A method for adjusting an etchability of a first borosilicate glass by heating the first borosilicate glass; combining the first borosilicate glass with a second borosilicate glass to form a composite; and etching the composite with an etchant. A material having a protrusive phase and a recessive phase, where the protrusive phase protrudes from the recessive phase to form a plurality of nanoscale surface features, and where the protrusive phase and the recessive phase have the same composition.

A production method and others according to the present embodiment are provided with a structure for effectively preventing occurrence of accidental spiking during drawing of a preform. In order to control the residual He-concentration in the center part of the preform, a transparent glass rod that has a predetermined outer diameter and is already sintered but is not doped with an alkali metal yet is annealed in in the atmosphere not containing He gas for an annealing time determined by referring to result data in which the relationship between the annealing time and the residual He-concentration is previously recorded for each outer diameter. In the result data, actually measured data of the residual He-concentration in a produced optical fiber preform and the annealing time are accumulated as annealing treatment results.

The present application provides a method for recovering and reusing quartz powder waste in an out-of-tube deposition process. The quartz powder recovered by this method meets the optical performance requirements for the preparation of an optical fiber preform rod having a functional cladding, reduces the production cost, and solves the problem of environmental pollution. Also, the present invention further provides a method for preparing an optical fiber preform rod by using the recovered quartz powder. The method reduces and simplifies the difficulty in the manufacturing of a core rod of a preform rod, and simplifies the difficulty in the manufacturing of some preform rods of special structures.

The present invention relates to a method of forming an optical fiber precursor including: forming an alkali metal doped tube; inserting an optical fiber core rod within the alkali metal doped tube; forming a cladding jacket around the alkali metal doped tube; and diffusing an alkali metal from the alkali metal doped tube through a surface of the optical fiber core rod. The present invention further relates to an optical fiber preform having: an optical fiber core rod; an alkali metal doped tube surrounding the optical fiber core rod; and a cladding jacket surrounding the alkali metal doped tube.

Multi-core optical fiber ribbons and methods for making multi-core optical fiber ribbons are described herein. In one embodiment, a multi-core optical fiber ribbon includes at least two core members formed from silica-based glass and oriented in parallel with one another in a single plane. Adjacent core members have a center-to-center spacing ≧15 microns and a cross-talk between adjacent core members is ≦−25 dB. In this embodiment each core member is single-moded with an index of refraction n.sub.c, and a core diameter d.sub.c. In an alternative embodiment, each core member is multi-moded and the center-to-center spacing between adjacent core members is ≧25 microns. A single cladding layer is formed from silica-based glass and surrounds and is in direct contact with the core members. The single cladding layer is substantially rectangular in cross section with a thickness ≦400 microns and an index of refraction n.sub.cl<n.sub.c.

A method for manufacturing an optical fiber preform including a core part and a cladding part is disclosed. The method includes: adding an alkali metal to an inner surface of a silica-based glass pipe; etching the inner surface of the silica-based glass pipe to which the alkali metal is added; making a glass rod by collapsing the silica-based glass pipe after the etching; and making an optical fiber preform using the glass rod. The silica-based glass pipe is heated in the adding such that a surface temperature of the silica-based glass pipe falls within a temperature range of 1500° C. or higher to lower than 2000° C.

A shaped tube (50,51) for use as a component in the fabrication of an antiresonant hollow core optical fibre, the shaped tube having a side wall with a transverse cross-sectional shape comprising a number of major curved portions (52) alternating with the same number of minor substantially straight portions (54), each curved portion (52) having an inwardly curving shape, and each straight portion (54) being equidistant from a central longitudinal axis of the shaped tube (50,51).

A method is provided that includes: forming a low-index trench region with a first density; forming an inner barrier layer comprising silica around the trench region at a second density greater than the first density; depositing silica-based soot around the first barrier layer to form an overclad region at a third density less than the second density; inserting a core cane into a trench-overclad structure; forming an outer barrier layer comprising silica in an outer portion of the overclad region at a fourth density greater than the third density; flowing a down dopant-containing gas through the trench-overclad structure to dope the trench region with the down dopant, and wherein the barrier layers mitigate diffusion of the down-dopant into the overclad region; and consolidating the trench-overclad and the core cane.

The invention relates to a method for producing a glass-fibre preform with a core of a polygonal cross section by using a rod-in-tube method and comprising the method steps of: providing a core rod (1) of a polygonal core rod cross section (2), producing a sectored sandwich tube (3) from a starting tube (4), wherein the lateral surface of the starting tube (4) is slit in the longitudinal direction into a series of outer segments (8), and so the tube cross section of the starting tube (4) is subdivided into a series of sectors of a circle (7), inserting the core rod (1) into the sectored sandwich tube (3) and aligning it and, in the case of one embodiment, inserting the core rod (1) and the sectored sandwich tube (3) into an outer casing tube (10) with a complete annular cross section and melting the sectored sandwich tube (3) and possibly the outer casing tube (10) onto the sectored sandwich tube (3), wherein the outer segments (8) of the sectored sandwich tube (3) are fused to the respective side surfaces (9) of the core rod (1).

The vacuum-based methods of forming an optical fiber preform include applying a vacuum to a preform assembly. The preform assembly has at least one glass cladding section with one or more axial through holes, with one or more canes respectively residing in the one or more axial through holes. The opposite ends of the at least one glass cladding section are capped to define a substantially sealed internal chamber. A vacuum is applied to the substantially sealed internal chamber to define a vacuum-held preform assembly. The methods also include heating the vacuum-held preform assembly to just above the glass softening point to consolidate the vacuum-held preform to form the cane-based glass preform. An optical fiber is formed by drawing the cane-based glass preform. The same furnace used to consolidate the vacuum-held preform can be used to draw the optical fiber.