C23C20/04

PRE-INITIATED OPTICAL FIBERS AND METHODS OF MAKING THEREOF
20220186376 · 2022-06-16 ·

Embodiments of the invention include a method of initiating an optical fiber of a tip assembly to form a finished tip assembly. In some embodiments, at least a portion of a distal portion of the optical fiber is coated with an energy absorbing initiating material. In some embodiments, the initiating material is an enamel material including a mixture of brass (copper and zinc) flakes or aluminum flakes in a solution of organic solvents. After the initiating material dries, a diode laser is fired through the optical fiber. The laser energy is at least partially absorbed in the initiating material and ignites the organic solvents. This combustion melts the material of the optical fiber, and impregnates the optical fiber with the metal flakes of the initiating material. The resulting initiated optical fiber is thus permanently modified so that the energy applied through the fiber is partially absorbed and converted to heat.

METHOD FOR PRODUCING BONDED OBJECT AND SEMICONDUCTOR DEVICE AND COPPER BONDING PASTE

An embodiment of the present invention provides a method for producing a bonded object. The method comprises a step for preparing a laminate in which a first member, a copper bonding paste, and a second member are laminated in order and a step for sintering the copper bonding paste under a pressure of 0.1-1 MPa. The copper bonding paste contains metal particles and a dispersion medium, wherein the content of metal particles is at 50 mass % or more with respect to the total mass of the copper bonding paste, and the metal particles contain 95 mass % or more of submicro copper particles with respect to the total mass of the metal particles.

Applying silicon metal-containing bond layer to ceramic or ceramic matrix composite substrates

In some examples, a method may include depositing, from a slurry comprising particles including silicon metal, a bond coat precursor layer including the particles comprising silicon metal directly on a ceramic matrix composite substrate. The method also may include locally heating the bond coat precursor layer to form a bond coat comprising silicon metal. Additionally, the method may include forming a protective coating on the bond coat. In some examples, an article may include a ceramic matrix composite substrate, a bond coat directly on the substrate, and a protective coating on the bond coat. The bond coat may include silicon metal and a metal comprising at least one of Zr, Y, Yb, Hf, Ti, Al, Cr, Mo, Nb, Ta, or a rare earth metal.

Applying silicon metal-containing bond layer to ceramic or ceramic matrix composite substrates

In some examples, a method may include depositing, from a slurry comprising particles including silicon metal, a bond coat precursor layer including the particles comprising silicon metal directly on a ceramic matrix composite substrate. The method also may include locally heating the bond coat precursor layer to form a bond coat comprising silicon metal. Additionally, the method may include forming a protective coating on the bond coat. In some examples, an article may include a ceramic matrix composite substrate, a bond coat directly on the substrate, and a protective coating on the bond coat. The bond coat may include silicon metal and a metal comprising at least one of Zr, Y, Yb, Hf, Ti, Al, Cr, Mo, Nb, Ta, or a rare earth metal.

ZINC-BASED PLATED STEEL SHEET HAVING POST-TREATED COATING FORMED THEREON AND POST-TREATMENT METHOD THEREFOR
20200399750 · 2020-12-24 ·

Provided is a zinc-based plated steel sheet having a post-treated coating filmed thereon including: a steel sheet; a zinc plated layer formed on the steel sheet; and a post-treated coating formed on the plated layer, wherein the atomic ratio (O/M) of oxygen (O) to metals (M) contained in the post-treated coating is greater than 2 and less than 20, and a method for post-treating a zinc-based plated steel sheet. According to this, the zinc-based plated steel sheet having the post-treated coating formed thereon has the effects excellent in lubricity, weldability, adhesiveness, film-removing property and paintability. As the method of post-treating a zinc-based plated steel sheet of the present invention employs a simple coating method irrespective of the kind of plating layer, the process is simple and economical and the process operation cost is low.

Coating process and coated materials
10814386 · 2020-10-27 · ·

The present invention relates to a method and an apparatus for coating large area solid substrates with metal based alloys or compounds by contacting the substrate surface with an unoxidised metal powders formed by in situ reaction of a metal halide and a reducing agent. The method is suitable for coating large area substrates such as flakes, powder, beads, and fibres with metal based alloys or compounds starting from low-cost chemicals such as metal chlorides. The method is particularly suited for production of substrates coated with metals, alloys and compounds based on Zn, Sn, Ag, Co, V, Ni, Cr, Fe, Cu, Pt, Pd, Ta, Nb, Rh, Ru, Mo, Os, Re and W.

Coating process and coated materials
10814386 · 2020-10-27 · ·

The present invention relates to a method and an apparatus for coating large area solid substrates with metal based alloys or compounds by contacting the substrate surface with an unoxidised metal powders formed by in situ reaction of a metal halide and a reducing agent. The method is suitable for coating large area substrates such as flakes, powder, beads, and fibres with metal based alloys or compounds starting from low-cost chemicals such as metal chlorides. The method is particularly suited for production of substrates coated with metals, alloys and compounds based on Zn, Sn, Ag, Co, V, Ni, Cr, Fe, Cu, Pt, Pd, Ta, Nb, Rh, Ru, Mo, Os, Re and W.

METHOD FOR PRODUCING AN OPEN-PORE MOLDED BODY WHICH IS MADE OF A METAL, AND A MOLDED BODY PRODUCED USING SAID METHOD

A method for producing open-pored molded bodies made of a metal. The surface of the metal open-pored molded body being used as a semi-finished product, is coated with particles of the same metal with which the semi-finished product is made or with particles of a chemical compound of the metal the semi-finished product is made, wherein the compound or particles can be reduced or thermally or chemically decomposed in a thermal treatment. After the coating process, a thermal treatment in a suitable atmosphere is carried out, in which the particles are connected to the surface of the semi-finished product and/or adjacent particles such that the specific surface area of the obtained open-pore molded body is increased to at least 30 m.sup.2/l and/or at least by a factor of 5 in comparison to the starting material.

METHOD FOR PRODUCING AN OPEN-PORE MOLDED BODY WHICH IS MADE OF A METAL, AND A MOLDED BODY PRODUCED USING SAID METHOD

A method for producing open-pored molded bodies made of a metal. The surface of the metal open-pored molded body being used as a semi-finished product, is coated with particles of the same metal with which the semi-finished product is made or with particles of a chemical compound of the metal the semi-finished product is made, wherein the compound or particles can be reduced or thermally or chemically decomposed in a thermal treatment. After the coating process, a thermal treatment in a suitable atmosphere is carried out, in which the particles are connected to the surface of the semi-finished product and/or adjacent particles such that the specific surface area of the obtained open-pore molded body is increased to at least 30 m.sup.2/l and/or at least by a factor of 5 in comparison to the starting material.

PRE-INITIATED OPTICAL FIBERS AND METHODS OF MAKING THEREOF
20200181777 · 2020-06-11 ·

Embodiments of the invention include a method of initiating an optical fiber. In some embodiments, a distal portion of the optical fiber is coated with an energy absorbing material. In some embodiments, the material includes a metal flakes or powder dispersed in a solution of organic solvents. After the material dries, laser energy is fired through the optical fiber. The laser energy can be absorbed in the material and ignites the organic solvents. This combustion melts the material of the optical fiber, and impregnates the optical fiber with the metal flakes or powder of the material. The resulting optical fiber is thus permanently modified so that the energy applied through the fiber is partially absorbed and converted to heat.