C04B35/5805

System and method for applying high temperature corrosion resistant amorphous based coatings

An embodiment relates to a material comprising a ceramic formed from an amorphous metal alloy (amorphous metal ceramic composite), wherein the composite exhibits a higher corrosion resistance than that of Haynes 230 when exposed to molten chlorides such as KCl or MgCl.sub.2 or combinations thereof at temperatures up to 750° C. Yet, another embodiment relates to a method comprising obtaining a substrate, forming a coating of an amorphous metal alloy, heating the coating, and transforming at least a portion the amorphous metal alloy into an amorphous metalceramic composite.

ADDITIVE MANUFACTURING POWDERS WITH IMPROVED PHYSICAL CHARACTERISTICS, METHOD OF MANUFACTURE AND USE THEREOF
20220288676 · 2022-09-15 ·

In additive manufacturing operations, powders used in stereolithographic processes need to be precisely spread out in a uniform fashion at every pass of the stereolithographic process to ensure predictability in powder surface morphology. Typically, this is difficult to achieve with conventional powders because often these powders suffer from poor flowability, which may further deteriorate over time, and impairs the efficiency of the stereolithographic processes. The present disclosure describes additive manufacturing powders having improved physical characteristics such as flowability and tap density, which are less sensitive or insensitive to ambient humidity. For example, there is described a powder that includes spherical particles having a particle size distribution of less than 1000 micrometers and having a measurable flowability as determined in accordance with ASTM B213 at 75% relative humidity.

Method of fabricating a composite material part by injecting a filled slurry into a fiber texture
11285638 · 2022-03-29 · ·

A method of fabricating a composite material part includes placing a fiber texture in a mold including in its bottom portion a porous material part on which a first face of the texture rests, injecting a liquid under pressure into the fiber texture, the liquid containing a powder of refractory ceramic particles, and draining through the porous material part the liquid that has passed through the fiber texture, while retaining the powder of refractory ceramic particles inside said texture by the porous material part. A perforated rigid element is interposed between the bottom of the mold and the porous material part.

Systems and methods for making ceramic powders

Systems and methods for making ceramic powders configured with consistent, tailored characteristics and/or properties are provided herein. In some embodiments a system for making ceramic powders, includes: a reactor body having a reaction chamber and configured with a heat source to provide a hot zone along the reaction chamber; a sweep gas inlet configured to direct a sweep gas into the reaction chamber and a sweep gas outlet configured to direct an exhaust gas from the reaction chamber; a plurality of containers, within the reactor body, configured to retain at least one preform, wherein each container is configured to permit the sweep gas to flow therethrough, wherein the preform is configured to permit the sweep gas to flow there through, such that the precursor mixture is reacted in the hot zone to form a ceramic powder product having uniform properties.

ADDITIVE MANUFACTURING METHOD FOR MAKING NON-OXIDE CERAMIC ARTICLES, AND AEROGELS, XEROGELS, AND POROUS CERAMIC ARTICLES

The present disclosure provides a method of making a non-oxide ceramic part. The method includes obtaining a photopolymerizable slurry; selectively curing the photopolymerizable slurry to obtain a gelled article; drying the gelled article to form an aerogel article or a xerogel article; heat treating the aerogel article or the xerogel article to form a porous ceramic article; and sintering the porous ceramic article to obtain a sintered ceramic article. The photopolymerizable slurry includes non-oxide ceramic particles; at least one radiation curable monomer; a solvent; a photoinitiator; an inhibitor; and at least one sintering aid. Further, aerogels, xerogels, porous ceramic articles, and non-oxide ceramic articles are provided. In addition, methods are provided, including receiving, by a manufacturing device having one or more processors, a digital object comprising data specifying an article; and generating, with the manufacturing device by an additive manufacturing process, the article based on the digital object. A system is also provided, including a display that displays a 3D model of an article; and one or more processors that, in response to the 3D model selected by a user, cause a 3D printer to create a physical object of an article.

Method for additive manufacturing of 3D-printed articles

The present invention provides a method of additive manufacturing a 3D-printed article, comprising: (a) printing and depositing one or more layers of a slurry by using a 3D printer, wherein the slurry comprises a ceramic powder composition; (b) further injecting an oil around the one or more layers of slurry, wherein the height of the injected oil is lower than the height of the slurry; (c) repeating steps (a) and (b) until a main body with desired geometric shape is obtained; and (d) sintering the main body by heating to obtain the 3D-printed article wherein the temperature of a printing carrier of the 3D printer is from 30 to 80° C.

NEGATIVE ELECTRODE ACTIVE MATERIAL, NEGATIVE ELECTRODE INCLUDING THE SAME, SECONDARY BATTERY INCLUDING THE NEGATIVE ELECTRODE, AND PREPARATION METHOD OF THE NEGATIVE ELECTRODE ACTIVE MATERIAL

A negative electrode active material including a silicon-carbon-based particle, the silicon-carbon-based particle having a SiC.sub.x matrix and boron doped in the SiC.sub.x matrix, wherein x of the SiC.sub.x matrix is 0.3 or more and less than 0.6.

SYSTEM AND METHOD FOR APPLYING HIGH TEMPERATURE CORROSION RESISTANT AMORPHOUS BASED COATINGS
20210198777 · 2021-07-01 ·

An embodiment relates to a material comprising a ceramic formed from an amorphous metal alloy (amorphous metal ceramic composite), wherein the composite exhibits a higher corrosion resistance than that of Haynes 230 when exposed to molten chlorides such as KCl or MgCl.sub.2 or combinations thereof at temperatures up to 750° C. Yet, another embodiment relates to a method comprising obtaining a substrate, forming a coating of an amorphous metal alloy, heating the coating, and transforming at least a portion the amorphous metal alloy into an amorphous metalceramic composite.

A ceramic nuclear fuel pellet, a fuel rod, and a fuel assembly

A fuel assembly for a nuclear reactor, a fuel rod of the fuel assembly, and a ceramic nuclear fuel pellet of the fuel rod are disclosed. The fuel pellet includes a first fissile material of UB.sub.2, The boron of the UB.sub.2 is enriched to have a concentration of the isotope .sup.11B that is higher than for natural B.

Method for Producing Non-Oxide Ceramic Powders
20210147301 · 2021-05-20 ·

The invention relates to a method for producing a non-oxide ceramic powder comprising a nitride, a carbide, a boride or at least one MAX phase with the general composition Mn+1AXn, where M=at least one element from the group of transition elements (Sc, Ti, V, Cr, Zr, Nb, Mo, Hf and Ta), A=at least one A group element from the group (Si, Al, Ga, Ge, As, Cd, In, Sn, Tl and Pb), X=carbon (C) and/or nitrogen (N) and/or boron (B), and n=1, 2 or 3. According to the invention, corresponding quantities of elementary starting materials or other precursors are mixed with at least one metal halide salt (NZ), compressed (pellet), and heated for synthesis with a metal halide salt (NZ). The compressed pellet is first enveloped with another metal halide salt, compressed again, arranged in a salt bath and heated therewith until the melting temperature of the salt is exceeded. Optionally, melted silicate can be added, which prevents the salt from evaporating at high temperatures. Advantageously, the method can be carried out in the presence of air.