Patent classifications
C01G23/053
Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates
A method of making a titanium dioxide nanowire array includes contacting a substrate with a solvent comprising a titanium (III) precursor, an acid, and an oxidant while microwave heating the solvent, thereby forming a hydrogen titanate H2Ti2O5.H2O nanowire array. The hydrogen titanate nanowire array is annealed to form a titanium dioxide nanowire array. The substrate is seeded with titanium dioxide before starting the hydrothermal synthesis of the hydrogen titanate nanowire array. The titanium dioxide nanowire array is loaded with a platinum group metal to form an exhaust gas catalyst. The titanium dioxide nanowire array can be used to catalyze oxidation of combustion exhaust.
Conductive materials made of Nb-doped TiO.SUB.2 .particles
A method for producing conductive materials from Nb-doped TiO2-particles, in which Nb-doped TiO2-particles are pressed to form bodies and the bodies are treated in an oxygen-containing atmosphere and at a reducing atmosphere.
Conductive materials made of Nb-doped TiO.SUB.2 .particles
A method for producing conductive materials from Nb-doped TiO2-particles, in which Nb-doped TiO2-particles are pressed to form bodies and the bodies are treated in an oxygen-containing atmosphere and at a reducing atmosphere.
RUTHENIUM-TITANIUM OXIDE AEROGEL CATALYST, METHOD FOR PREPARING THE SAME, AND METHOD FOR HYDROGENATION AND HYDRODEOXYGENATION USING THE SAME
Disclosed herein is a metal oxide aerogel catalyst for hydrogenation and/or hydrodeoxygenation, a method for preparing the same, and a method for hydrogenation and/or hydrodeoxygenation using the same. The catalyst consists of a metal and an oxide thereof, and the catalyst is in a form of an aerogel produced by supercritical drying. The catalyst has an effect of providing high hydrogenation and/or hydrodeoxygenation efficiency of an oxygen-containing compound.
Production of Nanoparticulate Titanium Dioxide
The invention relates to a method for obtaining nanoparticulate titanium dioxide in agglomerate form from a hydrolyzed acidic titanyl compound, the thus obtained titanium dioxide as well as the use thereof as a photocatalyst, process catalyst or adsorbent, especially in aqueous systems.
Production of Nanoparticulate Titanium Dioxide
The invention relates to a method for obtaining nanoparticulate titanium dioxide in agglomerate form from a hydrolyzed acidic titanyl compound, the thus obtained titanium dioxide as well as the use thereof as a photocatalyst, process catalyst or adsorbent, especially in aqueous systems.
Method for producing dispersion of iron-containing rutile titanium oxide fine particles, iron-containing rutile titanium oxide fine particles, and use thereof
Provided are titanium oxide fine particles which are excellent in transparency and are less photocatalytically active while maintaining a high refractive index, a dispersion of such fine particles, and a method for producing such a dispersion. The method for producing a dispersion of iron-containing rutile titanium oxide fine particles including a step (1) of neutralizing an aqueous metal mineral acid salt solution containing Ti and Fe in Fe.sub.2O.sub.3/(TiO.sub.2+Fe.sub.2O.sub.3)=0.001 to 0.010 to form an iron-containing hydrous titanic acid; a step (2) of adding an aqueous hydrogen peroxide solution to form an aqueous solution of iron-containing peroxotitanic acid having an average particle size of 15 to 50 nm; a step (3) of adding a tin compound so as to satisfy TiO.sub.2/SnO.sub.2=6 to 16; a step (4) of adding a sol of silica-based fine particles which contain Si and a metal element M in SiO.sub.2/MO.sub.x/2=99.9/0.1 to 80/20, the addition being made so as to satisfy SiO.sub.2/(oxides of the other elements)=0.08 to 0.22; and a step (5) of hydrothermally treating the solution obtained in the step (4).
Method for producing dispersion of iron-containing rutile titanium oxide fine particles, iron-containing rutile titanium oxide fine particles, and use thereof
Provided are titanium oxide fine particles which are excellent in transparency and are less photocatalytically active while maintaining a high refractive index, a dispersion of such fine particles, and a method for producing such a dispersion. The method for producing a dispersion of iron-containing rutile titanium oxide fine particles including a step (1) of neutralizing an aqueous metal mineral acid salt solution containing Ti and Fe in Fe.sub.2O.sub.3/(TiO.sub.2+Fe.sub.2O.sub.3)=0.001 to 0.010 to form an iron-containing hydrous titanic acid; a step (2) of adding an aqueous hydrogen peroxide solution to form an aqueous solution of iron-containing peroxotitanic acid having an average particle size of 15 to 50 nm; a step (3) of adding a tin compound so as to satisfy TiO.sub.2/SnO.sub.2=6 to 16; a step (4) of adding a sol of silica-based fine particles which contain Si and a metal element M in SiO.sub.2/MO.sub.x/2=99.9/0.1 to 80/20, the addition being made so as to satisfy SiO.sub.2/(oxides of the other elements)=0.08 to 0.22; and a step (5) of hydrothermally treating the solution obtained in the step (4).
CONTINUOUS FLOW PROCESS FOR MANUFACTURING SURFACE MODIFIED METAL OXIDE NANOPARTICLES BY SUPERCRITICAL SOLVOTHERMAL SYNTHESIS
The invention concerns a continuous flow process for manufacturing surface modified metal oxide nanoparticles by supercritical solvothermal synthesis in an reaction medium flowing within a continuous flow chamber, said continuous flow chamber containing a hydrolysis area and a supercritical area, said process comprising the introduction of a flow of metal oxide precursor into the continuous flow chamber at a point P located in the hydrolysis area or in the supercritical area, and the introduction of a flow of is located downstream of P1 with respect to the flow direction, as well as the device for carrying out this process.
Synthesis of Janus Nanomaterials
Synthesizing Janus nanoparticles including forming a lamellar phase having water layers, organic layers, and a surfactant, and reacting chemical precursors in the lamellar phase to form the Janus nanoparticles at interfaces of the water layers with the organic layers.