The present invention is directed to the use as a reactive component in the curing of compositions based on epoxy resins of a functionalized α-angelica lactone (XOMAL) having the general formula:

##STR00001##

wherein: R.sup.a is a C.sub.1-C.sub.30 alkyl, C.sub.3-C.sub.30 cycloalkyl, C.sub.6-C.sub.18 aryl or C.sub.2-C.sub.12 alkenyl group.

A preparation method of a crosslinking-type aqueous binder for lithium-ion batteries. An organic carboxylic group-, amino group- or hydroxyl group-containing hydrophilic polymer, and a hydroxyl group-, amine group- or carboxyl group-containing water-soluble small-molecule crosslinker, both serve as starting materials of the aqueous binder, and can be crosslinked by esterification or amidation under coating and drying conditions of lithium-ion battery electrode slurry. The preparation method of the crosslinking-type aqueous binder is simple, without the need of modifying the current process or conditions for lithium-ion battery manufacture. The obtained electrodes have excellent binding capacity, flexibility, and elasticity.

This invention relates to odor control molecules comprised of polyethyleneimine compounds containing N-halamine and derivatives thereof.

Described herein is a process for manufacturing ethoxylated polyethylene-imines. Also described herein are the ethoxylated polyethyleneimines and methods for using the ethoxylated polyethyleneimines.

An integrated process for manufacturing polyethyleneamine compounds selected from the group of polyethyleneamines and hydroxyethylethyleneamines is provided. The process includes in an adduction step, providing a CO.sub.2 adduct of a starting compound comprising a —NH—CH.sub.2—CH.sub.2—NH— moiety or a —NH—CH.sub.2—CH.sub.2—OH moiety, or HO—CH.sub.2—CH.sub.2—OH, in a reaction step reacting a hydroxy-functional compound selected from the group of ethanolamines and dihydroxyethane with an amine-functional compound, wherein at least part of the total of hydroxy-functional compounds and amine-functional compounds is provided in the form of a CO.sub.2 adduct, to form CO.sub.2 adduct of a product polyethyleneamine compound, in an elimination step converting CO.sub.2 adduct of product polyethyleneamine compound to the corresponding product polyethylene amine compound, wherein a fraction comprising a recycle compound comprising a —NH—CH.sub.2—CH.sub.2—NH— moiety or a —NH—CH.sub.2—CH.sub.2—OH moiety, or HO—CH.sub.2—CH.sub.2—OH, or CO.sub.2 adducts thereof, is provided from the end of the reaction step or the elimination step to the adduction step or to the reaction step, wherein the recycle compound has per molecule on average fewer of the total of —NH—CH.sub.2—CH.sub.2—NH— moieties and —NH—CH.sub.2—CH.sub.2—OH moieties than the product polyethyleneamine compound.

The invention relates to the preparation and development of a method for a process for preparing a Poly Methylamine surfactant. The process consists of a mixture of methanol and ethanolamine in a molar ratio ranging from 1.0-0.6 to 3.0-0.4 at a temperature of 45-50° C., resulting in a non-hazardous substance, without toxic effects for human health, at the same time having high-quality cleaning, high- and very low temperature resistance, with surface active agent (surfactant) properties. Used as a fuel additive, reduces harmful exhaust gas emissions to the atmosphere, raises the octane number in gasoline, prevents the formation of ice crystals in diesel fuel.

Two-dimensional (2D) polymers and methods for their formation are described herein. To create oriented 2D polymer films, monomers are combined with processing additives within a solvent, creating a solution that can be cast and dried to remove the solvent and form a solid film. The methods can enable transformation of the monomers into oriented films. Film quality can be controlled via multiple processing parameters, including monomer and additive concentrations, shear and elongational flow rates during casting, evaporation rates, and post-process rinsing, buffering, stretching, and thermal treatments. By combining stiff carbon-containing cyclic polymer nodal units with more compliant linear polymer bridge units in an ordered, 2D repeating molecular structure it is possible to tailor the mechanical properties of 2D polymers and their assemblies to provide high stiffness, strength, and toughness. The 2D polymer can also be combined with other 2D materials, linear polymers, or reinforcing materials to create 2D polymer composites.

The invention is directed to utilization of a series of cross-linked 1,4-benzenediamine-co-alkyldiamine polymers and the use of the polymers to remove mercury from a hydrocarbon in fluid form.

The invention relates to a method for producing poly(alkylene) guanidines, comprising at least the following steps: a) providing an alkylene diamine of the formula NH.sub.2(CH.sub.2)m-NH.sub.2 with m=4-12, in particular 6-10, in a reaction vessel and heating the alkylene diamine to a temperature greater than or equal to the melting temperature of the alkylene diamine in question, typically to a temperature in a range of 25 C. to 115 C., preferably 55 C. to 110 C., whereby a melt of the alkylene diamine is produced; b) adding a guanidinium salt, in particular guanidinium HCl, in portions and reacting same with the alkylene diamine until the formation of alkylene(guanidine) monomers is completed; c) reacting the monomers formed in step b), at at least the minimum temperature at which the polymerization to form the desired poly(alkylene) guanidine begins, until the formation of the poly(alkylene) guanidine is completed; wherein steps a) and b) for forming alkylene(guanidine) monomers are carried out at a temperature below the minimum polymerization temperature and the mixture is stirred during all method steps. The invention further relates to the homogeneous poly(alkylene) guanidines obtainable by means of the method described above, said poly(alkylene) guanidines having a content of at least 85 wt %, in particular at least 90% or 97%, of a desired linear poly(alkylene) guanidine having 3-14, preferably 4-10, alkylene monomer units in the molecule as a main product and a content of by-products, in particular branched isomers of said poly(alkylene) guanidine, of at most 15%, 10%, 5% or 3%.

Disclosed are methods and compositions for coagulating and clarifying produced waters for use as boiler feed waters, for example for the generation of steam. The methods and compositions are especially useful for treatment of produced waters from steam-injection methods of tertiary oil recovery such as steam-assisted gravitational drainage. Disclosed are compositions comprising a first copolymer having a high molecular weight and bearing a low molar cationic charge and a second copolymer having a lower molecular weight and bearing a high molar cationic charge. The compositions are suitable for addition as coagulants to produced waters that have been treated by warm lime softening. Also disclosed are methods of treating produced waters from steam-injection oil recovery for use as boiler feed waters to generate steam in such steam injection methods.