We provide methods and apparatus for preparing crystalline-clad and crystalline core optical fibers with minimal or no breakage by minimizing the influence of thermal stress during a liquid phase epitaxy (LPE) process as well as the fiber with precisely controlled number of modes propagated in the crystalline cladding and crystalline core fiber via precisely controlling the diameter of crystalline fiber core with under-saturated LPE flux. The resulting crystalline cladding and crystalline core optical fibers are also reported.

An ultrafine continuous fibrous ceramic filter, which comprises a filtering layer of a fibrous porous body, wherein the fibrous porous body comprises continuous ultrafine fibers of metal oxide which are randomly arranged and layered, and powdery nano-alumina incorporated into the ultrafine fibers or coated thereon, the ultrafine fibers being obtained by electrospinning a spinning solution comprising a metal oxide precursor sol-gel solution, and optionally, a polymer resin, and sintering the electrospun fibers, in which the ultrafine fibers have an average diameter of 10?500 nm, and the fibrous porous body has a pore size of maximum frequency ranging from 0.05 to 2 ?m, exhibits high filtration efficiency at a high flow rate, and can be regenerated.

A catalyst-free synthesis method for the formation of a metalorganic compound comprising a desired (first) metal may include, for example, selecting another (second) metal and an organic solvent, with the second metal being selected to (i) be more reactive with respect to the organic solvent than the first metal and (ii) form, upon exposure of the second metal to the organic solvent, a reaction by-product that is more soluble in the organic solvent than the metalorganic compound. An alloy comprising the first metal and the second metal may be first produced (e.g., formed or otherwise obtained) and then treated with the organic solvent in a liquid phase or a vapor phase to form a mixture comprising (i) the reaction by-product comprising the second metal and (ii) the metalorganic compound comprising the first metal. The metalorganic compound may then be separated from the mixture in the form of a solid.

A method is for the production of a scintillator fiber. In an embodiment, the method includes provisioning a suspension of a binder dissolved in a solvent and a scintillator material; and pressing the suspension into a precipitation bath in which the binder is insoluble.

We provide methods and apparatus for preparing crystalline-clad and crystalline core optical fibers with minimal or no breakage by minimizing the influence of thermal stress during a liquid phase epitaxy (LPE) process as well as the fiber with precisely controlled number of modes propagated in the crystalline cladding and crystalline core fiber via precisely controlling the diameter of crystalline fiber core with under-saturated LPE flux. The resulting crystalline cladding and crystalline core optical fibers are also reported.

An extrusion method and apparatus are described for producing ceramics, glass, glass-ceramics, or composites suitable for use as proppants. The method includes forming one or more green body materials, extruding the green body materials to form a green body extrudate, separating and shaping the green body extrudate into individual green bodies, and sintering the green bodies to form proppants. The apparatus includes a means for forming an intimate mixture of green body materials, means to produce a green body extrudate, means for separating and shaping the green body extrudate into individual green bodies, and means to sinter the green green bodies to form proppants.

A composite material that increases in temperature upon exposure to electromagnetic radiation includes single crystal silicon carbide whiskers and fibrils in a matrix material. Also disclosed are heat-generating objects that include the composite material, and a method of generating heat.

A method of forming a crystalline core/crystalline clad (C4) optical fiber. The method comprises coextruding a cladding mixture of a plasticizer and a binder with a yttrium aluminum garnet (YAG) core. The coextrusion dynamically clads a polycrystalline cladding onto the YAG core to yield a green C4 optical fiber. The C4 optical fiber is then densified, preferably in two steps sintering and hot isostatic pressing. The resulting optical C4 fiber has greater power capacity than a glass fiber labor host.

A tri-layer optical fiber. The fiber has a core which is preferably a single crystal and outer cladding, to reduce signal loss. The cladding process begins with high porosity particles, and is known to introduce porosity in the cladding and at the core/cladding interface. The porosity increases refraction and signal loss. The invention interposes a film layer intermediate the core and cladding. The film layer is sputter coated and preferably of the of same material as the cladding. The film prevents diffusion of the porous cladding into the core, minimizing porosity and improving signal transmission.

Sized short alumina-based inorganic oxide fiber comprises, based on the total weight of the sized short alumina-based inorganic oxide fiber: from 0.1 to 15 percent by weight of a size resin comprising a polyamide; and from 85 to 99.9 percent by weight of short alumina-based inorganic oxide fiber. Methods of making the sized short alumina-based inorganic oxide fiber and compositions comprising the sized short alumina-based inorganic oxide fiber in a polymeric matrix are also disclosed.