A method includes depositing a layer of alloy particles including rare earth permanent magnet phase above a substrate, laser scanning the layer while cooling the substrate to melt the particles, selectively initiate crystal nucleation, and promote columnar grain growth in a same direction as an easy axis of the rare earth permanent magnet phase. The method also includes repeating the depositing and scanning to form bulk anisotropic rare earth alloy magnet with aligned columnar grains.

A process for additive manufacturing of a metal alloy material is provided that includes: a) providing a feedstock powder comprising base powder particles with nanoparticles attached to surfaces of the base powder particles; b) providing an additive manufacturing system with a laser power source relatively movable at a scan speed; c) wherein the additive manufacturing system has a process window for the feedstock powder; and d) exposing the feedstock powder to a predetermined power input from the laser power source at a predetermined scan speed to produce the metal alloy material. The concentration by volume of nanoparticles within the feedstock powder is such that independent first and second microstructures may be produced within the metal alloy material.

A process for additive manufacturing of a metal alloy material is provided that includes: a) providing a feedstock powder comprising base powder particles with nanoparticles attached to surfaces of the base powder particles; b) providing an additive manufacturing system with a laser power source relatively movable at a scan speed; c) wherein the additive manufacturing system has a process window for the feedstock powder; and d) exposing the feedstock powder to a predetermined power input from the laser power source at a predetermined scan speed to produce the metal alloy material. The concentration by volume of nanoparticles within the feedstock powder is such that independent first and second microstructures may be produced within the metal alloy material.

In an aspect, an electrochemical cell comprises: a positive electrode; a negative electrode, said negative electrode having an alloy having a composition comprising V; and an electrolyte; wherein an additive is provided in said electrolyte to form primary vanadate ions upon dissociation of said additive in said electrolyte; and wherein the electrochemical cell is a metal hydride battery. In some embodiments of this aspect, the alloy is configured to sorb hydrogen during charging of said electrochemical cell and desorb hydrogen during discharging of said electrochemical cell. In some embodiments of this aspect, the electrolyte has a pH selected from the range of 13 to 15.

A superalloy target wherein the superalloy target has a polycrystalline structure of random grain orientation, the average grain size in the structure is smaller than 20 m, and the porosity in the structure is smaller than 10%. Furthermore, the invention includes a method of producing a superalloy target by powder metallurgical production, wherein the powder-metallurgical production starts from alloyed powder(s) of a superalloy and includes the step of spark plasma sintering (SPS) of the alloyed powder(s).

An object of the present invention is to provide an electroformed part favorable for an assembly part of a timepiece or the like and a timepiece using the same. The present invention relates to an electroformed part, which is an electroformed part composed of a nickel-iron alloy constituted by nickel, iron, and unavoidable impurities, containing iron at 5 to 25% by mass, and having a roughly layered form portion in which a stacked form portion having an inclined iron content in a thickness direction is repeatedly stacked a plurality of times. It is preferred that the stacked portion is constituted by crystal grains having an average grain diameter of 50 nm or less.

According to aspects of the present disclosure, a ternary alloy includes a dual-phase microstructure including a first phase and a second phase. The first phase defines a hexagonal close-packed structure with a stoichiometric ratio of Al.sub.4Fe.sub.1.7Si. The second phase defines a face-centered cubic structure with a stoichiometric ratio of Al.sub.3Fe.sub.2Si. The dual-phase microstructure is stable above about 800 C., and the dual-phase microstructure has a first-phase abundance greater than about 50 parts by weight and a second-phase abundance less than about 50 parts by weight based on 100 parts by weight of the ternary alloy.

Some variations provide a permanent-magnet structure comprising: a region having a plurality of magnetic domains and a region-average magnetic axis, wherein each of the magnetic domains has a domain magnetic axis that is substantially aligned with the region-average magnetic axis, and wherein the plurality of magnetic domains is characterized by an average magnetic domain size. Within the region, there is a plurality of metal-containing grains characterized by an average grain size, and each of the magnetic domains has a domain easy axis that is dictated by a crystallographic texture of the metal-containing grains. The region has a region-average easy axis based on the average value of the domain easy axis within that region. The region-average magnetic axis and the region-average easy axis form a region-average alignment angle that has a standard deviation less than 30 within the plurality of magnetic domains. Many permanent-magnet structures are disclosed herein.

Methods for grain refinement of beryllium articles are disclosed. Grain refinement allows the beryllium article to have beneficial properties in terms of strength and durability. One method stabilizes the ?-phase of the beryllium that is precipitated after cycling above a temperature that is greater than or equal to the beta transus temperature.

Methods for grain refinement of beryllium articles are disclosed. Grain refinement allows the beryllium article to have beneficial properties in terms of strength and durability. One method stabilizes the ?-phase of the beryllium that is precipitated after cycling above a temperature that is greater than or equal to the beta transus temperature.