C04B35/593

METHOD FOR PRODUCING CERAMIC SINTERED BODY, CERAMIC SINTERED BODY, AND LIGHT EMITTING DEVICE
20220106523 · 2022-04-07 · ·

Provided are a method for producing a ceramic sintered body having improved light emission intensity, a ceramic sintered body, and a light emitting device. The method for producing a ceramic sintered body comprises preparing a molded body that contains a nitride fluorescent material having a composition containing: at least one alkaline earth metal element M.sup.1 selected from the group consisting of Ba, Sr, Ca, and Mg; at least one metal element M.sup.2 selected from the group consisting of Eu, Ce, Tb, and Mn; Si; and N, wherein a total molar ratio of the alkaline earth metal element M.sup.1 and the metal element M.sup.2 in 1 mol of the composition is 2, a molar ratio of the metal element M.sup.2 is a product of 2 and a parameter y and wherein y is in a range of 0.001 or more and less than 0.5, a molar ratio of Si is 5, and a molar ratio of N is 8, and wherein the nitride fluorescent material has a crystallite size, as calculated by X-ray diffraction measurement using the Halder-Wagner method, of 550 Å or less, and calcining the molded body at a temperature in a range of 1,600° C. or more and 2,200° C. or less to obtain a sintered body.

Method of making whisker reinforced high fracture toughness ceramic threaded fasteners
11268560 · 2022-03-08 · ·

A high temperature fastener including a bolt and a nut, where the bolt and the nut are constructed of an aluminum oxide ceramic material reinforced with silicon-carbide crystal whiskers or silicon nitride.

Method of making whisker reinforced high fracture toughness ceramic threaded fasteners
11268560 · 2022-03-08 · ·

A high temperature fastener including a bolt and a nut, where the bolt and the nut are constructed of an aluminum oxide ceramic material reinforced with silicon-carbide crystal whiskers or silicon nitride.

INSERT AND CUTTING TOOL
20210323073 · 2021-10-21 ·

An insert may include a sintered silicon nitride including β-Si.sub.3N.sub.4 as a main component. The area up to 0.5 mm deep from a surface of the sintered silicon nitride is a first region. The first region may include an oxygen content of less than 0.8% by mass. The first region may include ReMgSi.sub.2O.sub.5N (Re is at least one of Yb and Y). A cutting tool may include a holder that extends from a first end toward a second end and includes a pocket on a side of the first end, and the insert located at the pocket.

Method for producing ceramic composite material, ceramic composite material, and light emitting device

Provided are a method for producing a ceramic composite material that has a high light emission intensity, a ceramic composite material, and a light emitting device. The method for producing a ceramic composite material, includes: preparing a green body containing a nitride fluorescent material having a composition represented by the following chemical formula (I) and aluminum oxide particles mixed with each other; and performing primary sintering the green body at a temperature in a range of 1,250° C. or more and 1,600° C. or less to provide a first sintered body:
M.sub.wLn.sup.1.sub.xA.sub.yN.sub.z  (I)
wherein in the chemical formula (I), M represents at least one element selected from the group consisting of Ce and Pr; Ln.sup.1 represents at least one element selected from the group consisting of Sc, Y, La, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, and Lu; A represents at least one element selected from the group consisting of Si and B; and w, x, y, and z each satisfy 0<w≤1.0, 2.5≤x≤3.5, 5.5≤y≤6.5, and 10≤z≤12.

Method for producing ceramic composite material, ceramic composite material, and light emitting device

Provided are a method for producing a ceramic composite material that has a high light emission intensity, a ceramic composite material, and a light emitting device. The method for producing a ceramic composite material, includes: preparing a green body containing a nitride fluorescent material having a composition represented by the following chemical formula (I) and aluminum oxide particles mixed with each other; and performing primary sintering the green body at a temperature in a range of 1,250° C. or more and 1,600° C. or less to provide a first sintered body:
M.sub.wLn.sup.1.sub.xA.sub.yN.sub.z  (I)
wherein in the chemical formula (I), M represents at least one element selected from the group consisting of Ce and Pr; Ln.sup.1 represents at least one element selected from the group consisting of Sc, Y, La, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, and Lu; A represents at least one element selected from the group consisting of Si and B; and w, x, y, and z each satisfy 0<w≤1.0, 2.5≤x≤3.5, 5.5≤y≤6.5, and 10≤z≤12.

Sliding Member, And Bearing, Motor, And Drive Device Using The Same

The sliding member according to the embodiment includes a silicon nitride sintered body that includes silicon nitride crystal grains and a grain boundary phase, in which a percentage of a number of the silicon nitride crystal grains including dislocation defect portions inside the silicon nitride crystal grains among any 50 of the silicon nitride crystal grains having completely visible contours in a 50 μm×50 μm observation region of any cross section or surface of the silicon nitride sintered body is not less than 0% and not more than 10%. The percentage is more preferably not less than 0% and not more than 3%.

Sliding Member, And Bearing, Motor, And Drive Device Using The Same

The sliding member according to the embodiment includes a silicon nitride sintered body that includes silicon nitride crystal grains and a grain boundary phase, in which a percentage of a number of the silicon nitride crystal grains including dislocation defect portions inside the silicon nitride crystal grains among any 50 of the silicon nitride crystal grains having completely visible contours in a 50 μm×50 μm observation region of any cross section or surface of the silicon nitride sintered body is not less than 0% and not more than 10%. The percentage is more preferably not less than 0% and not more than 3%.

Axial turbine

A turbine assembly includes an axial turbine with an axially arranged series of rotor sections and an external sheath providing structural support for the axial turbine, wherein the sheath is made from dense silicon nitride. Each rotor section includes an outer ring and rotor blades and the outer rings of the rotor sections connect to form a rotating outer casing, wherein the rotor sections are made from reaction bonded silicon nitride.

Ceramic laminate

The present invention provides a ceramic laminate having excellent mechanical properties, heat dissipation property, insulating property, heat resistance and anti-reactivity, and particularly an insulative heat dissipating body having an excellent thermal cycle reliability and a high withstand voltage. The ceramic laminate 1 according to the present invention is a ceramic laminate in which a ceramic film 3 is formed on a metal layer 2, wherein the ceramic film 3 has a minimum film thickness of 1 m or more, contains silicon nitride and inevitable impurities, and has silicon nitride crystal grains having an average grain size of 300 nm or less in the film thickness direction and an average grain size of 500 nm or less in the in-plane direction. As a result, the present invention can provide a ceramic laminate having excellent mechanical properties, heat dissipation property, insulating property, heat resistance and anti-reactivity, and particularly an insulative heat dissipating body having an excellent thermal cycle reliability and a high withstand voltage.