A method for liquefying niobium and tantalum and a method for producing a niobium solution and a tantalum solution, which can liquefy niobium and tantalum or produce a niobium solution and a tantalum solution safely and efficiently from a smelting raw material containing niobium and tantalum. Ammonium hydrogen sulfate is mixed as a reaction agent into a powdered substance containing at least one element of niobium or tantalum, and the mixture is melted under predetermined conditions to form a molten substance. A suspension formed by dissolving the molten substance having been solidified in an aqueous solution is subjected to solid-liquid separation to recover a precipitate. The precipitate is composed of niobium and/or tantalum with few impurities, and the precipitate is dissolved in one type of acid solution selected from hydrochloric acid, sulfuric acid, or nitric acid, whereby 90% or more of niobium and/or tantalum can be leached out.

The present disclosure relates to a method for treating an electromembrane process aqueous composition comprising sodium and/or potassium sulfate, said process comprising removing water from said electromembrane process aqueous composition under conditions suitable for substantially selectively precipitating sodium and/or potassium sulfate monohydrate.

The present disclosure relates to a method for treating an electromembrane process aqueous composition comprising sodium and/or potassium sulfate, said process comprising removing water from said electromembrane process aqueous composition under conditions suitable for substantially selectively precipitating sodium and/or potassium sulfate monohydrate.

An apparatus for extracting lithium from a lithium-bearing material. A mixer is configured to receive and mix lithium-bearing material with gypsum, a sulfur-containing material, and a calcium-containing material and form a feed mixture having a moisture content of at least 20 wt %. A dryer is configured to dry the feed mixture and form a dried mixture having a moisture content of less than 20 wt %. A roaster is configured to receive and roast the dried mixture and form a roasted mixture including a water-soluble lithium compound. A leach tank is configured to form a lithium-containing leachate from the water-soluble lithium compound using an aqueous solution.

An apparatus for extracting lithium from a lithium-bearing material. A mixer is configured to receive and mix lithium-bearing material with gypsum, a sulfur-containing material, and a calcium-containing material and form a feed mixture having a moisture content of at least 20 wt %. A dryer is configured to dry the feed mixture and form a dried mixture having a moisture content of less than 20 wt %. A roaster is configured to receive and roast the dried mixture and form a roasted mixture including a water-soluble lithium compound. A leach tank is configured to form a lithium-containing leachate from the water-soluble lithium compound using an aqueous solution.

Disclosed is a method for producing battery-grade nickel sulfate by using laterite nickel ore comprising the following steps: sorting the laterite nickel ore to obtain lump ore and sediment ore; crushing the lump ore, and then performing heap leaching, to obtain a crude nickel sulfate solution A; separating the sediment ore to obtain high chromium ore, low iron, high magnesium ore, and high iron, low magnesium ore, and drying, roasting, reducing, and sulfurating the low iron, high magnesium ore to obtain low nickel matte; blowing and performing water extraction on the low nickel matte, and then performing oxygen pressure leaching, to obtain a crude nickel sulfate solution B; performing pressure leaching on the high iron, low magnesium ore to obtain a crude nickel sulfate solution C; and performing extraction on the crude nickel sulfate solutions A, B, and C, and then evaporating and crystallizing, to obtain battery-grade nickel sulfate.

Disclosed is a method for producing battery-grade nickel sulfate by using laterite nickel ore comprising the following steps: sorting the laterite nickel ore to obtain lump ore and sediment ore; crushing the lump ore, and then performing heap leaching, to obtain a crude nickel sulfate solution A; separating the sediment ore to obtain high chromium ore, low iron, high magnesium ore, and high iron, low magnesium ore, and drying, roasting, reducing, and sulfurating the low iron, high magnesium ore to obtain low nickel matte; blowing and performing water extraction on the low nickel matte, and then performing oxygen pressure leaching, to obtain a crude nickel sulfate solution B; performing pressure leaching on the high iron, low magnesium ore to obtain a crude nickel sulfate solution C; and performing extraction on the crude nickel sulfate solutions A, B, and C, and then evaporating and crystallizing, to obtain battery-grade nickel sulfate.

A method for liquefying niobium and tantalum and a method for producing a niobium solution and a tantalum solution, which can liquefy niobium and tantalum or produce a niobium solution and a tantalum solution safely and efficiently from a smelting raw material containing niobium and tantalum. Ammonium hydrogen sulfate is mixed as a reaction agent into a powdered substance containing at least one element of niobium or tantalum, and the mixture is melted under predetermined conditions to form a molten substance. A suspension formed by dissolving the molten substance having been solidified in an aqueous solution is subjected to solid-liquid separation to recover a precipitate. The precipitate is composed of niobium and/or tantalum with few impurities, and the precipitate is dissolved in one type of acid solution selected from hydrochloric acid, sulfuric acid, or nitric acid, whereby 90% or more of niobium and/or tantalum can be leached out.

According to the present invention there is provided a method for the extraction of one or more valuable metals, preferably Li, Co, Mn and/or Ni, from black mass end-of-life battery waste, the method comprising the steps of: obtaining the black mass having a content of the one or more valuable metals; subjecting the black mass to a hydrothermal extraction medium defined by a molar excess of molten elemental sulfur, a predetermined amount of water, a first predetermined temperature and a first predetermined heated pressure, over a first predetermined period to provide a sulfur/metal roasted material; and converting the sulfur/metal roasted material to its respective metal sulfate/s by subjecting the sulfur/metal roasted material to an extraction medium defined by an excess of water, a flow of air, at a second predetermined temperature, at a second predetermined heated pressure over a second predetermined period.

According to the present invention there is provided a method for the extraction of one or more valuable metals, preferably Li, Co, Mn and/or Ni, from black mass end-of-life battery waste, the method comprising the steps of: obtaining the black mass having a content of the one or more valuable metals; subjecting the black mass to a hydrothermal extraction medium defined by a molar excess of molten elemental sulfur, a predetermined amount of water, a first predetermined temperature and a first predetermined heated pressure, over a first predetermined period to provide a sulfur/metal roasted material; and converting the sulfur/metal roasted material to its respective metal sulfate/s by subjecting the sulfur/metal roasted material to an extraction medium defined by an excess of water, a flow of air, at a second predetermined temperature, at a second predetermined heated pressure over a second predetermined period.