The invention relates to a method of making a reinforced catalytic microporous and/or mesoporous bound composition comprising the steps of: providing a pre-formed catalytic crystalline material; mixing the catalytic crystalline material with water, a metal oxide binder, and a reinforcing glass fiber to form an extrudable composition; extruding the extrudable slurry under conditions sufficient to form the reinforced catalytic bound extrudate; and calcining the reinforced catalytic bound extrudate at a temperature and for a time sufficient to form a calcined reinforced catalytic bound catalyst. Advantageously, the reinforcing glass fiber can have a diameter from 5-100 microns and a length-to-diameter ratio from 300:1-3000:1 and can be present in an amount from about 1-50 parts, based on about 1000 parts combined of catalytic crystalline material and metal oxide binder.

The invention relates to a method of making a reinforced catalytic microporous and/or mesoporous bound composition comprising the steps of: providing a pre-formed catalytic crystalline material; mixing the catalytic crystalline material with water, a metal oxide binder, and a reinforcing glass fiber to form an extrudable composition; extruding the extrudable slurry under conditions sufficient to form the reinforced catalytic bound extrudate; and calcining the reinforced catalytic bound extrudate at a temperature and for a time sufficient to form a calcined reinforced catalytic bound catalyst. Advantageously, the reinforcing glass fiber can have a diameter from 5-100 microns and a length-to-diameter ratio from 300:1-3000:1 and can be present in an amount from about 1-50 parts, based on about 1000 parts combined of catalytic crystalline material and metal oxide binder.

The present invention generally relates to the use of pre-formed bodies of Chemically Bonded Ceramics (CBCs) biomaterial for implantation purposes wherein the bodies are prepared ex vivo allowing process parameters to be optimized for desired long term properties of the resulting CBC biomaterial. More particularly, the pre-formed CBC material bodies of the present invention are sintered. The pre-formed body of CBC material is machined to the desired geometry and then implanted using a CBC cementation paste for fixation of the body to tissue. The invention also relates to a method of preparing pre-formed bodies of CBC biomaterial for implantation purposes, methods of preparing an implant thereof having desired geometry, and a method of implantation of the implant, as well as a kit for use in the method of implantation.

The present invention generally relates to the use of pre-formed bodies of Chemically Bonded Ceramics (CBCs) biomaterial for implantation purposes wherein the bodies are prepared ex vivo allowing process parameters to be optimized for desired long term properties of the resulting CBC biomaterial. More particularly, the pre-formed CBC material bodies of the present invention are sintered. The pre-formed body of CBC material is machined to the desired geometry and then implanted using a CBC cementation paste for fixation of the body to tissue. The invention also relates to a method of preparing pre-formed bodies of CBC biomaterial for implantation purposes, methods of preparing an implant thereof having desired geometry, and a method of implantation of the implant, as well as a kit for use in the method of implantation.

The invention concerns an article (20) formed of a ceramic matrix composite structure having a plurality of ceramic fiber layers (22) and a binder material (24) interspersed throughout said layers. The ceramic matrix composite material may be sintered. The ceramic fiber layers undulate relative to one or more outer surfaces (38;40) of the article. Thus support features (48) within the article are able to share a load in use between a plurality of layers. The invention may be suited to engine components such as turbine seal segments in a gas turbine engine.

The invention concerns an article (20) formed of a ceramic matrix composite structure having a plurality of ceramic fiber layers (22) and a binder material (24) interspersed throughout said layers. The ceramic matrix composite material may be sintered. The ceramic fiber layers undulate relative to one or more outer surfaces (38;40) of the article. Thus support features (48) within the article are able to share a load in use between a plurality of layers. The invention may be suited to engine components such as turbine seal segments in a gas turbine engine.

A method of manufacturing a catalytic sieve includes providing starting materials of an aggregate, a cementing agent, a sublimation agent and water. The sublimation agent (between 25% and 50% by weight of the cementing agent) is selected from molybdenum disulfide, tungsten disulfide, vanadium disulfide, copper sulfate, and combinations thereof. The aggregate contains at least 2% by weight of at least one transition metal. The method includes mixing the starting materials to achieve a mixture, placing the mixture into a form, and curing the mixture in the form to allow the mixture to become a solidified unit defined by a minimum dimension of thickness, length, width or diameter. The method further includes placing the solidified unit into a kiln, heating the kiln to 1115°−1350° C., maintaining the kiln at the temperature for between 10-60 minutes per centimeter of the minimum dimension, and removing the solidified unit from the kiln.

A method of manufacturing a catalytic sieve includes providing starting materials of an aggregate, a cementing agent, a sublimation agent and water. The sublimation agent (between 25% and 50% by weight of the cementing agent) is selected from molybdenum disulfide, tungsten disulfide, vanadium disulfide, copper sulfate, and combinations thereof. The aggregate contains at least 2% by weight of at least one transition metal. The method includes mixing the starting materials to achieve a mixture, placing the mixture into a form, and curing the mixture in the form to allow the mixture to become a solidified unit defined by a minimum dimension of thickness, length, width or diameter. The method further includes placing the solidified unit into a kiln, heating the kiln to 1115°−1350° C., maintaining the kiln at the temperature for between 10-60 minutes per centimeter of the minimum dimension, and removing the solidified unit from the kiln.

Disclosed is a calcium aluminate cement, including a calcium aluminate with a first crystallised mineralogical phase of calcium dialuminate CA2 including one calcium oxide CaO for two aluminium oxides Al.sub.2O.sub.3 and/or a second crystallised mineralogical phase of dicalcium alumina silicate C2AS including two calcium oxides CaO for one aluminium oxide Al.sub.2O.sub.3 and one silicon dioxide SiO.sub.2. The mass fraction of all of the first and second mineralogical phases in the calcium aluminate is greater than or equal to 80%.

Disclosed is a calcium aluminate cement, including a calcium aluminate with a first crystallised mineralogical phase of calcium dialuminate CA2 including one calcium oxide CaO for two aluminium oxides Al.sub.2O.sub.3 and/or a second crystallised mineralogical phase of dicalcium alumina silicate C2AS including two calcium oxides CaO for one aluminium oxide Al.sub.2O.sub.3 and one silicon dioxide SiO.sub.2. The mass fraction of all of the first and second mineralogical phases in the calcium aluminate is greater than or equal to 80%.