A method for producing a metal ingot by using an electron-beam melting furnace including an electron gun and a hearth that accumulates a molten metal of a metal raw material, in which, in a downstream region between an upstream region in which the metal raw material is supplied onto the surface of the molten metal and a first side wall, an irradiation line is disposed so as to block a lip portion and so that two end portions are positioned in the vicinity of the side wall of the hearth. A first electron beam is radiated onto the surface of the molten metal along the irradiation line, such that the surface temperature (T2) of the molten metal along the irradiation line is made higher than the average surface temperature (T0) of the entire surface of the molten metal in the hearth.

A metal titanium production apparatus includes: a reductor that subjects titanium tetrachloride to a reduction process in presence of bismuth and magnesium to obtain a liquid alloy containing titanium and the bismuth; a segregator that subjects the liquid alloy to a segregation process to obtain a precipitate; and a distillator that subjects the precipitate to a distillation process to obtain metal titanium, and the distillator sets an atmosphere so as to preferentially vaporize the bismuth attached to the precipitate and then sets the atmosphere so as to vaporize the bismuth forming the precipitate.

Provided is a method for preparing a reduced titanium powder by a multistage deep reduction, including the following steps of: uniformly mixing a dried titanium dioxide powder with a magnesium powder to obtain a mixture, adding the mixture in a self-propagating reaction furnace, triggering a self-propagating reaction, obtaining an intermediate product of which low-valence titanium oxides Ti.sub.xO are dispersed in an MgO matrix, leaching the intermediate product with a hydrochloric acid as a leaching solution, performing filtering, washing and vacuum drying to obtain a low-valence titanium oxide Ti.sub.xO precursor, uniformly mixing the low-valence titanium oxide Ti.sub.xO precursor with a calcium powder, performing a pressing to obtain semi-finished products, placing the semi-finished products in a vacuum reduction furnace for a second-time deep reduction, and leaching a deep reduction product with a hydrochloric acid as a leaching solution so as to obtain the reduced titanium powder.

A cold crucible structure according to an embodiment of the present invention includes a cold crucible structure according to an embodiment of the present invention includes: a cold crucible unit including hollow top and bottom caps, a plurality of segments connecting the top cap and the bottom cap, slits disposed between the segments, and a reaction area surrounded by the segments; and an induction coil unit disposed to cover the outer side of the cold crucible unit and disposed across the longitudinal directions of the segments and the slits, in which the diameter of the reaction area is defined as a crucible diameter, the crucible diameter is 100 to 300 mm, and a width of each of the slits is defined by $d_{\mathrm{slit}}\le 0.3\times \frac{\varnothing }{50}$
(mm)(where d.sub.slit is the width of each of the slits and Ø is the crucible diameter).

The invention is a microwave gun and arc plasma torch furnace used to refine titanium, Ti, from titanium dioxide, TiO.sub.2, powder. The furnace includes high frequency microwave emitters that create a high temperature zone strongly vibrating the titanium dioxide powder, TiO.sub.2, and lengthening and weakening the valence bonds in the titanium dioxide powder, TiO.sub.2, titanium, Ti, and oxygen, O, atoms. The furnace also uses nitrogen arc plasma torch generators to generate a N.sup.+ plasma to completely disassociate the titanium, Ti, and oxygen, O, atoms into titanium ions, Ti.sup.+ and oxygen ions, O.sup., and permitting the formation of nitrogen dioxide, NO.sub.2, and melted titanium, Ti.

The invention relates to a method for preparing titanium alloys based on aluminothermic self-propagating gradient reduction and slag-washing refining, and belongs to the technical field of titanium-aluminum alloys. The method comprises the following steps of pre-treating raw materials, weighing the raw materials in the mass ratio of rutile or high-titanium slags or titanium dioxide to aluminum powder to V.sub.2O.sub.5 powder to CaO to KClO.sub.3 being 1.0:(0.60-0.24):(0.042-0.048):(0.12-0.26):(0.22-0.30), performing an aluminothermic self-propagating reaction in a gradient feeding manner to obtain high-temperature melt, performing a gradient reduction melting, performing heat insulation and separating the melt after the feeding is completed, then adding CaF.sub.2CaOTiO.sub.2V.sub.2O.sub.5 based refining slags into the high-temperature melt, performing slag washing refining, and finally removing slags to obtain titanium alloys. This method has the advantages including short flow, low energy consumption, easy operation, easy control on Al and V contained in alloys, and so on.

A method for refining a titanium material, in which oxygen contained in a titanium material made of a pure titanium, a titanium alloy or an intermetallic compound containing titanium as one of main components is removed, the method includes: a first melting step of melting the titanium material under a noble gas atmosphere containing 5 to 70 vol % of hydrogen, thereby introducing hydrogen into a melt of the titanium material; and a second melting step of melting the titanium material into which hydrogen has been introduced in the first melting step under a noble gas atmosphere, thereby removing oxygen contained in the titanium material from the melt of the titanium material together with the hydrogen. Each of the first melting step and the second melting step is carried out at least once.

A method (500) for producing a titanium product is disclosed. The method (500) can include obtaining TiO.sub.2-slag (501) and reducing impurities in the TiO.sub.2-slag (502) to form purified TiO.sub.2 (503). The method (500) can also include reducing the purified TiO.sub.2 using a metallic reducing agent (504) to form a hydrogenated titanium product comprising TiH.sub.2 (505). The hydrogenated titanium product can be dehydrogenated (506) to form a titanium product (508). The titanium product can also be optionally deoxygenated (507) to reduce oxygen content.

A cold crucible structure according to an embodiment of the present invention includes a cold crucible structure according to an embodiment of the present invention includes: a cold crucible unit including hollow top and bottom caps, a plurality of segments connecting the top cap and the bottom cap, slits disposed between the segments, and a reaction area surrounded by the segments; and an induction coil unit disposed to cover the outer side of the cold crucible unit and disposed across the longitudinal directions of the segments and the slits, in which the diameter of the reaction area is defined as a crucible diameter, the crucible diameter is 100 to 300 mm, and gaps of the slits are defined by

[00001]$d_{\mathrm{slit}}0.3\frac{}{50}$

(mm)(where d.sub.slit is the gap between the slits and is the crucible diameter).

A method for producing a metal ingot by using an electron-beam melting furnace including an electron gun capable of controlling a radiation position of an electron beam, and a hearth that accumulates a molten metal of a metal raw material, in which, in a downstream region between an upstream region in which the metal raw material is supplied onto the surface of the molten metal and a first side wall, an irradiation line is disposed so as to block a lip portion and so that two end portions are positioned in the vicinity of the side wall of the hearth. A first electron beam is radiated onto the surface of the molten metal along the irradiation line, and the first electron beam is radiated along the irradiation line. By this means, the surface temperature (T2) of the molten metal along the irradiation line is made higher than the average surface temperature (T0) of the entire surface of the molten metal in the hearth, and a molten metal flow from the irradiation line toward upstream that is a direction toward the opposite side to the first side wall is formed in an outer layer of the molten metal.