Patent classifications
C07C69/88
ALKOXYLATED HYDROXYBENZOIC ACID ESTERS OR AMIDES
Alkoxylates according to the following formula (I)
##STR00001##
are described, wherein X is selected from ethoxy and mixtures of ethoxy and propoxy groups, T is selected from the group consisting of H, C.sub.1-C.sub.4 alkyl, SO.sub.3.sup.−, CH.sub.2—COO.sup.−, sulfosuccinate and PO.sub.3.sup.2−, R1, R2 and R4 are H, CO—NR8R3 or COO—[X.sub.1].sub.v—R3, whereby two of the substituents R1, R2 and R4 are H and the third of these substituents is CO—NR8R3 or COO—[X.sub.1].sub.v—R3, R8 is H or a linear or branched alkyl group with 1 to 4 C-atoms, R3 is a linear or branched saturated alkyl group with 6 to 30 carbon atoms, a linear or branched mono- or polyunsaturated alkenyl group with 6 to 30 carbon atoms, an aryl group with 6 to 10 carbon atoms, a group (CH.sub.2CH.sub.2O).sub.maryl, wherein the aryl group comprises 6 to 10 carbon atoms and m, on a molar average, is a number from 1 to 100, or an aryl-substituted linear or branched C.sub.1-C.sub.3 alkyl group wherein the aryl group comprises 6 to 10 carbon atoms, but in the case, that R1 and R4 are H and R2 is COOR3, R3 can only be an alkyl group, an alkenyl group or a group (CH.sub.2CH.sub.2O).sub.maryl as defined above, X.sub.1 is selected from ethoxy and mixtures of ethoxy and propoxy groups, u on a molar average, is a number of from 3 to 100, and v on a molar average, is a number of from 0 to 20.
The compounds of formula (I) may advantageously be used as anti-redeposition agents in laundry applications.
ALKOXYLATED HYDROXYBENZOIC ACID ESTERS OR AMIDES
Alkoxylates according to the following formula (I)
##STR00001##
are described, wherein X is selected from ethoxy and mixtures of ethoxy and propoxy groups, T is selected from the group consisting of H, C.sub.1-C.sub.4 alkyl, SO.sub.3.sup.−, CH.sub.2—COO.sup.−, sulfosuccinate and PO.sub.3.sup.2−, R1, R2 and R4 are H, CO—NR8R3 or COO—[X.sub.1].sub.v—R3, whereby two of the substituents R1, R2 and R4 are H and the third of these substituents is CO—NR8R3 or COO—[X.sub.1].sub.v—R3, R8 is H or a linear or branched alkyl group with 1 to 4 C-atoms, R3 is a linear or branched saturated alkyl group with 6 to 30 carbon atoms, a linear or branched mono- or polyunsaturated alkenyl group with 6 to 30 carbon atoms, an aryl group with 6 to 10 carbon atoms, a group (CH.sub.2CH.sub.2O).sub.maryl, wherein the aryl group comprises 6 to 10 carbon atoms and m, on a molar average, is a number from 1 to 100, or an aryl-substituted linear or branched C.sub.1-C.sub.3 alkyl group wherein the aryl group comprises 6 to 10 carbon atoms, but in the case, that R1 and R4 are H and R2 is COOR3, R3 can only be an alkyl group, an alkenyl group or a group (CH.sub.2CH.sub.2O).sub.maryl as defined above, X.sub.1 is selected from ethoxy and mixtures of ethoxy and propoxy groups, u on a molar average, is a number of from 3 to 100, and v on a molar average, is a number of from 0 to 20.
The compounds of formula (I) may advantageously be used as anti-redeposition agents in laundry applications.
METHOD FOR PREPARING CELLULOSE DOPE
The invention relates to a method for preparing a cellulose dope comprising mixing and dissolving the cellulosic raw material in dilute and concentrated aqueous organic solvent in a two-stage process to form a homogeneous slurry, followed by heating the homogeneous slurry to obtain a cellulose dope containing 11% to 20% cellulose by weight. The invention also relates to a cellulose dope comprising 11% to 20% cellulose by weight and 73% to 79% aqueous organic solvent wherein the concentration of the cellulosic and metallic impurities in the cellulose dope shows a percent reduction of 20% to 50% from the cellulosic raw material.
METHOD FOR PREPARING CELLULOSE DOPE
The invention relates to a method for preparing a cellulose dope comprising mixing and dissolving the cellulosic raw material in dilute and concentrated aqueous organic solvent in a two-stage process to form a homogeneous slurry, followed by heating the homogeneous slurry to obtain a cellulose dope containing 11% to 20% cellulose by weight. The invention also relates to a cellulose dope comprising 11% to 20% cellulose by weight and 73% to 79% aqueous organic solvent wherein the concentration of the cellulosic and metallic impurities in the cellulose dope shows a percent reduction of 20% to 50% from the cellulosic raw material.
Composition, method and use
A quaternary ammonium salt of formula (I): wherein X is a linking group; Y is O, NH or NR.sup.1 wherein R.sup.1 is H or an optionally substituted hydrocarbyl group; Q.sup.+ is a moiety that includes a quaternary ammonium cation; A.sup.− is an anion; R.sup.2 is an optionally substituted alkylene group; R.sup.3 is hydrogen or an optionally substituted hydrocarbyl group; and n is 0 or a positive integer; provided that n is not 0 when R.sup.3 is hydrogen. ##STR00001##
SOLID FORMS COMPRISING 4-AMINO-2-(2,6-DIOXOPIPERIDINE-3-YL)ISOINDOLINE-1,3-DIONE AND A COFORMER, COMPOSITIONS AND METHODS OF USE THEREOF
Provided herein are solid forms comprising (a) 4-amino-2-(2,6-dioxopiperidine-3-yl)isoindoline-1,3-dione and (b) a coformer. Pharmaceutical compositions comprising the solid forms (e.g., cocrystals) and methods for treating, preventing and managing various disorders are also disclosed.
SOLID FORMS COMPRISING 4-AMINO-2-(2,6-DIOXOPIPERIDINE-3-YL)ISOINDOLINE-1,3-DIONE AND A COFORMER, COMPOSITIONS AND METHODS OF USE THEREOF
Provided herein are solid forms comprising (a) 4-amino-2-(2,6-dioxopiperidine-3-yl)isoindoline-1,3-dione and (b) a coformer. Pharmaceutical compositions comprising the solid forms (e.g., cocrystals) and methods for treating, preventing and managing various disorders are also disclosed.
Method for preparing cellulose dope
The invention relates to a method for preparing a cellulose dope comprising mixing and dissolving the cellulosic raw material in dilute and concentrated aqueous organic solvent in a two-stage process to form a homogeneous slurry, followed by heating the homogeneous slurry to obtain a cellulose dope containing 11% to 20% cellulose by weight. The invention also relates to a cellulose dope comprising 11% to 20% cellulose by weight and 73% to 79% aqueous organic solvent wherein the concentration of the cellulosic and metallic impurities in the cellulose dope shows a percent reduction of 20% to 50% from the cellulosic raw material.
Method for preparing cellulose dope
The invention relates to a method for preparing a cellulose dope comprising mixing and dissolving the cellulosic raw material in dilute and concentrated aqueous organic solvent in a two-stage process to form a homogeneous slurry, followed by heating the homogeneous slurry to obtain a cellulose dope containing 11% to 20% cellulose by weight. The invention also relates to a cellulose dope comprising 11% to 20% cellulose by weight and 73% to 79% aqueous organic solvent wherein the concentration of the cellulosic and metallic impurities in the cellulose dope shows a percent reduction of 20% to 50% from the cellulosic raw material.
Solid forms comprising 4-amino-2-(2,6- dioxopiperidine-3-yl)isoindoline-1,3-dione and a coformer, compositions and methods of use thereof
Provided herein are solid forms comprising (a) 4-amino-2-(2,6-dioxopiperidine-3-yl)isoindoline-1,3-dione and (b) a coformer. Pharmaceutical compositions comprising the solid forms (e.g., cocrystals) and methods for treating, preventing and managing various disorders are also disclosed.