C22B23/00

Recovering heavy rare earth metals from magnet scrap

A method of treating rare earth metal-bearing permanent magnet scrap, waste or other material in a manner to recover the heavy rare earth metal content separately from the light rare earth metal content. The heavy rare earth metal content can be recovered either as a heavy rare earth metal-enriched iron based alloy or as a heavy rare earth metal based alloy.

PROCESSING METHOD OF POSITIVE ELECTRODE ACTIVE SUBSTANCE WASTE OF LITHIUM ION SECONDARY BATTERY

A method for processing positive electrode active material waste of lithium ion secondary batteries, the waste containing cobalt, nickel, manganese and lithium, the method including: a carbon mixing step of mixing the positive electrode active material waste in the form of powder with carbon to obtain a mixture having a ratio of a mass of carbon to a total mass of the positive electrode active material waste and the carbon of from 10% to 30%; a roasting step of roasting the mixture at a temperature of from 600° C. to 800° C. to obtain roasted powder; a dissolution step including a first dissolution process of dissolving lithium in the roasted powder in water or a lithium-containing solution, and a second dissolution process of dissolving the lithium in a residue obtained in the first dissolution process in water; and an acid leaching step of leaching a residue obtained in the lithium dissolution step with an acid.

REAGENT COMPOSITIONS FOR METAL SOLVENT EXTRACTION AND METHODS OF PREPARATION AND USE THEREOF
20210381080 · 2021-12-09 ·

Disclosed are reagent compositions for metal solvent extraction and methods of preparation and use thereof. In certain embodiments, the disclosure relates to recovering metal values from an aqueous process stream using solvent extraction and employing a mixture of oxime reagents that synergistically improves metal recovery, rate of degradation and/or metal selectivity.

RECOVERY OF CRITICAL ELEMENTS FROM END-OF-LIFE LITHIUM ION BATTERIES WITH SUPPORTED MEMBRANE SOLVENT EXTRACTION
20210376400 · 2021-12-02 ·

Single-stage and multi-stage systems and methods for the recovery of critical elements in substantially pure form from lithium ion batteries are provided. The systems and methods include supported membrane solvent extraction using an immobilized organic phase within the pores of permeable hollow fibers. The permeable hollow fibers are contacted by a feed solution on one side, and a strip solution on another side, to provide the simultaneous extraction and stripping of elements from dissolved lithium ion cathode materials, while rejecting other elements from the feed solution. The single- and multi-stage systems and methods can selectively recover cobalt, manganese, nickel, lithium, aluminum and other elements from spent battery cathodes and are not limited by equilibrium constraints as compared to traditional solvent extraction processes.

SYSTEMS AND METHODS FOR GENERATING HYDROGEN AND MAGNETITE FROM ROCK
20230271827 · 2023-08-31 ·

Systems and methods for sequestering carbon, evolving hydrogen gas, producing iron oxide as magnetite, and producing magnesium carbonate as magnesite through sequential carbonation and serpentinization/hydration reactions involving processed olivine- and/or pyroxene-rich ores, as typically found in mafic and ultramafic igneous rock. Precious or scarce metals, such nickel, cobalt, chromium, rare earth elements, and others, may be concentrated in the remaining ore to facilitate their recovery from any gangue material.

PROCESSES FOR TREATING SCRAP METAL MATERIAL
20220154309 · 2022-05-19 ·

There is provided a process for treating particulate scrap material. The process includes emplacing the particulate scrap material and a reagent material within a calcining zone with effect that a reactive process is effected such that a calcined metal material product is obtained, and carbonylating a carbonylation precusor material with effect that a carbonylated product is obtained, wherein the carbonylation precursor material is derived from the calcined metal material product.

ALLOY POWDER, METHOD FOR MANUFACTURING SAME, AND METHOD FOR RECOVERING VALUABLE METAL
20230256507 · 2023-08-17 · ·

Provided are: an alloy powder in which nickel and cobalt can be easily dissolved in an acid and stably leached with an acid; a manufacturing method with which an alloy powder that enables stable acid leaching can be obtained at low cost; and a method for recovering a valuable metal using the manufacturing method. An alloy powder according to the present invention includes copper (Cu), nickel (Ni), and cobalt (Co) as constituents, has a 50% cumulative diameter (D50) of 30 .Math.m to 85 .Math.m in the volume particle size distribution, and has an oxygen content of 0.01 mass% to 1.00 mass%.

PROCESSING THERMALLY PRETREATED AND UNTREATED BATTERIES AND THEIR PRODUCTION REJECTS
20230253641 · 2023-08-10 ·

Embodiments of the present invention relate to a system for processing battery waste. The system comprises a decomposing device for mechanically decomposing the battery waste to a, in particular strip-shaped or flake-shaped, lightweight portion and a heavyweight portion. The decomposing device comprises an outlet for commonly discharging the lightweight portion and the heavyweight portion. The system further comprises a separating unit for separating the lightweight portion from the heavyweight portion, wherein the separating unit is coupled with the decomposing device for receiving the lightweight portion and the heavyweight portion. The system further comprises a fiber compactor unit, wherein the fiber compactor unit is coupled with the separating unit for receiving the lightweight portion. The fiber compactor unit is configured for compacting the lightweight portion under a separation of a further active material.

Method for separating copper, and nickel and cobalt

Provided is a method for separating copper from nickel and cobalt, which can efficiently and selectively separate copper from nickel and cobalt in a substance containing copper, nickel, and cobalt in a waste lithium ion battery, etc. In this method, a substance containing copper, nickel, and cobalt is sulfurated to obtain a sulfide, the obtained sulfide that contains copper, nickel, and cobalt is brought into contact with an acid solution to obtain a solid containing copper and a leachate containing nickel and cobalt. The sulfide preferably contains copper sulfide as a main component, and contains nickel metal and cobalt metal. In-addition, when bringing the sulfide into contact with the acid solution, the added amounts of the sulfide and the acid solution are preferably adjusted such that the oxidation-reduction potential of the obtained leachate is maintained at 150 mV or less where a silver/silver chloride electrode is a reference electrode.

Chemical dismantling of permanent magnet material and battery material

Certain method embodiments are described and useful for recycling permanent magnet materials (e.g. permanent magnet alloys) and battery materials (e.g. battery electrode materials) to extract critical and/or valuable elements including REEs, Co and Ni. Method embodiments involve reacting such material with at least one of an ammonium salt and an iron (III) salt to achieve at least one of a liquid phase chemical reaction and a mechanochemical reaction.