Method and apparatus thereof to separate aluminum from aluminum-containing source material, such as fly ash, includes preparing a slurry of the source material and water in an agitation tank and adding a leaching reactant to the slurry in an amount dependent on the amount of aluminum in the source material. After agitation, transferring the mixture to a settling pond. After settling, transferring the liquid as a pregnant solution to an electric cell. Treating the pregnant solution in the electric cell by applying an electrical current that is periodically reversed as the pregnant solution passes between at least two metal plates in the electric cell. Collecting the treated solution in a cone bottom tank and separating aluminum particles from the treated solution using a filter press. Drying the particulate aluminum and pressing the aluminum into solid shapes. Another embodiment collects hydrogen generated in the electric cell from source material.

Method and apparatus thereof to separate aluminum from aluminum-containing source material, such as fly ash, includes preparing a slurry of the source material and water in an agitation tank and adding a leaching reactant to the slurry in an amount dependent on the amount of aluminum in the source material. After agitation, transferring the mixture to a settling pond. After settling, transferring the liquid as a pregnant solution to an electric cell. Treating the pregnant solution in the electric cell by applying an electrical current that is periodically reversed as the pregnant solution passes between at least two metal plates in the electric cell. Collecting the treated solution in a cone bottom tank and separating aluminum particles from the treated solution using a filter press. Drying the particulate aluminum and pressing the aluminum into solid shapes. Another embodiment collects hydrogen generated in the electric cell from source material.

Method and apparatus thereof to separate aluminum from aluminum-containing source material, such as fly ash, includes preparing a slurry of the source material and water in an agitation tank and adding a leaching reactant to the slurry in an amount dependent on the amount of aluminum in the source material. After agitation, transferring the mixture to a settling pond. After settling, transferring the liquid as a pregnant solution to an electric cell. Treating the pregnant solution in the electric cell by applying an electrical current that is periodically reversed as the pregnant solution passes between at least two metal plates in the electric cell. Collecting the treated solution in a cone bottom tank and separating aluminum particles from the treated solution using a filter press. Drying the particulate aluminum and pressing the aluminum into solid shapes.

Method and apparatus thereof to separate aluminum from aluminum-containing source material, such as fly ash, includes preparing a slurry of the source material and water in an agitation tank and adding a leaching reactant to the slurry in an amount dependent on the amount of aluminum in the source material. After agitation, transferring the mixture to a settling pond. After settling, transferring the liquid as a pregnant solution to an electric cell. Treating the pregnant solution in the electric cell by applying an electrical current that is periodically reversed as the pregnant solution passes between at least two metal plates in the electric cell. Collecting the treated solution in a cone bottom tank and separating aluminum particles from the treated solution using a filter press. Drying the particulate aluminum and pressing the aluminum into solid shapes.

The invention is directed to a process to prepare metal nanoparticles or metal oxide nanoparticles by applying a cathodic potential as an alternating current (ac) voltage to a solid starting metal object which solid metal object is in contact with a liquid electrolyte comprising a stabilising cation. The invention is also directed to the use of the nanoparticles as a catalyst.

The invention is directed to a process to prepare metal nanoparticles or metal oxide nanoparticles by applying a cathodic potential as an alternating current (ac) voltage to a solid starting metal object which solid metal object is in contact with a liquid electrolyte comprising a stabilising cation. The invention is also directed to the use of the nanoparticles as a catalyst.

An assembly for use in refining metals includes two adjacent capping board segments defining a joint interface there-between, a contact bar that may be a contact bar segment and is sized and configured to lay on the two capping boards and to span across the joint interface, and two engagement mechanisms provided on respective sides of the joint interface, to hold the capping board segments together. Each engagement mechanism may include a projecting anchor element and a retaining cavity sized and configured to receive a corresponding projecting anchor element. The contact bar may include the projecting anchor elements and the capping board segments may include the retaining cavities. Methods and uses of such contact bars and capping board segments are also provided for hydrometallurgical refining operations.

An assembly for use in refining metals includes two adjacent capping board segments defining a joint interface there-between, a contact bar that may be a contact bar segment and is sized and configured to lay on the two capping boards and to span across the joint interface, and two engagement mechanisms provided on respective sides of the joint interface, to hold the capping board segments together. Each engagement mechanism may include a projecting anchor element and a retaining cavity sized and configured to receive a corresponding projecting anchor element. The contact bar may include the projecting anchor elements and the capping board segments may include the retaining cavities. Methods and uses of such contact bars and capping board segments are also provided for hydrometallurgical refining operations.

Provided herein is an apparatus for electrolytic atomic hydrogen decrepitation and methods of use thereof.

Provided herein is an apparatus for electrolytic atomic hydrogen decrepitation and methods of use thereof.