C01G23/053

Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates
11465129 · 2022-10-11 · ·

A method of making a titanium dioxide nanowire array includes contacting a substrate with a solvent comprising a titanium (III) precursor, an acid, and an oxidant while microwave heating the solvent, thereby forming a hydrogen titanate H2Ti2O5.H2O nanowire array. The hydrogen titanate nanowire array is annealed to form a titanium dioxide nanowire array. The substrate is seeded with titanium dioxide before starting the hydrothermal synthesis of the hydrogen titanate nanowire array. The titanium dioxide nanowire array is loaded with a platinum group metal to form an exhaust gas catalyst. The titanium dioxide nanowire array can be used to catalyze oxidation of combustion exhaust.

Conductive materials made of Nb-doped TiO.SUB.2 .particles

A method for producing conductive materials from Nb-doped TiO2-particles, in which Nb-doped TiO2-particles are pressed to form bodies and the bodies are treated in an oxygen-containing atmosphere and at a reducing atmosphere.

Conductive materials made of Nb-doped TiO.SUB.2 .particles

A method for producing conductive materials from Nb-doped TiO2-particles, in which Nb-doped TiO2-particles are pressed to form bodies and the bodies are treated in an oxygen-containing atmosphere and at a reducing atmosphere.

RUTHENIUM-TITANIUM OXIDE AEROGEL CATALYST, METHOD FOR PREPARING THE SAME, AND METHOD FOR HYDROGENATION AND HYDRODEOXYGENATION USING THE SAME

Disclosed herein is a metal oxide aerogel catalyst for hydrogenation and/or hydrodeoxygenation, a method for preparing the same, and a method for hydrogenation and/or hydrodeoxygenation using the same. The catalyst consists of a metal and an oxide thereof, and the catalyst is in a form of an aerogel produced by supercritical drying. The catalyst has an effect of providing high hydrogenation and/or hydrodeoxygenation efficiency of an oxygen-containing compound.

Production of Nanoparticulate Titanium Dioxide
20170355612 · 2017-12-14 ·

The invention relates to a method for obtaining nanoparticulate titanium dioxide in agglomerate form from a hydrolyzed acidic titanyl compound, the thus obtained titanium dioxide as well as the use thereof as a photocatalyst, process catalyst or adsorbent, especially in aqueous systems.

Production of Nanoparticulate Titanium Dioxide
20170355612 · 2017-12-14 ·

The invention relates to a method for obtaining nanoparticulate titanium dioxide in agglomerate form from a hydrolyzed acidic titanyl compound, the thus obtained titanium dioxide as well as the use thereof as a photocatalyst, process catalyst or adsorbent, especially in aqueous systems.

Method for producing dispersion of iron-containing rutile titanium oxide fine particles, iron-containing rutile titanium oxide fine particles, and use thereof

Provided are titanium oxide fine particles which are excellent in transparency and are less photocatalytically active while maintaining a high refractive index, a dispersion of such fine particles, and a method for producing such a dispersion. The method for producing a dispersion of iron-containing rutile titanium oxide fine particles including a step (1) of neutralizing an aqueous metal mineral acid salt solution containing Ti and Fe in Fe.sub.2O.sub.3/(TiO.sub.2+Fe.sub.2O.sub.3)=0.001 to 0.010 to form an iron-containing hydrous titanic acid; a step (2) of adding an aqueous hydrogen peroxide solution to form an aqueous solution of iron-containing peroxotitanic acid having an average particle size of 15 to 50 nm; a step (3) of adding a tin compound so as to satisfy TiO.sub.2/SnO.sub.2=6 to 16; a step (4) of adding a sol of silica-based fine particles which contain Si and a metal element M in SiO.sub.2/MO.sub.x/2=99.9/0.1 to 80/20, the addition being made so as to satisfy SiO.sub.2/(oxides of the other elements)=0.08 to 0.22; and a step (5) of hydrothermally treating the solution obtained in the step (4).

Method for producing dispersion of iron-containing rutile titanium oxide fine particles, iron-containing rutile titanium oxide fine particles, and use thereof

Provided are titanium oxide fine particles which are excellent in transparency and are less photocatalytically active while maintaining a high refractive index, a dispersion of such fine particles, and a method for producing such a dispersion. The method for producing a dispersion of iron-containing rutile titanium oxide fine particles including a step (1) of neutralizing an aqueous metal mineral acid salt solution containing Ti and Fe in Fe.sub.2O.sub.3/(TiO.sub.2+Fe.sub.2O.sub.3)=0.001 to 0.010 to form an iron-containing hydrous titanic acid; a step (2) of adding an aqueous hydrogen peroxide solution to form an aqueous solution of iron-containing peroxotitanic acid having an average particle size of 15 to 50 nm; a step (3) of adding a tin compound so as to satisfy TiO.sub.2/SnO.sub.2=6 to 16; a step (4) of adding a sol of silica-based fine particles which contain Si and a metal element M in SiO.sub.2/MO.sub.x/2=99.9/0.1 to 80/20, the addition being made so as to satisfy SiO.sub.2/(oxides of the other elements)=0.08 to 0.22; and a step (5) of hydrothermally treating the solution obtained in the step (4).

CONTINUOUS FLOW PROCESS FOR MANUFACTURING SURFACE MODIFIED METAL OXIDE NANOPARTICLES BY SUPERCRITICAL SOLVOTHERMAL SYNTHESIS
20170349757 · 2017-12-07 ·

The invention concerns a continuous flow process for manufacturing surface modified metal oxide nanoparticles by supercritical solvothermal synthesis in an reaction medium flowing within a continuous flow chamber, said continuous flow chamber containing a hydrolysis area and a supercritical area, said process comprising the introduction of a flow of metal oxide precursor into the continuous flow chamber at a point P located in the hydrolysis area or in the supercritical area, and the introduction of a flow of is located downstream of P1 with respect to the flow direction, as well as the device for carrying out this process.

Synthesis of Janus Nanomaterials
20230183077 · 2023-06-15 ·

Synthesizing Janus nanoparticles including forming a lamellar phase having water layers, organic layers, and a surfactant, and reacting chemical precursors in the lamellar phase to form the Janus nanoparticles at interfaces of the water layers with the organic layers.