The present disclosure relates to compositions comprising at least two different carbonaceous components, at least one being a surface-modified carbonaceous particulate material typically having a relatively high spring-back, and at least one other component being a carbonaceous particulate material (such as graphite) generally having a lower spring-back and/or a higher BET specific surface area than the surface-modified carbonaceous material component. Such compositions are particularly useful for making negative electrodes for lithium-ion batteries and the like in view of their beneficial electrochemical properties, particularly in automotive and energy storage applications. The present disclosure also relates to the use of a low-spring-back carbonaceous particulate materials as an additive in carbonaceous compositions, wherein said compositions are used to prepare anodes for Li-ion batteries in order to increase the electrode density, the cell capacity and/or the cycling stability of said battery while maintaining the power density of the cell compared to a cell with an anode absent the carbonaceous additive.

The present disclosure relates to compositions comprising at least two different carbonaceous components, at least one being a surface-modified carbonaceous particulate material typically having a relatively high spring-back, and at least one other component being a carbonaceous particulate material (such as graphite) generally having a lower spring-back and/or a higher BET specific surface area than the surface-modified carbonaceous material component. Such compositions are particularly useful for making negative electrodes for lithium-ion batteries and the like in view of their beneficial electrochemical properties, particularly in automotive and energy storage applications. The present disclosure also relates to the use of a low-spring-back carbonaceous particulate materials as an additive in carbonaceous compositions, wherein said compositions are used to prepare anodes for Li-ion batteries in order to increase the electrode density, the cell capacity and/or the cycling stability of said battery while maintaining the power density of the cell compared to a cell with an anode absent the carbonaceous additive.

The present invention provides a method for the manufacture of reduced graphene oxide from Kish graphite.

The present invention provides a method for the manufacture of reduced graphene oxide from Kish graphite.

To provide a manufacturing method of graphene oxide that allows mass production through a relatively simple process, at low costs, and with safety and efficiency. A hydrogen peroxide solution, sulfuric acid, and flake graphite are put in a reaction container, and the mixture is stirred to obtain expansion graphite. The synthesized expansion graphite is washed not with pure water but with a saturated aqueous solution of magnesium sulfate (MgSO.sub.4) or an organic solvent, whereby a large amount of sulfuric acid is contained between graphite layers. The expansion graphite is subjected to heat treatment or microwave irradiation to form expanded graphite, and a graphite layer is peeled by ultrasonic treatment and then oxidized to form a graphene compound.

To provide a manufacturing method of graphene oxide that allows mass production through a relatively simple process, at low costs, and with safety and efficiency. A hydrogen peroxide solution, sulfuric acid, and flake graphite are put in a reaction container, and the mixture is stirred to obtain expansion graphite. The synthesized expansion graphite is washed not with pure water but with a saturated aqueous solution of magnesium sulfate (MgSO.sub.4) or an organic solvent, whereby a large amount of sulfuric acid is contained between graphite layers. The expansion graphite is subjected to heat treatment or microwave irradiation to form expanded graphite, and a graphite layer is peeled by ultrasonic treatment and then oxidized to form a graphene compound.

The present invention relates to a mechanochemically carbonated magnesium silicate which has a BET surface area within the range of 20 to 100 m.sup.2/g, preferably 30 to 80 m.sup.2/g, more preferably 40 to 70 m.sup.2/g, most preferably 45 to 65 m.sup.2/g and/or an amorphous content as determined by XRD of at least 30 wt. %, preferably at least 40 wt. %, more preferably at least 50 wt. %, even more preferably at least 60 wt. % a CO.sub.2 content of at least 3 wt. %. The invention further relates to methods of its production and uses thereof, for example as a filler in polymers. The compositions comprising the mechanochemically carbonated magnesium silicate and a polymer (such as a polyolefin) provide the benefits of being a CO.sub.2 negative material having excellent functional properties which can be used for a variety of purposes, for example as a component of clothing or apparel, or as a component of backpacks such as a buckle.

A water-based wellbore fluid may include an aqueous base fluid and a modified graphene shale inhibitor that comprises one or more substituents that are covalently bonded to graphene via a linking group. One of the one or more substituents may be a hydrocarbon group that has a number of carbon atoms in the range from 8 to 14.

A water-based wellbore fluid may include an aqueous base fluid and a modified graphene shale inhibitor that comprises one or more substituents that are covalently bonded to graphene via a linking group. One of the one or more substituents may be a hydrocarbon group that has a number of carbon atoms in the range from 8 to 14.

A hydrogen sensor that efficiently detects hydrogen gas at room temperature comprising a gold decorated reduced graphene oxide/zinc oxide (Au/rGO/ZnO) heterostructured composite, methods for making this sensor and a method for sensitive room temperature detection of hydrogen using the sensor.