The present invention is directed to a method and a system for the production of at least one polymeric yarn comprising means for mixing a polymer (1) with a first solvent yielding a mixture; means for homogenizing the mixture; means for rendering the mixture inert (21, 22, 23); means for dipping the mixture into a quenching bath (30), wherein an air gap is maintained before the mixture reaches the quenching bath (30) liquid surface forming at least one polymeric yarn; means for drawing (41) the at least one polymeric yarn at least once; means for washing (5) the at least one polymeric yarn with a second solvent that is more volatile than the first solvent; means for heating the at least one polymeric yarn (6); means for drawing at room temperature (7) the at least one polymeric yarn at least once; and means for heat drawing (8) the at least one polymeric yarn at least once. The instant invention also concerns a system and method of dosing a polymer mixture with a first solvent into an extruder (26), a device (5), a system and a method of solvent extraction from at least one polymeric yarn, and a method and system of mechanical pre-recovery (4) of at least one liquid in at least one polymeric yarn.

This application describes a method of preparation of a natural graphene cellulose blended spunbond nonwoven fabric, which comprises using a graphite powder as a raw material for preparing a graphene solution, adding the graphene solution to a slurry formed by mixing and dissolving a wood pulp with N-methylmorpholine N-oxide (NMMO), removing the water content thereof to form a spinning dope, and then directly preparing the natural graphene cellulose blended spunbond nonwoven fabric by a spunbond process. The present method does not require a highly toxic hydrazine hydrate solution. Further, by increasing the adding ratio of the graphene solution in the manufacturing process, control of the antistatic properties and thermal transferring function can be achieved, and thereby various requirements of different consumers can be satisfied. Besides, the fabric can decompose naturally after being used, and thus the product is harmless, natural, and environmentally friendly.

This application describes a method of preparation of a natural graphene cellulose blended spunbond nonwoven fabric, which comprises using a graphite powder as a raw material for preparing a graphene solution, adding the graphene solution to a slurry formed by mixing and dissolving a wood pulp with N-methylmorpholine N-oxide (NMMO), removing the water content thereof to form a spinning dope, and then directly preparing the natural graphene cellulose blended spunbond nonwoven fabric by a spunbond process. The present method does not require a highly toxic hydrazine hydrate solution. Further, by increasing the adding ratio of the graphene solution in the manufacturing process, control of the antistatic properties and thermal transferring function can be achieved, and thereby various requirements of different consumers can be satisfied. Besides, the fabric can decompose naturally after being used, and thus the product is harmless, natural, and environmentally friendly.

This application describes a method of preparation of a natural graphene cellulose blended meltblown nonwoven fabric, which comprises using a graphite powder as a raw material for preparing a graphene solution, adding the graphene solution to a slurry formed by mixing and dissolving a wood pulp with N-methylmorpholine N-oxide (NMMO), removing the water content thereof to form a spinning dope, and then directly preparing the natural graphene cellulose blended meltblown nonwoven fabric by a meltblown process. The present method does not require a highly toxic hydrazine hydrate solution. Further, by increasing the adding ratio of the graphene solution in the manufacturing process, control of the antistatic properties and thermal transferring function can be achieved, and thereby various requirements of different consumers can be satisfied. Besides, the fabric can decompose naturally after being used, and thus the product is harmless, natural, and environmentally friendly.

This application describes a method of preparation of a natural graphene cellulose blended meltblown nonwoven fabric, which comprises using a graphite powder as a raw material for preparing a graphene solution, adding the graphene solution to a slurry formed by mixing and dissolving a wood pulp with N-methylmorpholine N-oxide (NMMO), removing the water content thereof to form a spinning dope, and then directly preparing the natural graphene cellulose blended meltblown nonwoven fabric by a meltblown process. The present method does not require a highly toxic hydrazine hydrate solution. Further, by increasing the adding ratio of the graphene solution in the manufacturing process, control of the antistatic properties and thermal transferring function can be achieved, and thereby various requirements of different consumers can be satisfied. Besides, the fabric can decompose naturally after being used, and thus the product is harmless, natural, and environmentally friendly.

The invention discloses a purification method, system and a detection method of N-methylmorpholine N-oxide (NMMO), and a N-methylmorpholine N-oxide obtained thereof. The NMMO is derived from a NMMO crude product prepared by the reaction of N-methylmorpholine with hydrogen peroxide. The mass concentration of NMMO in the NMMO crude product is 50% to 60%. The purification method includes: performing cooling crystallization to the NMMO crude product between ?20? C. and 78? C. to obtain crystalline NMMO. The NMMO purification method has a low cost, a high purity of the obtained NMMO product, and almost no generation of exhaust gas, waste water, and solid waste. Different from current NMMO purification process, the purification method of the invention does not require ion-exchange resin, thus completely solved problems of significant amount of wastewater with high concentration of salt and COD and spent ion-exchange resin caused by the regeneration of ion-exchange resin.

The invention discloses a purification method, system and a detection method of N-methylmorpholine N-oxide (NMMO), and a N-methylmorpholine N-oxide obtained thereof. The NMMO is derived from a NMMO crude product prepared by the reaction of N-methylmorpholine with hydrogen peroxide. The mass concentration of NMMO in the NMMO crude product is 50% to 60%. The purification method includes: performing cooling crystallization to the NMMO crude product between ?20? C. and 78? C. to obtain crystalline NMMO. The NMMO purification method has a low cost, a high purity of the obtained NMMO product, and almost no generation of exhaust gas, waste water, and solid waste. Different from current NMMO purification process, the purification method of the invention does not require ion-exchange resin, thus completely solved problems of significant amount of wastewater with high concentration of salt and COD and spent ion-exchange resin caused by the regeneration of ion-exchange resin.

The present invention provides a fabricating method for meltblown nonwoven from natural cellulose fiber blended with nano silver, which comprises following steps. Firstly, prepare nano silver colloidal sol by reduction titration for mixture of polyvinyl alcohol (PVA), silver nitrate (AgNO.sub.3) and sodium borohydride (NaBH.sub.4). Secondly, prepare mixing cellulose serum by blending agitation for mixture of wood pulp, N-methylmorpholine N-oxide (NMMO) and stabilizer. Thirdly, prepare blending mucilage from mixing cellulose serum via blending process. Fourthly, produce spinning dope by blending and dehydrating the nano silver colloidal sol and mixing cellulose serum. Fifthly, produce molten filament tow by meltblown spinning method in association with coagulation, regeneration in coagulation bath, and water rinse. Finally, by post treatments of hydro-entangled needle punching, drying, winding-up processes in proper order, obtain final product of meltblown nonwoven from natural cellulose fiber blended with nano silver, which is biodegradable with features of antibacterial and antistatic capabilities.

The present invention provides a fabricating method for natural cellulose fiber blended with nano silver. The fabricating method comprises following steps: Firstly, prepare nano silver colloidal sol by reduction titration for mixture of polyvinyl alcohol (PVA), silver nitrate (AgNO.sub.3) and sodium borohydride (NaBH.sub.4). Secondly, prepare mixing cellulose serum by blending agitation for mixture of wood pulp, N-methylmorpholine N-oxide (NMMO) and stabilizer. Thirdly, produce spinning dope by blending and dehydrating the nano silver colloidal sol and mixing cellulose serum. Fourthly, produce fibrous tow by Dry-Jet Wet Spinning method in association with coagulation, regeneration in coagulation bath, and water rinse. Finally, obtain final product of natural cellulose fiber blended with nano silver by post treatments of dry, oil and coil in proper order.

Provided are an extractant for ultra-high molecular weight PE fibers and membranes, and methods of preparing and applying the same, relating to the technical field of polyethylene preparation. An extractant for ultra-high molecular weight PE fibers and membranes comprises an ionic liquid, which is one or more of an imidazolium tetrafluoroborate salt, a betaine salt, an imidazolium acetate salt, an imidazolium dicyanamide salt, an imidazolium ethyl sulfate salt, an imidazolium bis (fluorosulfonyl) imide salt and a bis((trifluoromethyl) sulfonyl) imide salt. The extractant of the present invention is characterized by a reasonable and scientific formula, high dispersibility and stability, a good degreasing effect on ultra-high molecular weight polyethylene fibers and membranes and excellent effects of subsequent separation and recycle of white oil, and has the advantages of convenient preparation of raw materials, simple process steps, low requirements for apparatuses, high operability, and suitable for industrial production.