Patent classifications
C01B33/155
Aerogel particle and method of producing the same
An aerogel particle is produced by following processes. A mixing process: an alkoxysilane compound is mixed with an organic solvent to form a first mixed solution. A hydrolysis process: an acid catalyst is added into the first mixed solution to perform a hydrolysis reaction, thereby obtaining a sol. A condensation process: an alkali catalyst is added into the sol to perform a condensation reaction, and a hydrophobic dispersion solvent is added and stirred during the condensation process, thereby subjecting sol to be gelled when it is stirred, further producing the aerogel particle with a uniform structure.
Aerogel-containing composition and insulation blanket prepared using the same
The present disclosure provides an aerogel-containing composition including an aerogel, a water-soluble binder, a foaming agent, and a mixture of water and a polar organic solvent as a solvent, and an insulation blanket prepared using the same. In the aerogel-containing composition, the aerogel is uniformly dispersed in the composition, and when preparing a blanket, an insulation blanket having low thermal conductivity and flexibility of low density is prepared without concern of shrinkage of the substrate for a blanket and detachment of the aerogel during a drying process.
METHOD FOR PURIFYING WASTE SOLVENT
Provided is a method for purifying a waste solvent by removing carbon dioxide contained in a waste solvent derived from supercritical waste liquid generated after supercritical drying by a decompression process, and removing ammonia by a multi-stage distillation process to obtain a solvent of high purity, which can be reused in producing silica aerogel or a silica aerogel blanket.
Process for producing organically modified aerogels
It is an object of the invention to provide an economically viable process for the production of hydrophobized aerogels which works both inexpensively and in a resource-conserving manner. 2.2. This object is achieved by the provision of a process for producing organically modified aerogels by producing a sol containing [SiO.sub.4/2] units and [R.sub.xSiO.sub.(4X)/2] a units, where x may be the same or different and is 1, 2 or 3, and R may be the same or different and is hydrogen or an organic substituted or unsubstituted radical, using the sol to form a gel, surface-modifying the gel obtained in the presence of more than 0.1% by weight of a phase modifier in a mixture comprising organosiloxane and initiator, wherein the mixture contains at least 20% by weight of organosiloxane and wherein the initiator consists of acid or organosiloxane or mixtures thereof and the gels obtained are dried. 2.3. The aerogels provided can be used as insulating materials, especially in thermal insulation.
Process for producing organically modified aerogels
It is an object of the invention to provide an economically viable process for the production of hydrophobized aerogels which works both inexpensively and in a resource-conserving manner. 2.2. This object is achieved by the provision of a process for producing organically modified aerogels by producing a sol containing [SiO.sub.4/2] units and [R.sub.xSiO.sub.(4X)/2] a units, where x may be the same or different and is 1, 2 or 3, and R may be the same or different and is hydrogen or an organic substituted or unsubstituted radical, using the sol to form a gel, surface-modifying the gel obtained in the presence of more than 0.1% by weight of a phase modifier in a mixture comprising organosiloxane and initiator, wherein the mixture contains at least 20% by weight of organosiloxane and wherein the initiator consists of acid or organosiloxane or mixtures thereof and the gels obtained are dried. 2.3. The aerogels provided can be used as insulating materials, especially in thermal insulation.
Process for producing of inorganic particulate material
The present invention is directed to a process for producing inorganic particulate material, the material obtainable by such process, a modified release delivery system comprising the material and the use of the material for the administration of a bioactive agent.
Process for producing of inorganic particulate material
The present invention is directed to a process for producing inorganic particulate material, the material obtainable by such process, a modified release delivery system comprising the material and the use of the material for the administration of a bioactive agent.
Method for preparing a monolithic nanoporous silicate sol-gel material
A method for preparing a monolithic nanoporous silicate sol-gel material for modulating the pore size distribution for one single starting composition without the addition of a structuring agent. The method includes the following steps: a) synthesising a gel from at least one organosilylated precursor, the synthesis being carried out in an aqueous medium, optionally including an organic solvent and without a structuring agent, and b) drying the gel obtained in step a) at a temperature between 10 C. and 70 C., preferably between 15 C. and 55 C. and more preferably between 20 C. and 40 C., in a gas flow in a drying chamber to obtain a monolithic nanoporous silicate sol-gel material and a residual relative humidity in the drying chamber of between 0.1 and 20%, preferably between 0.5 and 10% and more preferably about 5%.
Method for preparing a monolithic nanoporous silicate sol-gel material
A method for preparing a monolithic nanoporous silicate sol-gel material for modulating the pore size distribution for one single starting composition without the addition of a structuring agent. The method includes the following steps: a) synthesising a gel from at least one organosilylated precursor, the synthesis being carried out in an aqueous medium, optionally including an organic solvent and without a structuring agent, and b) drying the gel obtained in step a) at a temperature between 10 C. and 70 C., preferably between 15 C. and 55 C. and more preferably between 20 C. and 40 C., in a gas flow in a drying chamber to obtain a monolithic nanoporous silicate sol-gel material and a residual relative humidity in the drying chamber of between 0.1 and 20%, preferably between 0.5 and 10% and more preferably about 5%.
Apparatus and method for manufacturing composite sheet comprising aerogel sheet
The present invention relates to a method for manufacturing a composite sheet comprising an aerogel sheet, which comprises: a step (S10) of preparing a fiber sheet (10); a step (S20) of laminating the aerogel sheet (30) on each of both surfaces of the fiber sheet (10); and a step (S30) of applying heat and a pressure to the aerogel sheet (30) and the fiber sheet (10), which are laminated, to bond the sheets to each other and to manufacture the composite sheet (40) in which the aerogel sheet (30), the fiber sheet (10), the aerogel sheet (30) are laminated.