Patent classifications
C22B7/007
Method for recycling hydrogen fuel cell of new energy vehicle
Disclosed is a method for recycling a hydrogen fuel cell of a new energy vehicle, including the following steps of: (1) discharging and disassembling a hydrogen fuel cell in turn to obtain a hydrogen supply system, an air supply system, a cooling system and a galvanic pile; (2) disassembling the galvanic pile into a catalyst and carbon cloth, and ashing to obtain ash; (3) adding an auxiliary agent into the ash, mixing, introducing inert gas, heating, introducing oxidizing gas, and absorbing tail gas by using an ammonium salt solution; and (4) adding a reducing agent into the ammonium salt solution absorbing the tail gas in step (3) to react, filtering, taking and cleaning a filter residue to obtain Pt.
Process for the preparation of precursor compounds for lithium battery cathodes
The present disclosure concerns the production of precursor compounds for lithium battery cathodes. Batteries or their scrap are smelted in reducing conditions, thereby forming an alloy suitable for further hydrometallurgical refining, and a slag. The alloy is leached in acidic conditions, producing a Ni- and Co-bearing solution, which is refined. The refining steps are greatly simplified as most elements susceptible to interfere with the refining steps concentrate in the slag. Metals such as Co, Ni and Mn are then precipitated from the solution, forming a suitable starting product for the synthesis of new battery precursor compounds.
Method for disposal of waste printed circuit board thermal cracking slag and smelting soot
The invention discloses a method for cracking slag and smelting soot of the waste circuit board, belongs to the field of comprehensive recycling of valuable elements from typical soot of waste circuit boards, and particularly relates to a method for cracking slag and smelting soot of the waste circuit board for debromination and comprehensive recovery of copper and zinc. The method includes the following steps of: crushing and sorting, mixture roasting, reinforced leaching, replacement and silver precipitation, sulfuration and copper precipitation, and evaporation crystallization. Compared to traditional recycling technology, the purpose of treating two kinds of solid waste in a coupling mode through one recycling technology is achieved. Through mixed sulfuric acid roasting, the requirement of bromide synergistic removal of the waste circuit board cracking slag and smelting soot is met, and the purpose of selective conversion of copper and zinc is achieved.
RECOVERY OF NOBLE METALS
Recovery of noble metals (including the recovery of gold and/or silver from gold and/or silver containing material) is generally described. The gold and/or silver can be recovered selectively, in some cases, such that gold and/or silver are at least partially separated from non-silver and/or non-gold material. Gold and/or silver may be recovered from material using mixtures of acids, in some instances. In some cases, the mixture can comprise nitric acid and at least one supplemental acid, such as sulfuric acid, phosphoric acid, and/or a sulfonic acid. The amount of nitric acid within the mixture can be, in some instances, relatively small compared to the amount of sulfuric acid or phosphoric acid within the mixture. In some cases, the recovery of gold and/or silver using the acid mixtures can be enhanced by transporting an electric current between an electrode and the gold and/or silver of the material. In some cases, acid mixtures can be used to recover silver from particular types of materials, such as material comprising silver metal and cadmium oxide and/or material comprising silver metal and tungsten metal.
METHOD FOR RECYCLING LI-ION BATTERIES
A method for recycling a battery including the following steps: a) dissolution of a battery waste, for example an electrode, including lithium and a metal selected from cobalt and manganese, such that a solution to be treated containing lithium ions and metal ions is formed, b) addition of a peroxymonosulfate salt to the solution to be treated, the solution to be treated being regulated at a pH ranging from 1 to 4 when the metal is cobalt or at a pH ranging from 0.1 to 2.5 when the metal is manganese, such that the metal ions are selectively precipitated in the form of metal oxyhydroxide, c) separation of the lithium ions from the solution to be treated. Advantageously, the solution further comprises nickel ions.
SYSTEM AND METHOD FOR RECOVERING CONSTITUENTS FROM BATTERIES
An apparatus, method and system are provided to recover constituent components from single use batteries. In particular, the apparatus, method and system may be used to recover zinc and manganese in the form of sulfates from depleted commercial which in turn may be subsequently used for other applications, such as micronutrients and fertilizers.
Method and system for neutralizing asbestos
A system for asbestos neutralization, that includes a neutralization unit having a module configured for sorting of asbestos waste, an asbestos waste grinder; a concentrated sulfuric acid tank, a vat containing a hot diluted acid solution, for which temperature is between 70° C. and 100° C., in which grinded asbestos waste containing asbestos is dipped, the solution is configured for neutralizing asbestos contained in the grinded asbestos waste, a filtration unit to separate, at the end of the neutralization reaction, a solid inert waste from a liquid phase of the diluted acid solution, a regeneration unit for the diluted acid solution, which adjusts the hydrogen potential of the extracted liquid phase by adding concentrated sulfuric acid from the tank, and means for transferring the regenerated solution into the vat.
METHOD FOR THERMAL BARRIER COATING PRODUCTION BY RECYCLING THERMAL BARRIER COATING MATERIALS
Disclosed are methods to produce Thermal Barrier Coating (TBC) products using materials recycled from TBC waste. These methods include ways to produce zirconium and rare earth chemicals and raw materials appropriate for producing TBC materials.
Method and system for separation of rare earth elements from secondary sources
Recovery of rare earth elements (REEs) from electronic wastes is a promising approach. The existing methods for separation of REE from the secondary sources are not economically viable and scalable. A method and system for separation of rare earth metals from a plurality of secondary sources has been provided. The magnet is obtained from the secondary sources which is then crushed to a coarser size. The powder is then demagnetized by heating and roasted at high temperature to obtain the metal oxides. The metals oxides are then dissolved by acid leaching to obtain leach liquor. Iron is removed from leach liquor by precipitation and separated by filtration. The individual REE is then separated by liquid-liquid extraction. The conditions in liquid-liquid extraction are adjusted such that only desired REE is separated. The extracted REE is then stripped out by acid. The individual rare earth element is then precipitated and dried.
Method for preparing lead directly from lead-containing material by solid phase reaction
A method for preparing lead directly from a lead-containing material by a solid phase reaction, includes: step 1, adding the lead-containing material to be processed to the grinder, and adding a metal substance and water to the grinder, wherein an activity of the metal substance is larger than that of lead; the solid phase reaction between the lead-containing material and the metal substance is caused directly by the grinder through a mechanical force to obtain a reaction product; step 2, washing and filtering the reaction product to obtain the lead and a metal salt solution corresponding to the metal substance; step 3, performing a melt casting on the lead to obtain a crude lead, crystallizing the metal salt solution to obtain a metal salt corresponding to the metal substance.