Patent classifications
C07C37/74
SEPARATION OF CANNABINOIDS FROM CANNABINOID MIXTURES BY DERIVATIZATION
The present disclosure relates to isolating one or more cannabinoids from an input mixture. There is disclosed an apparatus that comprises a first reaction vessel, a volatizing unit, and a distillation unit. The first reaction vessel provides a derivatized input mixture that comprises one or more derivatized cannabinoids. The volatizing unit volatilizes the derivatized input mixture into a derivatized cannabinoid-containing vapor-stream and a residue. The distillation unit receives the derivatized cannabinoid-containing vapor stream and separates a first derivatized cannabinoid within the derivatized cannabinoid-containing vapor stream from at least a second cannabinoid. There is also a method that comprises the steps of derivatizing one or more cannabinoids in an input mixture; volatilizing the derivatized input mixture to provided a derivatized cannabinoid-containing vapor stream; conducting the derivatized cannabinoid-containing vapor stream to distillation unit; and collecting a product that comprises the first derivatized cannabinoid.
SEPARATION OF CANNABINOIDS FROM CANNABINOID MIXTURES BY DERIVATIZATION
The present disclosure relates to isolating one or more cannabinoids from an input mixture. There is disclosed an apparatus that comprises a first reaction vessel, a volatizing unit, and a distillation unit. The first reaction vessel provides a derivatized input mixture that comprises one or more derivatized cannabinoids. The volatizing unit volatilizes the derivatized input mixture into a derivatized cannabinoid-containing vapor-stream and a residue. The distillation unit receives the derivatized cannabinoid-containing vapor stream and separates a first derivatized cannabinoid within the derivatized cannabinoid-containing vapor stream from at least a second cannabinoid. There is also a method that comprises the steps of derivatizing one or more cannabinoids in an input mixture; volatilizing the derivatized input mixture to provided a derivatized cannabinoid-containing vapor stream; conducting the derivatized cannabinoid-containing vapor stream to distillation unit; and collecting a product that comprises the first derivatized cannabinoid.
Method and apparatus for decomposing phenolic by-product
The present disclosure relates to a method and an apparatus for decomposing a phenolic by-product generated in a bisphenol A preparation process, the method including: a step (S10) of feeding the phenolic by-product to a multistage reactive distillation column; a step (S20) of separating the phenolic by-product into an upper discharge stream containing an active component, a side discharge stream containing acetophenone, and a bottom discharge stream containing tar by the multistage reactive distillation column; and a step (S30) of mixing the side discharge stream discharged from the multistage reactive distillation column and the bottom discharge stream discharged from the multistage reactive distillation column to form a mixed discharge stream.
Method and apparatus for decomposing phenolic by-product
The present disclosure relates to a method and an apparatus for decomposing a phenolic by-product generated in a bisphenol A preparation process, the method including: a step (S10) of feeding the phenolic by-product to a multistage reactive distillation column; a step (S20) of separating the phenolic by-product into an upper discharge stream containing an active component, a side discharge stream containing acetophenone, and a bottom discharge stream containing tar by the multistage reactive distillation column; and a step (S30) of mixing the side discharge stream discharged from the multistage reactive distillation column and the bottom discharge stream discharged from the multistage reactive distillation column to form a mixed discharge stream.
CONTINUOUS VACUUM FRACTIONATION SYSTEM FOR SEPARATION OF VARIABLE CANNABIS EXTRACTS
A continuous vacuum fractionation system for separation of one or more of the plurality of components present in a raw cannabis extract into at least an overhead fraction, a bottoms fraction, and a side stream fraction, wherein the raw cannabis extract may be prepared by any of a variety of extraction techniques. The system includes an extract supply assembly having a primary feed pump, and one or more continuous fractionation units each including a modular fractionation column. Each column has a re-boiler, a close-coupled overhead condenser, and at least one modular fractionation stage, and further, the columns are operable in either series or parallel configurations. The close-coupled overhead condenser has an oversized impingement plate overlying a condenser inlet to minimize non-vapor components from entering and contacting the condenser. A vacuum assembly is provided to maintain at least the modular fractionation columns under a predetermined vacuum during operation.
CONTINUOUS VACUUM FRACTIONATION SYSTEM FOR SEPARATION OF VARIABLE CANNABIS EXTRACTS
A continuous vacuum fractionation system for separation of one or more of the plurality of components present in a raw cannabis extract into at least an overhead fraction, a bottoms fraction, and a side stream fraction, wherein the raw cannabis extract may be prepared by any of a variety of extraction techniques. The system includes an extract supply assembly having a primary feed pump, and one or more continuous fractionation units each including a modular fractionation column. Each column has a re-boiler, a close-coupled overhead condenser, and at least one modular fractionation stage, and further, the columns are operable in either series or parallel configurations. The close-coupled overhead condenser has an oversized impingement plate overlying a condenser inlet to minimize non-vapor components from entering and contacting the condenser. A vacuum assembly is provided to maintain at least the modular fractionation columns under a predetermined vacuum during operation.
PROCESS FOR GENERATING HEMP OIL WITH A HIGH CANNABIDIOL (CBD) CONTENT
A method for producing hemp oil, comprising decarboxylation of CBDA in hemp oil; short-path evaporation of CBD from the decarboxylated hemp oil to produce CBD oil; selective THC to CBN conversion performed on the decarboxylated hemp oil.
PROCESS FOR GENERATING HEMP OIL WITH A HIGH CANNABIDIOL (CBD) CONTENT
A method for producing hemp oil, comprising decarboxylation of CBDA in hemp oil; short-path evaporation of CBD from the decarboxylated hemp oil to produce CBD oil; selective THC to CBN conversion performed on the decarboxylated hemp oil.
METHOD FOR PRODUCING A HYDROXY COMPOUND BY DECARBOXYLATION IN THE ABSENCE OF A CATALYST
The invention relates to a method for producing a specific hydroxyl compound by decarboxylating a specific carboxylic acid compound or a salt of said carboxylic acid compound in the absence of a catalyst and to a method for producing a bisphenol.
METHOD FOR PRODUCING A HYDROXY COMPOUND BY DECARBOXYLATION IN THE ABSENCE OF A CATALYST
The invention relates to a method for producing a specific hydroxyl compound by decarboxylating a specific carboxylic acid compound or a salt of said carboxylic acid compound in the absence of a catalyst and to a method for producing a bisphenol.