combination of citric acid and Na.sub.5DTPA, or a combination of any two or more thereof, where the method further includes centrifuging the mixture to yield a first treated composition, wherein the first treated composition has less total metals and less phosphorus than the composition.

The present invention provides an improved method for purification of a primary triacylglyceride oil comprising the steps of washing the primary triacylglyceride oil, trapping assisted removal of chlorinated precursors of MCPDEs by admixing the primary triacylglyceride oil with an auxiliary trapping agent; crystallising the auxiliary trapping agent or the primary triacylglyceride oil; and separating solid and liquid phases of the product.

The present invention provides an improved method for purification of a primary triacylglyceride oil comprising the steps of washing the primary triacylglyceride oil, trapping assisted removal of chlorinated precursors of MCPDEs by admixing the primary triacylglyceride oil with an auxiliary trapping agent; crystallising the auxiliary trapping agent or the primary triacylglyceride oil; and separating solid and liquid phases of the product.

There is a method for extracting bio-oil from algal biomass, in particular oily microalgae, using solvents of a Deep Eutectic Solvents (DES) capable of producing a bio-oil with a low content of phospholipids and inorganic salts, mainly sodium chloride.

The present invention relates to a polyunsaturated fatty acid composition comprising Omega-3 fatty acids, 17-HDHA and 18-HEPE. The composition can furthermore comprise DPA and/or an acceptable carrier and can be present in a capsule or other suitable dosage unit. The invention also relates to the process of obtaining the composition and methods for using same.