C22B23/00

Processing method for lithium ion battery scrap

A method for processing lithium ion battery scrap includes a leaching step of leaching lithium ion battery scrap and subjecting the resulting leached solution to solid-liquid separation to obtain a first separated solution; an iron removal step of adding an oxidizing agent to the first separated solution and adjusting a pH of the first separated solution in a range of from 3.0 to 4.0, then performing solid-liquid separation and removing iron in the first separated solution to obtain a second separated solution; and an aluminum removal step of neutralizing the second separated solution to a pH range of from 4.0 to 6.0, then performing solid-liquid separation and removing aluminum in the second separated solution to obtain a third separated solution.

Process and system for extraction of iron oxide from ore

A method and system of extracting iron oxide from ore is provided, which may include adding a chelating agent to an iron ore to form an iron ore and chelating agent solution, heating the solution to reflux in water, and filtering the solution to yield an extraction residue and a chelated iron solution. The chelated iron solution may be treated with a potassium hydroxide and water solution to yield iron hydroxide.

METHOD FOR PRODUCING NICKEL POWDER
20200376564 · 2020-12-03 ·

Provided is a method for manufacturing coarse particles of a so-called high-purity nickel powder with a small amount of impurities, particularly having a low sulfur grade, from a nickel sulfate amine complex solution using a fine nickel powder. A method for manufacturing a nickel powder includes the following treatment steps (1) to (6) in a process for manufacturing a nickel powder from a nickel sulfate solution: (1) a hydroxylation step; (2) a complexation step; (3) a reduction step; (4) a solid/liquid separation step; (5) a nickel recovery step of repeatedly supplying the recovered nickel powder to step (2) and/or step (3), sulfurating the recovered final reduction solution, and then solid/liquid separating the sulfurated solution to generate nickel sulfide and a nickel post-reduction solution; and (6) a nickel regeneration step of oxidatively leaching the nickel sulfide obtained in step (5) and repeatedly supplying the obtained nickel sulfate solution to step (1).

METHOD FOR TREATING LITHIUM ION BATTERY WASTE

Provided is a treatment method whereby it becomes possible to recovery copper, nickel and cobalt, which are valuable metals, contained in a lithium ion battery waste and to separate copper, nickel and cobalt from one another effectively. A method for treating a lithium ion battery waste according to the present invention includes: an alloy production step S1 of introducing the lithium ion battery waste into a furnace and then melting the lithium ion battery waste by heating, thereby producing an alloy containing copper, nickel and cobalt; and an electrolytic purification step S2 of subjecting the alloy to such an electrolytic treatment that the alloy is charged as an anode into a sulfuric acid solution and then electricity is conducted between the anode and a cathode to electrodeposit copper contained in the alloy onto the cathode, thereby separating nickel and cobalt from each other.

Oxygen injection in fluid bed ore concentrate roasting

Oxygen is injected into the windbox of a fluidized bed ore roaster to form a fluidizing and oxidizing gas stream of elevated oxygen content which is fed into only the feed zone into which the ore to be fluidized is fed.

METHOD FOR SEPARATING COPPER FROM NICKEL AND COBALT

Provided is a method for separating copper from nickel and cobalt, which is capable of efficiently and selectively separating copper, and nickel and cobalt from an alloy containing copper, nickel and cobalt such as a highly anticorrosive alloy that is obtained by subjecting a waste lithium ion battery to a dry treatment and contains copper, nickel and cobalt. According to the present invention, an alloy containing copper, nickel and cobalt is brought into contact with an acid in the coexistence of a sulfurization agent, thereby obtaining a solid that contains copper and a leachate that contains nickel and cobalt.

Mineral ore slurry pretreatment method, and method for manufacturing mineral ore slurry

There is provided a method capable of effectively reducing the amount of acid used in a leaching step and the amount of a neutralizer used in a final neutralization step while nickel yield in a hydrometallurgical process for nickel oxide ore is not reduced. A method for pre-treating ore slurry according to the present invention is a method for pre-treating ore slurry to be provided to a leaching treatment in a hydrometallurgical process for nickel oxide ore, the method including: a first separation step for separating ore slurry into a coarse particle fraction and a fine particle fraction; a second separation step for separating the coarse particle fraction separated in the first separation step into a heavy specific gravity fraction and a light specific gravity fraction; and a vibration sieving step for separating, by a vibration sieve, the light specific gravity fraction.

LITHIUM ION BATTERY SCRAP TREATMENT METHOD

The present invention relates to a method for treating lithium ion battery scrap containing Li, Ni, Co, Mn, Al, Cu and Fe, the method comprising carrying out a calcination step, a crushing step and a sieving step in this order, and after the steps, the method comprising: a leaching step of leaching the lithium ion battery scrap by adding it to an acidic solution to leave at least a part of Cu as a solid; a Fe/Al removal step comprising allowing a leached solution obtained in the leaching step to pass through a Fe removal process for separating and removing Fe by addition of an oxidizing agent and an Al removal process for separating and removing a part of Al by neutralization in any order; an Al/Mn extraction step of extracting and removing a residue of Al and Mn from a separated solution obtained in the Fe/Al removal step by solvent extraction; a Co recovery step of extracting and back-extracting Co from a first extracted solution obtained in the Al/Mn extraction step by solvent extraction and recovering the Co by electrolytic winning; a Ni recovery step of extracting and back-extracting, by solvent extraction, a part of Ni from a second extracted solution obtained by the solvent extraction in the Co recovery step and recovering the Ni by electrolytic winning; a Li concentration step of extracting and back-extracting, by solvent extraction, a residue of Ni and Li from a third extracted solution obtained by the solvent extraction in the Ni recovery step and repeating the operations of the extracting and the back-extracting to concentrate Li; and a Li recovery step of carbonating Li in a Li concentrated solution obtained in the Li concentration step to recover the Li as lithium carbonate.

LITHIUM ION BATTERY SCRAP TREATMENT METHOD

The present invention relates to a method for treating lithium ion battery scrap containing Li, Ni, Co, Mn, Al, Cu and Fe, the method comprising carrying out a calcination step, a crushing step and a sieving step in this order, and after the steps, the method comprising: a leaching step of leaching the lithium ion battery scrap by adding it to an acidic solution to leave at least a part of Cu as a solid; a Fe/Al removal step comprising allowing a leached solution obtained in the leaching step to pass through a Fe removal process for separating and removing Fe by addition of an oxidizing agent and an Al removal process for separating and removing a part of Al by neutralization in any order; an Al/Mn extraction step of extracting and removing a residue of Al and Mn from a separated solution obtained in the Fe/Al removal step by solvent extraction; a Co recovery step of extracting and back-extracting Co from a first extracted solution obtained in the Al/Mn extraction step by solvent extraction and recovering the Co by electrolytic winning; a Ni recovery step of extracting and back-extracting, by solvent extraction, a part of Ni from a second extracted solution obtained by the solvent extraction in the Co recovery step and recovering the Ni by electrolytic winning; a Li concentration step of extracting and back-extracting, by solvent extraction, a residue of Ni and Li from a third extracted solution obtained by the solvent extraction in the Ni recovery step and repeating the operations of the extracting and the back-extracting to concentrate Li; and a Li recovery step of carbonating Li in a Li concentrated solution obtained in the Li concentration step to recover the Li as lithium carbonate.

RECYCLING OF SMART WINDOWS
20200016641 · 2020-01-16 · ·

The present invention relates to the methods of recycling electrochromic devices and also designing such devices while keeping recyclability in perspective. Recyclability includes recovering of certain materials for re-use within the same application or other applications. Using recycling reduces or eliminates waste stream quantities to be disposed of and/or reduces toxicity of these waste streams.