C22B3/30

Processing method for lithium ion battery scrap

A method for processing lithium ion battery scrap includes a leaching step of leaching lithium ion battery scrap and subjecting the resulting leached solution to solid-liquid separation to obtain a first separated solution; an iron removal step of adding an oxidizing agent to the first separated solution and adjusting a pH of the first separated solution in a range of from 3.0 to 4.0, then performing solid-liquid separation and removing iron in the first separated solution to obtain a second separated solution; and an aluminum removal step of neutralizing the second separated solution to a pH range of from 4.0 to 6.0, then performing solid-liquid separation and removing aluminum in the second separated solution to obtain a third separated solution.

Processing method for lithium ion battery scrap

A method for processing lithium ion battery scrap according to this invention includes a leaching step of leaching lithium ion battery scrap to obtain a leached solution; an aluminum removal step of neutralizing the leached solution to a pH range of from 4.0 to 6.0, then performing solid-liquid separation and removing aluminum in the leached solution to obtain a first separated solution; and an iron removal step of adding an oxidizing agent to the first separated solution and adjusting the pH in a range of from 3.0 to 5.0, then performing solid-liquid separation and removing iron in the first separated solution to obtain a second separated solution.

Processing method for lithium ion battery scrap

A method for processing lithium ion battery scrap according to this invention includes a leaching step of leaching lithium ion battery scrap to obtain a leached solution; an aluminum removal step of neutralizing the leached solution to a pH range of from 4.0 to 6.0, then performing solid-liquid separation and removing aluminum in the leached solution to obtain a first separated solution; and an iron removal step of adding an oxidizing agent to the first separated solution and adjusting the pH in a range of from 3.0 to 5.0, then performing solid-liquid separation and removing iron in the first separated solution to obtain a second separated solution.

RECOVERY METHOD FOR COPPER-INDIUM-GALLIUM-SELENIUM MATERIAL

Provided is a recovery method for a copper-indium-gallium-selenium material, mainly comprising the steps of sulfuric acid aeration leaching at a high temperature, reducing selenium with sodium sulfite, separating copper by extracting, separating indium and gallium with an alkali, replacing indium, electrolyzing gallium, etc. In the recovery method for a copper-indium-gallium-selenium material, a sulfuric acid aeration leaching means is used, thus reducing acid gas pollution; at the same time, an extraction agent for copper is used to extract copper, wherein the separating effect is good and the cost is low, and the extracted copper is directly electrolyzed so as to obtain a high-purity metal copper; moreover, an alkali is used to separate gallium, wherein realizing the separation of indium and gallium only requires the adjustment of the pH value of a solution, the separating effect is good and the obtained indium and gallium products have a relatively high purity.

METHOD FOR RECYCLING COPPER INDIUM GALLIUM SELENIUM MATERIALS

A method for recycling copper indium gallium selenium materials comprises the steps of sulphating roasting, acid dissolution, extraction and electrolysis of metal copper, production of a gallium hydroxide deposition, replacement of indium, and the like. In the method, deselenization is carried by using sulphating roasting, and residues after roasting are oxidizing slags capable of being directly subjected to acid dissolution, thereby reducing acid gas pollution; in addition, copper is extracted by using a copper extractant, the separation effect is good and costs are low, the extracted copper can be directly electrolyzed, so as to obtain high-purity metal copper; and in another aspect, in the method, alkali separation of gallium is carried out, separation between indium and gallium can be implemented by merely adjusting the pH of a solution, thereby resolving the problem of co-extraction in the extraction of indium and gallium and the separation between indium and gallium, the separation effect is good, the purities of obtained indium and gallium products are high.

A Method of Pretreatment and Bromine Recovery of PCB Incineration Ash
20200262712 · 2020-08-20 ·

A method of pretreatment and bromine recovery of PCB Incineration ash is disclosed that relates to the field of comprehensive recovery of valuable metals by full wet method, especially relates to a method of valuable metals and bromine recovery, precious metals enrichment in pretreatment process of PCB Incineration ash. The major steps includes alkali leaching, Cu extraction back-extraction, neutralization-precipitation to separate, Bromine evaporative crystallization, regeneration, acid pickling, Zn evaporative crystallization, removal of Zn and Cu. Compared with the traditional comprehensive recovery process of ash, the invention can separate bromine from ash and recover valuable metals such as copper, zinc and lead with the maximum extent, at the same time, the enrichment of silver and other precious metals is beneficial to the subsequent recovery of precious metals. It has high added recovery value and no tailless discharge.

Renewable isoparaffins as diluent in hydrometallurgical liquid-liquid extraction process

The present disclosure relates to hydrometallurgical technologies wherein liquid-liquid extraction, also called solvent extraction, is used to separate and concentrate metal ions. Exemplary embodiments relate to solvent extraction of copper and a diluent useful in copper solvent extraction. A bio-based composition can fulfil physico-chemical properties that are desired for solvent extraction. Moreover, a composition is disclosed, which in addition to providing more environmental friendly alternative, can also improve the solvent extraction process of copper.

Renewable isoparaffins as diluent in hydrometallurgical liquid-liquid extraction process

The present disclosure relates to hydrometallurgical technologies wherein liquid-liquid extraction, also called solvent extraction, is used to separate and concentrate metal ions. Exemplary embodiments relate to solvent extraction of copper and a diluent useful in copper solvent extraction. A bio-based composition can fulfil physico-chemical properties that are desired for solvent extraction. Moreover, a composition is disclosed, which in addition to providing more environmental friendly alternative, can also improve the solvent extraction process of copper.

Treatment of degraded oxime metal extractants in process organic solutions
10662499 · 2020-05-26 · ·

The invention relates to a method for regenerating the extractive potential of an organic hydroxyoxime-based extraction solution used in the recovery of metals by liquid-liquid extraction. The method is two-stage, in which a solid hydroxylamine is used in the reaction stage, and the removal of the undesirable compounds generated in the reaction occurs in the second stage by adsorption purification. The method of the invention is suitable for treatment of degraded oxime metal extractants in various process organic solutions both in aldehyde and ketoxime extractant solutions. The method can also be used to treat a mixture of degraded oxime extractants.

Treatment of degraded oxime metal extractants in process organic solutions
10662499 · 2020-05-26 · ·

The invention relates to a method for regenerating the extractive potential of an organic hydroxyoxime-based extraction solution used in the recovery of metals by liquid-liquid extraction. The method is two-stage, in which a solid hydroxylamine is used in the reaction stage, and the removal of the undesirable compounds generated in the reaction occurs in the second stage by adsorption purification. The method of the invention is suitable for treatment of degraded oxime metal extractants in various process organic solutions both in aldehyde and ketoxime extractant solutions. The method can also be used to treat a mixture of degraded oxime extractants.