C22B3/00

METHOD FOR PRODUCING MIXED METAL SOLUTION AND METHOD FOR PRODUCING MIXED METAL SALT

A method for producing a mixed metal solution containing manganese ions and at least one of cobalt ions and nickel ions, the method including: an Al removal step of subjecting an acidic solution containing at least manganese ions and aluminum ions, and at least one of cobalt ions and nickel ions, to removal of the aluminum ions by extracting the aluminum ions into a solvent while leaving at least a part of the manganese ions in the acidic solution in an aqueous phase, the acidic solution being obtained by subjecting battery powder of lithium ion batteries to a leaching step; and a metal extraction step of bringing an extracted residual liquid obtained in the Al removal step to an equilibrium pH of 6.5 to 7.5 using a solvent containing a carboxylic acid-based extracting agent, extracting at least one of the manganese ions and at least one of the cobalt ions and the nickel ions into the solvent, and then back-extracting the manganese ions and at least one of the cobalt ions and nickel ions.

Method And Apparatus For Recycling Lithium-Ion Batteries
20230198040 · 2023-06-22 ·

Cathode material from exhausted lithium ion batteries are dissolved in a solution for extracting the useful elements Co (cobalt), Ni (nickel), Al (Aluminum) and Mn (manganese) to produce active cathode materials for new batteries. The solution includes compounds of desirable materials such as cobalt, nickel, aluminum and manganese dissolved as compounds from the exhausted cathode material of spent cells. Depending on a desired proportion, or ratio, of the desired materials, raw materials are added to the solution to achieve the desired ratio of the commingled compounds for the recycled cathode material for new cells. The desired materials precipitate out of solution without extensive heating or separation of the desired materials into individual compounds or elements. The resulting active cathode material has the predetermined ratio for use in new cells, and avoids high heat typically required to separate the useful elements because the desired materials remain commingled in solution.

Systems and Methods for Recovering Lithium from Brines
20230192503 · 2023-06-22 ·

Systems and methods using solar evaporation to preconcentrate lithium containing brines to at or near lithium saturation, followed by a separation processes to separate lithium from impurities. A separated impurity stream is recycled to a point in the evaporation sequence where conditions are favorable for their precipitation and removal or disposed in a separate evaporation pond or reinjected underground, while a lower impurity stream is transferred to one or more of the removal location, to a subsequent pond in the sequence, or to a lithium plant or concentration facility. Further concentration of lithium by evaporation can then take place because impurities are removed thus eliminating lithium losses due to co-precipitation and achieving significantly higher concentrations of lithium.

FERRONICKEL ALLOY DIRECT REFINING PROCESSES AND PROCESSES FOR PRODUCING NICKLE SULFATE OR OTHER NICKEL PRODUCTS

Processes and methods for refining ferronickel alloy, and producing nickel sulfate or other nickel product, are provided, where the ferronickel alloy is treated with an oxidizing leach. The oxidizing leach may be, for example, a pressure oxidation (POX) leach or a leach with peroxide or copper (II) ions. The treatment may be in the presence of added copper, such as by providing a copper sulfate solution. Producing nickel sulfate may comprise removing copper and iron after the leach, removing impurities, and either crystallizing the nickel sulfate or precipitating/winning another nickel product.

Process for the recovery of gold from anode slimes
09839885 · 2017-12-12 · ·

An apparatus for the recovery of gold from a gold-bearing aqueous filtrate, the process comprising the steps of: (A) Contacting the aqueous filtrate with dibutyl carbitol (DBC) in a two-stage solvent extraction process to remove the gold from the aqueous filtrate into the DBC to form a gold-loaded DBC; and (D) Contacting the gold-loaded DBC with an aqueous acid scrub of hydrochloric acid in a four-stage countercurrent scrub process to remove impurities, e.g., non-gold metal, from the DBC into the aqueous scrub solution to form an impurity-loaded aqueous scrub. Each stage of the solvent extraction circuit and the aqueous acid scrub circuit is equipped with a mixing assembly and a phase separation tank in a head-tail arrangement such that the mixing assembly of one stage is adjacent to the phase separation tank of the adjacent stage.

Method for recovering a copper sulfide concentrate from an ore containing an iron sulfide

In a method for recovering a copper sulfide concentrate by froth flotation from an ore containing an iron sulfide, wet grinding of the ore with grinding media made of high chromium cast iron alloy having a chromium content of from 10 to 35% by weight is combined with an addition of hydrogen peroxide to the conditioned mineral pulp before or during flotation in order to improve concentrate grade and recovery of copper sulfides.

PROCESS FOR REMOVING PRECIOUS METAL FROM PRECIOUS METAL-CONTAINING CATALYST FORM BODIES

Process for removing precious metal from precious metal-containing catalyst form bodies comprising form bodies and precious metal, whereby the precious metal to be removed is at least one precious metal selected from the group consisting of Au, Ag, Pd, Pt, Ir, Rh, Ru, Os, and Re, comprising the steps of: (a) producing a mixture of precious metal-containing catalyst form bodies in at least one mineral acid that is at least 1N; (b) supplying inert or oxidising gas into the mixture containing noble metal-containing catalyst form bodies and mineral acid; (c) introducing at least one oxidation agent, in solid or liquid form, into the mixture containing noble metal-containing catalyst form body and mineral acid; and (d) separating the form bodies from the liquid.

Heap Leaching Method
20170349972 · 2017-12-07 ·

A method for recovering one or more of copper, uranium and a precious metal from an ore material, including: (a) forming a heap of the ore material; (b) during active heap irrigation, contacting the heap of the ore material with an iron containing acidic leach liquor having a high chloride content in the presence of an oxygen containing gas, and producing a pregnant leach solution; and (c) recovering one or more of copper, uranium and a precious metal from the pregnant leach solution.

Processes for recycling spent catalysts, recycling rechargeable batteries, and integrated processes thereof

Integrated recycling method and processes including recycling spent catalyst to produce one or more water-soluble metal salts and one or more water-insoluble tail byproducts, and recycling rechargeable batteries to produce one or more battery-grade metals and one or more pure metallic byproducts, wherein the water insoluble tail byproduct is a feedstock in recycling the rechargeable batteries, the impure metallic byproduct is a feedstock in recycling the spent catalyst, or both.

METHOD FOR PRODUCING ELECTROLYTE FOR VANADIUM BATTERIES FROM OIL SAND WASTE
20170349971 · 2017-12-07 · ·

A method for recovering Vanadium from a secondary source such as fly ash. Leaching is involved using single or combined acids such as hydrochloric and sulfuric in a temperature range of 20° C. and 100° C. The leaching is performed in sequential operations with recovery of Vanadium in the range of 92%. The recovered Vanadium can be formulated into an electrolyte for redox batteries