C04B2235/726

RESIN FORMULATIONS FOR POLYMER-DERIVED CERAMIC MATERIALS
20190077921 · 2019-03-14 ·

This disclosure enables direct 3D printing of preceramic polymers, which can be converted to fully dense ceramics. Some variations provide a preceramic resin formulation comprising a molecule with two or more CX double bonds or CX triple bonds, wherein X is selected from C, S, N, or O, and wherein the molecule further comprises at least one non-carbon atom selected from Si, B, Al, Ti, Zn, P, Ge, S, N, or O; a photoinitiator; a free-radical inhibitor; and a 3D-printing resolution agent. The disclosed preceramic resin formulations can be 3D-printed using stereolithography into objects with complex shape. The polymeric objects may be directly converted to fully dense ceramics with properties that approach the theoretical maximum strength of the base materials. Low-cost structures are obtained that are lightweight, strong, and stiff, but stable in the presence of a high-temperature oxidizing environment.

Resin formulations for polymer-derived ceramic materials
10221284 · 2019-03-05 · ·

This disclosure enables direct 3D printing of preceramic polymers, which can be converted to fully dense ceramics. Some variations provide a preceramic resin formulation comprising a molecule with two or more CX double bonds or CX triple bonds, wherein X is selected from C, S, N, or O, and wherein the molecule further comprises at least one non-carbon atom selected from Si, B, Al, Ti, Zn, P, Ge, S, N, or O; a photoinitiator; a free-radical inhibitor; and a 3D-printing resolution agent. The disclosed preceramic resin formulations can be 3D-printed using stereolithography into objects with complex shape. The polymeric objects may be directly converted to fully dense ceramics with properties that approach the theoretical maximum strength of the base materials. Low-cost structures are obtained that are lightweight, strong, and stiff, but stable in the presence of a high-temperature oxidizing environment.

Method for the production of graphite bodies

The present invention relates to a method for production of graphite bodies. Carbon bodies are formed from a mixture of electric calcined coke particles calcined at a temperature between 1200 and 3000 C. and a binder where the coke particles have sulphur-and nitrogen content varying between 0 and 1.5% by weight and where the coke particles have an average sulphur content less than 0.6% by weight and a nitrogen content of less than 0.6% by weight, baking of the carbon bodies at a temperature between 700 and 1400 C. and graphitizing of the baked carbon bodies at a temperature above 2300 C.

Ferrite ceramics, ferrite sintered plate and ferrite sintered sheet

An object or technical task of the present invention is to provide a ferrite sintered sheet having a dense ferrite microfine structure which has a large value, a small value, and a small temperature-dependent change of the value thereof. The present invention relates to a ferrite ceramics having a composition comprising 47.5 to 49.8 mol % of Fe.sub.2O.sub.3, 13.5 to 19.5 mol % of NiO, 21 to 27 mol % of ZnO, 7.5 to 12.5 mol % of CuO and 0.2 to 0.8 mol % of CoO, all of the molar amounts being calculated in terms of the respective oxides, the ferrite ceramics further comprising 0.2 to 1.4% by weight of SnO.sub.2 and 0.005 to 0.03% by weight of S and having a density of 5.05 to 5.30 g/cm.sup.3; and a ferrite sintered sheet comprising the ferrite sintered plate on a surface of which a groove or grooves are formed, and an adhesive layer and/or a protective layer formed on the ferrite sintered plate.

SILICON CARBIDE/GRAPHITE COMPOSITE AND ARTICLES AND ASSEMBLIES COMPRISING SAME

A silicon carbide-graphite composite is described, including (i) interior bulk graphite material and (ii) exterior silicon carbide matrix material, wherein the interior bulk graphite material and exterior silicon carbide matrix material inter-penetrate one another at an interfacial region therebetween, and wherein graphite is present in inclusions in the exterior silicon carbide matrix material. Such material may be formed by contacting a precursor graphite article with silicon monoxide (SiO) gas under chemical reaction conditions that are effective to convert an exterior portion of the precursor graphite article to a silicon carbide matrix material in which graphite is present in inclusions therein, and wherein the silicon carbide matrix material and interior bulk graphite material interpenetrate one another at an interfacial region therebetween. Such silicon carbide-graphite composite is usefully employed in applications such as implant hard masks in manufacturing solar cells or other optical, optoelectronic, photonic, semiconductor and microelectronic products, as well as in ion implantation system materials, components, and assemblies, such as beam line assemblies, beam steering lenses, ionization chamber liners, beam stops, and ion source chambers.

Method for manufacturing high-density artificial graphite electrode

Provided is a method for manufacturing a high-density artificial graphite electrode without substantially changing a particle size or a proportion of needle coke used, increasing an amount of binder pitch, or performing extrusion molding at a high molding pressure. The method for manufacturing a high-density artificial graphite electrode is kneading binder pitch into needle coke, performing extrusion molding thereof, and then calcining and graphitizing thereof, wherein needle coke obtained by performing coke shape changing treatment for at least some of pulverized needle coke to be used, thereby increasing a ratio of an enveloping perimeter/a perimeter by 1% or more as compared with a value before the changing is used. Here, the enveloping perimeter is a length of a perimeter when apexes of convex portions of the pulverized needle coke are connected to each other via the shortest distance, and the perimeter is a length of a perimeter of a particle.

METHOD OF PRODUCING NEEDLE COKE FOR LOW CTE GRAPHITE ELECTRODES

A method of producing low CTE graphite electrodes from needle coke formed from a coal tar distillate material having a relatively high initial boiling point.

Aluminum dry-coated and heat treated cathode material precursors
09876226 · 2018-01-23 · ·

Aluminum dry-coated and heat treated cathode material precursors. A particulate precursor compound for manufacturing an aluminum coatedlithium transition metal (M)-oxide powder usable as an active positive electrode material in lithium-ion batteries includes a transition metal (M)-oxide core and a non-amorphous aluminum oxide coating layercovering the core. By providing a heat treatment process for mixed metal precursors that may be combined with an aluminum dry-coating process, novel aluminum containing precursors that may be used to form high quality nickel based cathode materials are obtained. The aluminum dry-coated and heat treated precursors include particles have, compared to prior art precursors, relatively low impurity levels of carbonate and/or sulfide, and can be produced at lower cost.

METHOD FOR SYNTHESIZING TITANIUM DIBORIDE POWDER
20240409420 · 2024-12-12 ·

A method for synthesizing a TiB.sub.2 powder includes the reduction of titanium oxide by carbon in the presence of a source of boron, the method includes heating a mixture of a carbon source, a boron carbide powder whose median particle diameter is between 5 and 100 microns and a powder of titanium oxide whose median particle diameter is between 5 and 80 microns, the mixture being placed in an enclosure under an inert gas sweep flow rate between 0.5 and 10 L/min/m/m.sup.3 of enclosure at a temperature of between 1500 C. and 2000 C., as well as the TiB.sub.2 powder obtained by such a method.

METHOD OF MANUFACTURING CERAMIC COMPOSITE WITH CONDUCTIVE OR SUPERCONDUCTING OVER ROOM TEMPERATURE AT ATMOSPHERIC (AMBIENT) PRESSURE AND THE CERAMIC COMPOSITE

The present invention discloses a method for producing room temperature and atmospheric pressure superconducting ceramic compounds and the ceramic compounds themselves.

The method for producing room temperature and atmospheric pressure superconducting ceramic compounds according to the present invention involves mixing in molar ratios according to Chemical Formula 1, heating and reacting the mixture under vacuum for out gassing, powderizing the reaction product, and conducting secondary heating for vaporization under vacuum.


Pb10-xAx(B(O1-yCy)4)6Dz<Chemical Formula 1> A: Cu, Ag, Sn, or combinations thereof, B: P, S, or combinations thereof C: S and O D: S, O, e-, or combinations thereof (x ranges from 0.1 to 7.0, y ranges from 0.001 to 10.0, z ranges from 1 to 4)

Thereby, the effect of exhibiting superconducting properties at room temperature and atmospheric pressure is achieved.