C01B25/36

Source of phosphate for agriculture and the food industry
10464853 · 2019-11-05 · ·

A source of phosphate for agriculture and food industry comprises a phosphate salt in solid form of formula M.sub.n(HPO4)y.zH2O in which M is Na, K, NH4, n=2, and y=1; or M is Ca, n=1, y=1; or M is Al or Fe, n=2, y=3; and in which z is 0, 1 or 2, wherein said phosphate salt has a phosphate content expressed as a P2O5 content of between 30 and 50% by weight of the phosphate salt, and it has a cadmium content lower than 0.40 ppm.

Method of treating phosphate-containing ash from waste-incineration plants by wet-chemical digestion in order to obtain compounds of aluminium, calcium, phosphorus and nitrogen

The invention concerns a method of treating phosphate-containing waste, in particular phosphate-containing ash from waste-incineration plants, by wet-chemical digestion in order to obtain compounds of aluminum, calcium, phosphorus and nitrogen.

Method of treating phosphate-containing ash from waste-incineration plants by wet-chemical digestion in order to obtain compounds of aluminium, calcium, phosphorus and nitrogen

The invention concerns a method of treating phosphate-containing waste, in particular phosphate-containing ash from waste-incineration plants, by wet-chemical digestion in order to obtain compounds of aluminum, calcium, phosphorus and nitrogen.

METHOD FOR PREPARATION OF ALUMINIUM PHOSPHATE GEL FOR APPLICATION IN VACCINE FORMULATIONS

The present invention relates to an improved process for production of Aluminium phosphate (AlPhos) gel wherein the solutions of aluminium salt and alkaline phosphate salt are added to water by maintaining the pH under stirring to obtain the precipitate, followed by sterilization of the said precipitate and finally obtaining the Aluminum phosphate gel.

METHOD FOR PREPARATION OF ALUMINIUM PHOSPHATE GEL FOR APPLICATION IN VACCINE FORMULATIONS

The present invention relates to an improved process for production of Aluminium phosphate (AlPhos) gel wherein the solutions of aluminium salt and alkaline phosphate salt are added to water by maintaining the pH under stirring to obtain the precipitate, followed by sterilization of the said precipitate and finally obtaining the Aluminum phosphate gel.

System and method for concentrating rare earth elements from coal byproducts/slag

The disclosure relates to a method for concentrating rare earth elements (REEs) from a coal byproduct. The method includes mixing the coal byproduct input with aluminum phosphate, sulfur and/or other compounds used as an additive; heating the coal byproduct input in air for a period of 3 minutes or longer at a temperature above a liquid starting temperature of the coal byproduct input, forming a molten coal byproduct; cooling the molten coal byproduct at a rate slower than critical glass transition cooling rate of the melt, forming REE phosphate product; heating the coal byproduct input above the liquid starting temperature of the coal byproduct after REE phosphate product is formed; and cooling the coal byproduct input at a rate faster than the critical glass transition cooling rate of the melt, minimizing forming unwanted solids.

System and method for concentrating rare earth elements from coal byproducts/slag

The disclosure relates to a method for concentrating rare earth elements (REEs) from a coal byproduct. The method includes mixing the coal byproduct input with aluminum phosphate, sulfur and/or other compounds used as an additive; heating the coal byproduct input in air for a period of 3 minutes or longer at a temperature above a liquid starting temperature of the coal byproduct input, forming a molten coal byproduct; cooling the molten coal byproduct at a rate slower than critical glass transition cooling rate of the melt, forming REE phosphate product; heating the coal byproduct input above the liquid starting temperature of the coal byproduct after REE phosphate product is formed; and cooling the coal byproduct input at a rate faster than the critical glass transition cooling rate of the melt, minimizing forming unwanted solids.

METHOD FOR THE HIGH EFFICIENCY RECYCLING OF IRON PHOSPHATE BLACK POWDER SLAG

This method recycles iron phosphate slag, which is produced as waste during lithium iron phosphate battery recycling processes that contain leaching or crushing for the sole extraction of lithium. This method extracts aluminum phosphate, iron phosphate, and lithium phosphate from the waste slag. The recycling process comprises these steps: (a) extraction of aluminum phosphate through addition of sodium hydroxide; (b) removal of carbon additives, graphite and other organic compounds through solvation of solely lithium, iron, and phosphate compounds through addition of sulfuric acid; (c) precipitation of iron phosphate by addition of hydrogen peroxide; (d) extraction of lithium phosphate from the mother liquor; (e) recycling of mother liquor into water and sodium sulfate. This process wastes few chemicals while still having a high reclamation efficiency in terms of purity and quantity. Furthermore, due to its relatively low costs, the profit margin of this process is very good.

METHOD FOR THE HIGH EFFICIENCY RECYCLING OF IRON PHOSPHATE BLACK POWDER SLAG

This method recycles iron phosphate slag, which is produced as waste during lithium iron phosphate battery recycling processes that contain leaching or crushing for the sole extraction of lithium. This method extracts aluminum phosphate, iron phosphate, and lithium phosphate from the waste slag. The recycling process comprises these steps: (a) extraction of aluminum phosphate through addition of sodium hydroxide; (b) removal of carbon additives, graphite and other organic compounds through solvation of solely lithium, iron, and phosphate compounds through addition of sulfuric acid; (c) precipitation of iron phosphate by addition of hydrogen peroxide; (d) extraction of lithium phosphate from the mother liquor; (e) recycling of mother liquor into water and sodium sulfate. This process wastes few chemicals while still having a high reclamation efficiency in terms of purity and quantity. Furthermore, due to its relatively low costs, the profit margin of this process is very good.

Aqueous Solution Containing Aluminum Ions, Lactate Ions, and Phosphate Ions, and a Method for Their Production

The invention relates to an aqueous solution containing aluminum ions, characterized in that the solution contains aluminum ions in a proportion of 0.5-15% (converted, if necessary, to Al.sup.3+) based on the total mass of the solution, as well as anions of lactic acid (lactate ions) and of phosphoric acid (phosphate ions), and has the theoretical composition Al.sup.3+.sub.A(C.sub.3H.sub.5O.sub.3.sup.).sub.x.AS.sup.M.sub.y.A(H.sub.2PO.sub.4.sup.).sub.z.A(OH).sup..sub.(3A-x.A-M.y.A-z.A), wherein S is the anion of an acid with the charge M, x is a value in the range of 0.5-2.8, y is a value in the range of 0-1.5, and z is a value in the range of 0.01-1.5.