A method for producing a chemically treated alloy material is provided that suppresses a decrease in chemical treatability even in a case where chemical treatment is repeatedly performed. The method for producing a chemically treated alloy material of the present disclosure includes a chemical treatment step and a treatment solution regeneration step. In the chemical treatment step, an alloy material (6) is immersed in an oxalate treatment solution (4) containing oxalate ions and fluorine ions to perform a chemical treatment. In the treatment solution regeneration step, light is radiated to the oxalate treatment solution (4) during the chemical treatment and/or the oxalate treatment solution (4) after the chemical treatment.

The invention relates to a method for producing a silane-modified silicate. In order to obtain optimal corrosion protection properties, a silane compound according to the invention is at least partially hydrolyzed and/or condensed in the presence of a silicate compound at a pH value greater than or equal to 8 and then a pH value less than or equal to 7 is set by adding acid. The invention further relates to an aqueous acidic passivation composition for metal substrate coated with the passivation composition.

The invention relates to a method for producing a silane-modified silicate. In order to obtain optimal corrosion protection properties, a silane compound according to the invention is at least partially hydrolyzed and/or condensed in the presence of a silicate compound at a pH value greater than or equal to 8 and then a pH value less than or equal to 7 is set by adding acid. The invention further relates to an aqueous acidic passivation composition for metal substrate coated with the passivation composition.

Provided herein is a reductive solution for preventing rouge formation on stainless steel, said solution comprising complexing anions, Fe.sup.2+, and, optionally, one or more pH modifiers. Further provided are methods for manufacturing said solution, methods for prevention of rouge formation on stainless steel surfaces, and related uses of the aforementioned reductive solution.

Provided herein is a reductive solution for preventing rouge formation on stainless steel, said solution comprising complexing anions, Fe.sup.2+, and, optionally, one or more pH modifiers. Further provided are methods for manufacturing said solution, methods for prevention of rouge formation on stainless steel surfaces, and related uses of the aforementioned reductive solution.

A method for producing a chemically treated alloy material is provided that suppresses a decrease in chemical treatability even in a case where chemical treatment is repeatedly performed. The method for producing a chemically treated alloy material of the present disclosure includes a chemical treatment step and a treatment solution regeneration step. In the chemical treatment step, an alloy material (6) is immersed in an oxalate treatment solution (4) containing oxalate ions and fluorine ions to perform a chemical treatment. In the treatment solution regeneration step, light is radiated to the oxalate treatment solution (4) during the chemical treatment and/or the oxalate treatment solution (4) after the chemical treatment.

A method for producing a chemically treated alloy material is provided that suppresses a decrease in chemical treatability even in a case where chemical treatment is repeatedly performed. The method for producing a chemically treated alloy material of the present disclosure includes a chemical treatment step and a treatment solution regeneration step. In the chemical treatment step, an alloy material (6) is immersed in an oxalate treatment solution (4) containing oxalate ions and fluorine ions to perform a chemical treatment. In the treatment solution regeneration step, light is radiated to the oxalate treatment solution (4) during the chemical treatment and/or the oxalate treatment solution (4) after the chemical treatment.

A highly reactive conversion coating chemistry is used during CAVF processing of high hardness steel alloys such as AMS 6509 and AMS 6517 steel alloys. This chemistry produces a hard, thin, black conversion coating that is not fully rubbed off by the media during the CAVF process. Distressed material regions on the surface of the alloys are not susceptible to forming the conversion coating and remain white. Visual inspection for the presence of such regions is facilitated.

A highly reactive conversion coating chemistry is used during CAVF processing of high hardness steel alloys such as AMS 6509 and AMS 6517 steel alloys. This chemistry produces a hard, thin, black conversion coating that is not fully rubbed off by the media during the CAVF process. Distressed material regions on the surface of the alloys are not susceptible to forming the conversion coating and remain white. Visual inspection for the presence of such regions is facilitated.

Methods for treatment shaped bodies are described herein. The methods generally include contacting at least one shaped body with an aqueous acidic composition to form a conversion layer on a surface of the at least one shaped body, wherein the surface includes iron or steel and a carbon content in a range of 0 to 2.06 wt. % and a chrome content in a range of 0 to <10 wt. % and wherein the surface is optionally galvanized or alloy galvanized. The aqueous acidic composition includes water; from 2 to 500 g/L oxalic acid; and from 0.01 to 20 g/L of at least one catalyst based on guanidine, nitrate or combinations thereof, wherein a pickling removal of the aqueous acidic composition is in a range of 1 to 6 g/m.sup.2.