D21C3/00

Combination approach to delignification of biomass under ambient conditions

Method of delignification of plant material, said method comprising: providing said plant material comprising cellulose fibres and lignin; exposing said plant material requiring to a composition comprising: an acid; a modifying agent selected from the group consisting of: sulfamic acid; imidazole; N-alkylimidazole derivative; taurine; a taurine derivative; a taurine-related compound; alkylsulfonic acid; arylsulfonic acid; triethanolamine; and combinations thereof; a metal oxide; and a peroxide; adding an organic solvent to the resulting mixture; allowing a delignification reaction to occur for a period of time sufficient to remove at least 80% of the lignin present on said plant material.

Temperature-controlled delignification of biomass

A process to delignify biomass, said process comprising the steps of: providing a vessel; providing biomass comprising lignin, hemicellulose and cellulose fibers into said vessel; providing a aqueous acidic composition comprising a sulfuric acid component; providing a peroxide component; exposing said biomass to said sulfuric acid component and peroxide component, creating a reaction mass; allowing said sulfuric acid component and peroxide component to come into contact with said biomass for a period of time sufficient to a delignification reaction to occur and remove over 90 wt % of said lignin and hemicellulose from said biomass; and controlling the temperature of the delignification reaction to maintain it below 55? C.

METHOD FOR EXTRACTING CELLUSOSE, HEMICELLULOSE AND LIGNIN FROM LIGNOCELLULOSE FROM PLANT BIOMASS

A process for obtaining cellulose, hemicellulose and lignin from lignocellulose can be carried out in an environmentally friendly manner when it comprises the following steps: step a) wherein a lignocellulose from plant biomass is provided, step b) wherein the lignocellulose is brought into contact with a first mixture M1 containing water and an alkaline component, and a first suspension S1 forms, the first suspension S1 comprises a first solid F1 and a first liquid phase P1, wherein the first solid F1 contains a crude cellulose, and the first liquid phase P1 contains hemicellulose and lignin, and step c) wherein the crude-cellulose-containing solid F1 is brought into contact with a second mixture M2 containing formic acid and water and optionally acetic acid, and a second suspension S2 forms, the second suspension S2 comprises a second solid F2 and a second liquid phase P2, wherein the second solid F2 contains a pure cellulose, and the second liquid phase P2 contains hemicellulose and lignin.

Low Temperature and Efficient Fractionation of Lignocellulosic Biomass Using Recyclable Organic Solid Acids
20190233596 · 2019-08-01 ·

Methods of fractionating lignocellulosic biomass using hydrotropic solid organic acids are provided. Also provided are methods of forming lignin particles, furans, sugars, and/or lignocellulosic micro- and nanofibrils from the liquid and solid fractions produced by fractionation process. The fractionation can be carried out at low temperatures with short reaction times.

Method for improved pulping using an environmentally friendly pulping aid
20190226142 · 2019-07-25 ·

A safe and environmentally friendly pulping aid comprising a mixture of natural terpene-based chemicals and a dispersant blend. The pulping aid is used in the pulping of lignocellulosic biomass to simultaneously increase screened pulp yield and reduce the extractives content of pulp. The flash point of the pulping aid is at least 49 C.

METHOD FOR DIGESTING LIGNOCELLULOSIC MATERIAL

A method for digesting lignocellulosic material includes combining a lignocellulosic material comprising lignocellulosic biomass, a polymerized naphthalene sulfonate, a sodium xylene sulfonate, and a white liquor comprising sodium hydroxide and sodium sulfide to form a mixture. Further, the method includes heating the mixture to digest at least a portion of the lignocellulosic material.

Foam-Based Manufacturing System and Process

A system comprising a pulper configured to (i) accept surfactant, a liquid and fiber stock and (ii) generate a foam that suspends the fiber stock, wherein the foam has a half-life; a headbox configured to receive the foam-suspended fiber stock from the pulper and displace the foam-suspended fiber stock onto a forming wire, wherein a time it takes the foam-suspended fiber stock to move from the pulper to the headbox is less than the half-life; and a foam return device that removes at least some of the foam from the forming wire and returns the at least some of the foam to the pulper.

Hydrothermal-mechanical conversion of lignocellulosic biomass to ethanol or other fermentation products

A low-cost process is provided to render lignocellulosic biomass accessible to cellulase enzymes, to produce fermentable sugars. Some variations provide a process to produce ethanol from lignocellulosic biomass (such as sugarcane bagasse or corn stover), comprising introducing a lignocellulosic biomass feedstock to a single-stage digestor; exposing the feedstock to a reaction solution comprising steam or liquid hot water within the digestor, to solubilize the hemicellulose in a liquid phase and to provide a cellulose-rich solid phase; refining the cellulose-rich solid phase, together with the liquid phase, in a mechanical refiner, thereby providing a mixture of refined cellulose-rich solids and the liquid phase; enzymatically hydrolyzing the mixture in a hydrolysis reactor with cellulase enzymes, to generate fermentable sugars; and fermenting the fermentable sugars to produce ethanol. Many alternative process configurations are described. The disclosed processes may be employed for other fermentation products.

Hydrothermal-mechanical conversion of lignocellulosic biomass to ethanol or other fermentation products

A low-cost process is provided to render lignocellulosic biomass accessible to cellulase enzymes, to produce fermentable sugars. Some variations provide a process to produce ethanol from lignocellulosic biomass (such as sugarcane bagasse or corn stover), comprising introducing a lignocellulosic biomass feedstock to a single-stage digestor; exposing the feedstock to a reaction solution comprising steam or liquid hot water within the digestor, to solubilize the hemicellulose in a liquid phase and to provide a cellulose-rich solid phase; refining the cellulose-rich solid phase, together with the liquid phase, in a mechanical refiner, thereby providing a mixture of refined cellulose-rich solids and the liquid phase; enzymatically hydrolyzing the mixture in a hydrolysis reactor with cellulase enzymes, to generate fermentable sugars; and fermenting the fermentable sugars to produce ethanol. Many alternative process configurations are described. The disclosed processes may be employed for other fermentation products.

Process for individualizing trichomes

A process for individualizing (separating) trichome fibers from a trichome source, such as a leaf and/or a stem, and more particularly to a process for individualizing (separating) trichome fibers from a trichome source utilizing a chemical separation process are provided.