Provided is a method for obtaining a solution having a high concentration of nickel and/or cobalt from an alloy that contains copper as well as nickel and/or cobalt, in a waste lithium-ion battery. A method for treating an alloy comprises: a leaching step S1 for subjecting an alloy that contains copper as well as nickel and/or cobalt to a leaching treatment by using an acid solution in the presence of a sulfiding agent to obtain a leachate and a leaching residue; and a reduction step S2 for adding a reducing agent to a part of the obtained leachate and performing a reduction treatment to obtain a post-reduction solution and a reduction residue, wherein in the leaching step S1, the leachate that has not been provided in the reduction treatment in the reduction step S2, is repeatedly used as part or all of the acid solution added in the leaching treatment.

Provided is a method that is for producing, from a raw material containing an oxide including nickel and cobalt, a valuable metal containing said nickel and cobalt, and that enables the degree of reduction of an alloy obtained through a melting process to be adjusted efficiently and properly. The method comprises: a melting step for obtaining a melted product; and a slag separation step for separating a slag from the melted product and recovering an alloy containing the valuable metal. In the melting step, the degree of reduction in the melting process is determined on the basis of the proportion of the amount of cobalt (cobalt recovery rate) in the produced alloy, with respect to the amount of cobalt in the raw material, and, if the degree of reduction is determined to be excessive, the raw material containing an oxide including nickel and cobalt is added as an oxidizer.

The present invention relates to a method of simultaneously recovering cobalt (Co) and manganese (Mn) from lithium-based BATTERY, and more particularly, to a method that is capable of simultaneously recovering cobalt and manganese from lithium-based BATTERY, i.e., recycled resources that contain large amounts of cobalt and manganese, with high purities using multistage leaching and electrowinning methods. According to the method of the present invention, cobalt and manganese can be simultaneously recovered from lithium-based BATTERY as recycled resources, and a recovery method that is cost-effective compared to conventional methods can be provided.

This invention relates to a process for recovering valuable metals from ore with significantly reduced water consumption through the discrete treatment and storage of coarse tailings. Ore is ground to produce a coarse particulate ore. The coarse particulate ore is treated in a coarse flotation stage to produce a low grade concentrate fraction and a coarse tailings fraction. The low grade concentrate fraction is treated to produce fine tailings and a saleable concentrate. The coarse tailings are treated separately from the fine tailings and water is recovered from the coarse tailings by hydraulically stacking; filtering or screening, whereafter the coarse tailings are dry stacked, without being recombined with the fine tailings.

Provided is a method for manufacturing a nickel and cobalt mixed sulfide that is capable of stabilizing nickel and cobalt concentrations in the sulfidation end solution at low levels and of limiting decreases in nickel and cobalt recovery rates without increasing cost even when processing with a sulfuric acid acidic solution containing nickel and cobalt and a high iron ions concentration as the sulfidation start solution. This method generates a sulfidation reaction by blowing hydrogen sulfide gas into a sulfuric acid acidic solution comprising nickel and cobalt to obtain a mixed sulfide, wherein: the sulfuric acid acidic solution, which is the sulfidation start solution, contains iron ions at a rate of 1.0-4.0 g/L; and the sulfidation reaction is generated by blowing hydrogen sulfide gas into the sulfidation start solution and adding sodium hydrogensulfide (NaHS) obtained by absorbing hydrogen sulfide gas-containing exhaust gas, generated by the sulfidation, in an alkaline solution.

Provided is a method for manufacturing a nickel and cobalt mixed sulfide that is capable of stabilizing nickel and cobalt concentrations in the sulfidation end solution at low levels and of limiting decreases in nickel and cobalt recovery rates without increasing cost even when processing with a sulfuric acid acidic solution containing nickel and cobalt and a high iron ions concentration as the sulfidation start solution. This method generates a sulfidation reaction by blowing hydrogen sulfide gas into a sulfuric acid acidic solution comprising nickel and cobalt to obtain a mixed sulfide, wherein: the sulfuric acid acidic solution, which is the sulfidation start solution, contains iron ions at a rate of 1.0-4.0 g/L; and the sulfidation reaction is generated by blowing hydrogen sulfide gas into the sulfidation start solution and adding sodium hydrogensulfide (NaHS) obtained by absorbing hydrogen sulfide gas-containing exhaust gas, generated by the sulfidation, in an alkaline solution.

Methods for forming interconnects that include cobalt. An interconnect opening is formed in a dielectric layer that penetrates from a top surface of the dielectric layer into the dielectric layer. A first cobalt layer is formed at a bottom of the interconnect opening and partially fills the interconnect opening. A second cobalt layer is selectively deposited on the first cobalt layer and grows upwardly from the first cobalt layer at the bottom of the interconnect opening.

A process of treating complex sulfide concentrate includes the steps of roasting wet or slurried complex sulfide concentrate in a furnace at a temperature of at least 720 C. to obtain a calcine; smelting the calcine under inert or oxygen free atmosphere in a smelting furnace to obtain a matte, and optionally granulating the matte to obtain a granulated matte.

There is provided a method capable of effectively reducing the amount of acid used in a leaching step and the amount of a neutralizer used in a final neutralization step while nickel yield in a hydrometallurgical process for nickel oxide ore is not reduced. A method for pre-treating ore slurry according to the present invention is a method for pre-treating ore slurry to be provided to a leaching treatment in a hydrometallurgical process for nickel oxide ore, the method including: a first separation step for separating ore slurry into a coarse particle fraction and a fine particle fraction; a second separation step for separating the coarse particle fraction separated in the first separation step into a heavy specific gravity fraction and a light specific gravity fraction; and a vibration sieving step for separating, by a vibration sieve, the light specific gravity fraction.

Provided is a gravity separation device wherein occurrences of shelving, flashing, and the like inside the device can be suppressed, variations in the flow rate of underflow obtained by gravity separation can be minimized and underflow can be stably extracted. This gravity separation device, which separates overflow and underflow using differences in specific gravity from mixed material, is provided with a separation section that has a supply pipe for supplying a slurry of the mixed material at the top and separates that slurry into overflow and underflow, and a deposition section that is positioned below the separation section and wherein the underflow that has been separated by precipitation is deposited. An extraction pipe for extracting the underflow is connected to the deposition section, and a valve for extracting the underflow and a metering pump for quantitatively extracting the underflow are provided in the extraction pipe.