C22B34/14

Methods for reducing impurities in magnesium, purified magnesium, and zirconium metal production methods
10422017 · 2019-09-24 · ·

A method for reducing impurities in magnesium comprises: combining a zirconium-containing material with a molten low-impurity magnesium including no more than 1.0 weight percent of total impurities in a vessel to provide a mixture; holding the mixture in a molten state for a period of time sufficient to allow at least a portion of the zirconium-containing material to react with at least a portion of the impurities and form intermetallic compounds; and separating at least a portion of the molten magnesium in the mixture from at least a portion of the intermetallic compounds to provide a purified magnesium, wherein the purified magnesium includes an increased level of zirconium compared to the low-impurity magnesium, wherein the purified magnesium includes greater than 1000 ppm zirconium, and wherein the purified magnesium includes a reduced level of impurities other than zirconium compared to the low-impurity magnesium. A purified magnesium including at least 1000 ppm zirconium and methods for producing zirconium metal using magnesium reductant also are disclosed.

Methods for reducing impurities in magnesium, purified magnesium, and zirconium metal production methods
10422017 · 2019-09-24 · ·

A method for reducing impurities in magnesium comprises: combining a zirconium-containing material with a molten low-impurity magnesium including no more than 1.0 weight percent of total impurities in a vessel to provide a mixture; holding the mixture in a molten state for a period of time sufficient to allow at least a portion of the zirconium-containing material to react with at least a portion of the impurities and form intermetallic compounds; and separating at least a portion of the molten magnesium in the mixture from at least a portion of the intermetallic compounds to provide a purified magnesium, wherein the purified magnesium includes an increased level of zirconium compared to the low-impurity magnesium, wherein the purified magnesium includes greater than 1000 ppm zirconium, and wherein the purified magnesium includes a reduced level of impurities other than zirconium compared to the low-impurity magnesium. A purified magnesium including at least 1000 ppm zirconium and methods for producing zirconium metal using magnesium reductant also are disclosed.

METHOD OF RECOVERING METAL COMPOUNDS FROM SOLID OXIDE FUEL CELL SCRAP

A method of recovering metal compounds from solid oxide fuel cell scrap includes processing the solid oxide fuel cell scrap to form a powder, digesting the processed scrap, extracting lanthanum oxide and cerium oxide from a solution containing the digested processed scrap, extracting a zirconium compound from the solution after extracting the lanthanum oxide and cerium oxide, and extracting scandium compound from the solution extracting the zirconium compound from the solution.

System and process for the recovery of titanium, titanium alloy, zirconium and zirconium alloy scrap
12012645 · 2024-06-18 ·

A system for the recovery of titanium, titanium alloys, zirconium and zirconium alloys is disclosed. The system is fed with a mixture of chips including titanium chips, titanium alloy chips, zirconium chips and zirconium alloy chips, ferromagnetic chips and electrically conductive non-ferromagnetic chips. The system has at least one magnetic separator, a drying device and an Eddy current separator.

System and process for the recovery of titanium, titanium alloy, zirconium and zirconium alloy scrap
12012645 · 2024-06-18 ·

A system for the recovery of titanium, titanium alloys, zirconium and zirconium alloys is disclosed. The system is fed with a mixture of chips including titanium chips, titanium alloy chips, zirconium chips and zirconium alloy chips, ferromagnetic chips and electrically conductive non-ferromagnetic chips. The system has at least one magnetic separator, a drying device and an Eddy current separator.

Production system for a hafnium crystal bar and the method thereof

The present invention discloses a production system for a hafnium crystal bar and the method thereof. The technical program includes a power supply unit with large DC current, an iodizer, a molybdenum insulator provided inside the iodizer, a thermostatic device, a cooling unit, a vacuum unit, an iodine box for iodizing the iodizer, an electrode unit electrically connected to the power supply unit, wherein the electrode unit is disposed above the iodizer, a crystallization unit provided inside the iodizer, wherein the crystallization unit is connected to the electrode unit, and a rough hafnium provided between the iodizer and the molybdenum insulator. The thermostatic device is a structure with an insulation layer provided outside an inner tank, and an electric heating wire is provided between the inner tank and the insulation layer. The inner tank of the thermostatic device is filled with a saline solution.

Production system for a hafnium crystal bar and the method thereof

The present invention discloses a production system for a hafnium crystal bar and the method thereof. The technical program includes a power supply unit with large DC current, an iodizer, a molybdenum insulator provided inside the iodizer, a thermostatic device, a cooling unit, a vacuum unit, an iodine box for iodizing the iodizer, an electrode unit electrically connected to the power supply unit, wherein the electrode unit is disposed above the iodizer, a crystallization unit provided inside the iodizer, wherein the crystallization unit is connected to the electrode unit, and a rough hafnium provided between the iodizer and the molybdenum insulator. The thermostatic device is a structure with an insulation layer provided outside an inner tank, and an electric heating wire is provided between the inner tank and the insulation layer. The inner tank of the thermostatic device is filled with a saline solution.

METHODS FOR REDUCING IMPURITIES IN MAGNESIUM, PURIFIED MAGNESIUM, AND ZIRCONIUM METAL PRODUCTION METHODS
20180327885 · 2018-11-15 ·

A method for reducing impurities in magnesium comprises: combining a zirconium-containing material with a molten low-impurity magnesium including no more than 1.0 weight percent of total impurities in a vessel to provide a mixture; holding the mixture in a molten state for a period of time sufficient to allow at least a portion of the zirconium-containing material to react with at least a portion of the impurities and form intermetallic compounds; and separating at least a portion of the molten magnesium in the mixture from at least a portion of the intermetallic compounds to provide a purified magnesium, wherein the purified magnesium includes an increased level of zirconium compared to the low-impurity magnesium, wherein the purified magnesium includes greater than 1000 ppm zirconium, and wherein the purified magnesium includes a reduced level of impurities other than zirconium compared to the low-impurity magnesium. A purified magnesium including at least 1000 ppm zirconium and methods for producing zirconium metal using magnesium reductant also are disclosed.

METHODS FOR REDUCING IMPURITIES IN MAGNESIUM, PURIFIED MAGNESIUM, AND ZIRCONIUM METAL PRODUCTION METHODS
20180327885 · 2018-11-15 ·

A method for reducing impurities in magnesium comprises: combining a zirconium-containing material with a molten low-impurity magnesium including no more than 1.0 weight percent of total impurities in a vessel to provide a mixture; holding the mixture in a molten state for a period of time sufficient to allow at least a portion of the zirconium-containing material to react with at least a portion of the impurities and form intermetallic compounds; and separating at least a portion of the molten magnesium in the mixture from at least a portion of the intermetallic compounds to provide a purified magnesium, wherein the purified magnesium includes an increased level of zirconium compared to the low-impurity magnesium, wherein the purified magnesium includes greater than 1000 ppm zirconium, and wherein the purified magnesium includes a reduced level of impurities other than zirconium compared to the low-impurity magnesium. A purified magnesium including at least 1000 ppm zirconium and methods for producing zirconium metal using magnesium reductant also are disclosed.

METHOD OF REFINING OF SCANDIUM OXIDE FROM CONCENTRATES USING SOLVENT EXTRACTION

A method of selectively removing impurities from a scandium-containing feed solution includes contacting an aqueous scandium-containing solution with an organic solvent stream containing an extractant, thereby forming a loaded organic solvent stream containing the impurity or impurities while leaving the scandium in the raffinate. The aqueous stream containing the scandium is washed, diluted and has inorganic salts added before being contacted with a second organic solvent stream to extract the scandium selectively, and followed by stripping the scandium from the scandium-containing loaded organic extractant stream by adding oxalic acid to the loaded organic extractant stream to form scandium oxalate.