C22B3/10

Rare earth metal oxide process including extracting rare earth metal from acidic solution with an ionic liquid composition

A method for extracting a rare earth metal from a mixture of one or more rare earth metals, said method comprising contacting an acidic solution of the rare earth metal with a composition which comprises an ionic liquid to form an aqueous phase and a non-aqueous phase into which the rare earth metal has been selectively extracted; recovering the rare earth metal from the non-aqueous phase; and processing the recovered rare earth metal into a rare earth metal oxide.

Processing of lithium containing material including HCl sparge
11286170 · 2022-03-29 · ·

A process (10) for the treatment of a lithium containing material (12), the process comprising the steps of: (i) Preparing a process solution from the lithium containing material (12); (ii) Passing the process solution from step (i) to a series of impurity removal steps, one of which is an HCl sparging step 58, thereby providing a substantially purified lithium chloride solution; and (iii) Passing the purified lithium chloride solution of step (ii) to an electrolysis step (70) thereby producing a lithium hydroxide solution. An additional step in which the lithium hydroxide solution produced in step (iii) is carbonated by passing compressed carbon dioxide (88) through the solution, thereby producing a lithium carbonate precipitate, is also disclosed.

Processing of lithium containing material including HCl sparge
11286170 · 2022-03-29 · ·

A process (10) for the treatment of a lithium containing material (12), the process comprising the steps of: (i) Preparing a process solution from the lithium containing material (12); (ii) Passing the process solution from step (i) to a series of impurity removal steps, one of which is an HCl sparging step 58, thereby providing a substantially purified lithium chloride solution; and (iii) Passing the purified lithium chloride solution of step (ii) to an electrolysis step (70) thereby producing a lithium hydroxide solution. An additional step in which the lithium hydroxide solution produced in step (iii) is carbonated by passing compressed carbon dioxide (88) through the solution, thereby producing a lithium carbonate precipitate, is also disclosed.

Method for recovering a minor metal and/or rare-earth metal

An object of the present invention is to recover a minor metal and/or rare-earth metal. The present invention provides a method for recovering a minor metal and/or rare-earth metal from a post-chlorination residue in titanium smelting. The minor metal and/or rare-earth metal is one or more metal selected from the group consisting of Sc, V, Nb, Zr, Y, La, Ce, Pr, and Nd.

Method for extracting rare earth elements from rare earth element hyperaccumulator

A method for extracting rare earth elements (REEs) from a REE hyperaccumulator, including: subjecting the REE hyperaccumulator to microwave-assisted digestion to obtain a REE extract; subjecting the REE extract to absorption with a chelating resin and elution to obtain a purified REE solution; and subjecting the purified REE solution to precipitation and calcination to obtain high-purity rare earth compound.

Method for extracting rare earth elements from rare earth element hyperaccumulator

A method for extracting rare earth elements (REEs) from a REE hyperaccumulator, including: subjecting the REE hyperaccumulator to microwave-assisted digestion to obtain a REE extract; subjecting the REE extract to absorption with a chelating resin and elution to obtain a purified REE solution; and subjecting the purified REE solution to precipitation and calcination to obtain high-purity rare earth compound.

PROCESS FOR METALLURGY AND SEPARATING RARE EARTH CONCENTRATE USING COMBINATION METHOD

The present invention provides a process for metallurgy and separating a rare earth concentrate using a combination method, the process including: treating the rare earth concentrate containing bastnaesite by using a method including roasting under an atmosphere, leaching with hydrochloric acids, and roasting with a sulfuric acid, wherein stepping acid leaching with low-concentration hydrochloric acids is controlled during the leaching with the hydrochloric acids so as to obtain a rare earth solution with a high concentration (150-250 g/L REO), such that a leaching rate of Ce reaches 60% or more, and the content of F.sup.− in a leaching liquor is reduced by aging; and rare earth is further recovered from a leach residue by roasting with the sulfuric acid and leaching with water, and the total yield of the rare earth reaches 95% or more.

PROCESS FOR METALLURGY AND SEPARATING RARE EARTH CONCENTRATE USING COMBINATION METHOD

The present invention provides a process for metallurgy and separating a rare earth concentrate using a combination method, the process including: treating the rare earth concentrate containing bastnaesite by using a method including roasting under an atmosphere, leaching with hydrochloric acids, and roasting with a sulfuric acid, wherein stepping acid leaching with low-concentration hydrochloric acids is controlled during the leaching with the hydrochloric acids so as to obtain a rare earth solution with a high concentration (150-250 g/L REO), such that a leaching rate of Ce reaches 60% or more, and the content of F.sup.− in a leaching liquor is reduced by aging; and rare earth is further recovered from a leach residue by roasting with the sulfuric acid and leaching with water, and the total yield of the rare earth reaches 95% or more.

METHOD FOR PRODUCING LITHIUM CHLORIDE, AND LITHIUM CARBONATE

The present invention is related to a method for producing lithium chloride aqueous solution and a method for producing lithium carbonate, and comprises introducing calcium chloride into a slurry containing a solvent and lithium phosphate; and obtaining a precipitate of chloroapatite which is an poorly soluble phosphoric acid compound and a lithium chloride aqueous solution by reacting lithium phosphate and calcium chloride in the slurry containing the solvent and lithium phosphate.

METHOD FOR PRODUCING LITHIUM CHLORIDE, AND LITHIUM CARBONATE

The present invention is related to a method for producing lithium chloride aqueous solution and a method for producing lithium carbonate, and comprises introducing calcium chloride into a slurry containing a solvent and lithium phosphate; and obtaining a precipitate of chloroapatite which is an poorly soluble phosphoric acid compound and a lithium chloride aqueous solution by reacting lithium phosphate and calcium chloride in the slurry containing the solvent and lithium phosphate.