Patent classifications
C01G23/053
Manufacturing method of titanium dioxide solution and titanium dioxide film
The manufacturing method of titanium dioxide solution includes: mixing choline chloride, urea, boric acid, and titanium tetrachloride to form a first solution, wherein a molar concentration ratio of choline chloride to urea is 1:2, a molar concentration of titanium tetrachloride is 0.2 M to 0.4 M, and weight/volume of boric acid is 5 g/300 ml to 15 g/300 ml; and heating the first solute ion to form a second solution, wherein the second solution contains carbon/nitrogen doped titanium dioxide. In the manufacturing method of the present disclosure, the deep eutectic solution formed by choline chloride and urea may be used as a solvent, and may also be used as a carbon source and/or a nitrogen source. Therefore, titanium dioxide may be doped with carbon and/or nitrogen during the formation process.
METHOD FOR MAKING COFFEE HUSK REDUCING AGENT
An efficient green method for the synthesis of noble metal/transition metal oxide nanocomposite comprising reducing noble metal salt and a templating metal oxide is disclosed. The method is a one-step method comprises mixing coffee seed husk extract, a noble metal precursor, and a transition metal precursor; and filtering and drying the nanocomposite. The nanocomposite prepared by the method of the invention displays all the characteristics and biocidal activity of a composite prepared by traditional methods.
ROOM TEMPERATURE MULTIFERROIC THIN FILMS
Various examples are provided for multiferroic thin films. In one example, a multiferroic thin film device includes a thin film of multiferroic material and an electrode disposed on a side of the thin film of multiferroic material. The multiferroic material can be (Fe.sub.x,Sr.sub.1-x)TiO.sub.3 In another example, a method for producing a multiferroic thin film includes forming a multiferroic pre-cursor; disposing the multiferroic precursor on a substrate to form a multiferroic coating; pre-baking the multiferroic coating on the substrate to form a pre-baked multiferroic thin film; and annealing the pre-baked multiferroic thin film under an oxygen atmosphere to form a crystalized multiferroic thin film. One or more electrodes can be formed on the crystalized multiferroic thin film.
ROOM TEMPERATURE MULTIFERROIC THIN FILMS
Various examples are provided for multiferroic thin films. In one example, a multiferroic thin film device includes a thin film of multiferroic material and an electrode disposed on a side of the thin film of multiferroic material. The multiferroic material can be (Fe.sub.x,Sr.sub.1-x)TiO.sub.3 In another example, a method for producing a multiferroic thin film includes forming a multiferroic pre-cursor; disposing the multiferroic precursor on a substrate to form a multiferroic coating; pre-baking the multiferroic coating on the substrate to form a pre-baked multiferroic thin film; and annealing the pre-baked multiferroic thin film under an oxygen atmosphere to form a crystalized multiferroic thin film. One or more electrodes can be formed on the crystalized multiferroic thin film.
METHOD FOR PRODUCING TITANIUM OXIDE PARTICLES, TITANIUM OXIDE PARTICLES, DISPERSION SOLUTION OF TITANIUM OXIDE PARTICLES, TITANIUM OXIDE PASTE, TITANIUM OXIDE FILM, AND DYE-SENSITIZED SOLAR CELL
The present invention relates to a method for producing titanium oxide particles, comprising a step of producing a mixed solution by mixing a hydrolysis product of a titanium alkoxide or a titanium metal salt and a compound having a five-membered ring containing nitrogen and a step of generating titanium oxide fine particles by heating and pressurizing the mixed solution, titanium oxide particles produced by the same production method, a dispersion solution of titanium oxide particles produced using the same titanium oxide particles, titanium oxide paste, a titanium oxide film, and a dye-sensitized solar cell.
METHOD FOR PRODUCING TITANIUM OXIDE PARTICLES, TITANIUM OXIDE PARTICLES, DISPERSION SOLUTION OF TITANIUM OXIDE PARTICLES, TITANIUM OXIDE PASTE, TITANIUM OXIDE FILM, AND DYE-SENSITIZED SOLAR CELL
The present invention relates to a method for producing titanium oxide particles, comprising a step of producing a mixed solution by mixing a hydrolysis product of a titanium alkoxide or a titanium metal salt and a compound having a five-membered ring containing nitrogen and a step of generating titanium oxide fine particles by heating and pressurizing the mixed solution, titanium oxide particles produced by the same production method, a dispersion solution of titanium oxide particles produced using the same titanium oxide particles, titanium oxide paste, a titanium oxide film, and a dye-sensitized solar cell.
TITANIUM OXIDE POWDER, AND DISPERSION AND COSMETICS USING SAME
A titanium oxide powder of the present invention has a BET specific surface area of 5 m.sup.2/g or higher and 15 m.sup.2/g or lower and contains single-crystalline titanium oxide particles, in which a value (d10/d50) that is obtained by dividing a value (d10), which is obtained when a particle size distribution represented by a cumulative volume percentage of primary particle diameters of the titanium oxide particles is 10%, by a value (d50), which is obtained when a particle size distribution represented by a cumulative volume percentage thereof is 50%, is 0.3 or higher and 1 or lower, an amount of titanium oxide thereof is 99.0% by mass or more, and the titanium oxide powder has an anatase-type crystalline phase.
METHOD FOR PRODUCING CHIRAL METAL OXIDE STRUCTURE, AND CHIRAL POROUS STRUCTURE
A method for producing a chiral metal oxide structure, involves a sol-gel step of allowing a transition metal compound having a bi- or higher dentate chelate ligand to act on a chiral supramolecular crystal of an acid-base complex containing a polymer having a linear polyethyleneimine skeleton and a chiral dicarboxylic acid compound having two carboxyl groups and four or more carbon atoms to form a metal oxide layer on a surface of the chiral supramolecular crystal; and a calcination step of thermally decomposing the organic chiral supramolecular crystal after the sol-gel step to generate a transition metal oxide structure composed of the metal oxide layer prepared with the supramolecular crystal as a template.
METHOD FOR PRODUCING CHIRAL METAL OXIDE STRUCTURE, AND CHIRAL POROUS STRUCTURE
A method for producing a chiral metal oxide structure, involves a sol-gel step of allowing a transition metal compound having a bi- or higher dentate chelate ligand to act on a chiral supramolecular crystal of an acid-base complex containing a polymer having a linear polyethyleneimine skeleton and a chiral dicarboxylic acid compound having two carboxyl groups and four or more carbon atoms to form a metal oxide layer on a surface of the chiral supramolecular crystal; and a calcination step of thermally decomposing the organic chiral supramolecular crystal after the sol-gel step to generate a transition metal oxide structure composed of the metal oxide layer prepared with the supramolecular crystal as a template.
Anode for secondary battery, method for producing same, and secondary battery
In this anode for a secondary battery, method for producing same, and secondary battery, an anode active material is laminated on a surface of a metal foil, the anode active material contains at least titanium dioxide, and the titanium dioxide contains a Brookite crystal phase and contains an amorphous phase in a ratio of 1 vol % to 20 vol %.