C04B2235/77

METHOD FOR PRODUCING METAL NITRIDE
20220411267 · 2022-12-29 · ·

The present invention relates to a method for producing a metal nitride by igniting a raw material powder containing a metal powder filled in a reaction vessel under a nitrogen atmosphere and propagating nitriding combustion heat generated by a nitriding reaction of the metal to the whole raw material powder, the method including forming a heat insulating layer made of a material having nitrogen permeability and inert to the nitriding reaction on an upper surface of a layer made of the raw material powder. According to the present invention, it is possible to provide a method for reducing the amount of unreacted metal powder when producing a metal nitride by a combustion synthesis method.

Zirconia composition, pre-sintered body and sintered body, and method of producing the same
11535564 · 2022-12-27 · ·

A composition comprises a zirconia powder, in which 55% or more thereof is monoclinic, and a stabilizer capable of suppressing phase transition of zirconia. An average particle diameter of zirconia particles and particles of the stabilizer is 0.06 μm to 0.17 μm. At least a portion of the stabilizer does not form a solid solution with zirconia.

Black sintered body and method for producing the same

A sintered body includes a solid solution containing cobalt and iron, with the balance being zirconia. The total content of cobalt in terms of CoO and iron in terms of Fe.sub.2O.sub.3 is more than 0.1 wt % and less than 3.0 wt %, and the proportion of cobalt regions larger than 5.5 μm.sup.2 in an elemental map obtained using an electron probe microanalyzer is 25% or less.

Process for Treating a Porous Dental Zirconia Block with Coloring Solutions
20220402830 · 2022-12-22 ·

Process for treating a porous dental zirconia block with a coloring solution, the process comprising the steps of providing a porous dental zirconia block having two opposing surfaces, surface U and surface L, treating the upper surface U of the porous dental zirconia block with a coloring solution A.sub.1, wherein the coloring solution is provided with a volume VA.sub.1, turning the porous dental zirconia block around, treating the lower surface L with a coloring solution A.sub.2 which is provided with a volume VA.sub.2. wherein the coloring solutions A.sub.1 and A.sub.2 comprise a solvent and coloring ions, wherein the volume of at least one of the coloring solutions A.sub.1 or A.sub.2 is applied in portions, wherein the following condition is met: Vo=ΣV.sub.AX, with x≥2, with Vo being the overall amount of coloring solution used to infiltrate the porous dental zirconia block.

Ceramic

The present invention relates to a ceramic, to a process for preparing the ceramic and to the use of the ceramic as a dielectric in a capacitor.

MOLYBDENUM OXYCHLORIDE WITH IMPROVED BULK DENSITY

Molybdenum oxychloride consolidated masses, comprising molybdenum oxychloride and less than 10 wt % binder. The consolidated masses have a bulk density greater than 0.85 g/cc.

METHOD FOR MANUFACTURING SILICON NITRIDE SINTERED COMPACT
20220402826 · 2022-12-22 · ·

The present invention is directed to a method for producing a silicon nitride sintered material, the method including heating a molded article, which contains a silicon nitride powder having a β phase ratio of 80% or more, a dissolved oxygen content of 0.2% by mass or less, and a specific surface area of 5 to 20 m.sup.2/g, and a sintering auxiliary containing a compound having no oxygen bond, and which has an overall oxygen content controlled to be 1 to 15% by mass and an aluminum element overall content controlled to be 800 ppm or less, to a temperature of 1,200 to 1,800° C. in an inert gas atmosphere under a pressure of 0 MPa.Math.G or more and less than 0.1 MPa.Math.G to sinter the silicon nitride.

In the present invention, there can be provided a method for producing a silicon nitride sintered material, which method is advantageous in that a silicon nitride sintered material having high thermal conductivity can be obtained even when using a silicon nitride powder having a high β phase ratio and conducting calcination under normal pressure or substantially normal pressure.

METHOD FOR PRODUCING TOUGHENED ZIRCONIA MATERIALS FOR PROSTHESES

A disclosure is provided for methods to prepare high-strength and high-toughness partially stabilized zirconia (PSZ) materials by incorporating a starting ceramic powder in which the stabilizing oxide agent is pre-alloyed with the zirconia material powder. The ceramic powder is pre-stabilized so there is little or no remaining free stabilizing oxide, thereby resulting in an improved material that is more convenient to process using conventional ceramic processing techniques.

Shaped abrasive particles, methods of making, and abrasive articles including the same

A method of making abrasive particles includes: providing a slurry comprising non-colloidal solid particles and a liquid vehicle; forming at least a portion of the slurry into shaped bodies contacting a substrate; at least partially drying the shaped bodies to provide shaped abrasive precursor particles; separating at least a portion of the shaped abrasive precursor particles from the substrate; and converting at least a portion of the shaped abrasive precursor particles into shaped abrasive particles. The shaped abrasive particles comprise alpha alumina having an average crystal grain size of 0.8 to 8 microns and an apparent density that is at least 92 percent of the true density. Each shaped abrasive particle has a respective surface comprising a plurality of smooth sides that form at least four vertexes. Shaped abrasive particles, abrasive articles including them, and methods of using are also disclosed.

Fully ceramic microencapsulated fuels containing tristructural-isotropic particles with a coating layer having higher shrinkage than matrix

The present invention relates to a method for preparing a fully ceramic capsulated nuclear fuel material containing three-layer-structured isotropic nuclear fuel particles coated with a ceramic having a composition which has a higher shrinkage than a matrix in order to prevent cracking of ceramic nuclear fuel, wherein the three-layer-structured nuclear fuel particles before coating is included in the range of between 5 and 40 fractions by volume based on after sintering. More specifically, the present invention provides a composition for preparing a fully ceramic capsulated nuclear fuel containing three-layer-structured isotropic particles coated with the substance which includes, as a main ingredient, a silicon carbine derived from a precursor of the silicon carbide wherein a condition of ΔL.sub.c>ΔL.sub.m at normal pressure sintering is created, where the sintering shrinkage of the coating layer of the three-layer-structured isotropic nuclear fuel particles is ΔL.sub.c and the sintering shrinkage of the silicon carbide matrix is ΔL.sub.m; material produced therefrom; and a method for manufacturing the material. The residual porosity of the fully ceramic capsulated nuclear fuel material is 4% or less.