A method of treating silicon carbide fibers comprises phosphating heat treatment in a reactive gas so as to form a coating around each fiber for protection against oxidation. The coating comprises a surface layer of silicon pyrophosphate crystals and at least one underlying bilayer system comprising a layer of a phosphosilicate glass and a layer of microporous carbon.

Provided herein is a method of manufacturing a nanoscale coated network, which includes providing nanofibers, capable of forming a network in the presence of a liquid vehicle and providing a nanoscale solid substance in the presence of the liquid vehicle. The method may also include forming a network of the nanofibers and the nanoscale solid substance and redistributing at least a portion of the nanoscale solid substance within the network to produce a network of nanofibers coated with the nanoscale solid substance. Also provided herein is a nanoscale coated network with an active material coating that is redistributed to cover and electrochemically isolate the network from materials outside the network.

A CMC sandwich used to fabricate CMC structures includes facesheets bonded to a core reinforced with a ceramic truss comprising an array of CMC pins. The binder matrix in the ends of the pins is removed, leaving exposed, flexible ceramic fibers. The exposed ceramic fibers are bent so as to extend parallel to the facesheets, and are bonded to one or more plies of the facesheets. The binder matrix in the ends of the ceramic pins may be removed by mechanical or chemical processes.

The present disclosure relates to a method of fabricating a ceramic composite components. The method may include providing at least a first layer of reinforcing fiber material which may be a pre-impregnated fiber. An additively manufactured component may be provided on or near the first layer. A second layer of reinforcing fiber, which may be a pre-impregnated fiber may be formed on top the additively manufactured component. A precursor is densified to consolidates at least the first and second layer into a densified composite, wherein the additively manufactured material defines at least one cooling passage in the densified composite component.

A method of manufacturing a component includes forming an inner wrap about a mandrel. The inner wrap has first and second walls joined by a base portion and an outer wall. A rod is arranged at each of the first and second walls. An outer wrap is formed about the inner wrap and the rods to form a body. Features are formed in the first and second walls.

Fiber tows including a heat-activatable sizing are described. The sizing compositions have a first modulus at 25° C. of at least 150 megapascals (MPa) and no greater than 400 MPa; and a second modulus of 100,000 pascals (Pa) at a temperature of no greater than 160° C. Methods of preparing articles from such sized fiber tows and the articles comprising such sized fiber tows, including unidirectional and bidirectional constructions are also described.

A catalyst-free synthesis method for the formation of a metalorganic compound comprising a desired (first) metal may include, for example, selecting another (second) metal and an organic solvent, with the second metal being selected to (i) be more reactive with respect to the organic solvent than the first metal and (ii) form, upon exposure of the second metal to the organic solvent, a reaction by-product that is more soluble in the organic solvent than the metalorganic compound. An alloy comprising the first metal and the second metal may be first produced (e.g., formed or otherwise obtained) and then treated with the organic solvent in a liquid phase or a vapor phase to form a mixture comprising (i) the reaction by-product comprising the second metal and (ii) the metalorganic compound comprising the first metal. The metalorganic compound may then be separated from the mixture in the form of a solid.

The invention relates to a feedstock injector (2′) for injecting an atomized hydrocarbon feedstock into a tubular-type reactor with substantially upward or downward flow that is intended to be used in a fluid catalytic cracking unit, having: at least one hollow cylindrical body (41); at least a first and a second inlet openings (40, 42) for respectively injecting a liquid hydrocarbon feedstock to be cracked and an atomizing gas into said cylindrical body (41); at least one contact chamber (46) arranged inside said hollow cylindrical body, in which said liquid hydrocarbon feedstock to be cracked and said atomizing gas are intended to be brought into contact in order to atomize said liquid hydrocarbon feedstock to be cracked; and at least one outlet opening (44) that opens on the inside of said reactor in order to eject said liquid hydrocarbon feedstock thus atomized. According to the invention, each element of the injector (2′) is formed of a ceramic material.

A method is provided for growing a fiber structure, where the method includes: obtaining a substrate, growing an array of pedestal fibers on the substrate, growing fibers on the pedestal fibers, and depositing a coating surrounding each of the fibers. In another aspect, a method of fabricating a fiber structure includes obtaining a substrate and growing a plurality of fibers on the substrate according to 1½D printing. In another aspect, a multilayer functional fiber is provided produced by, for instance, the above-noted methods.

A ceramic article includes a ceramic matrix composite that has a porous reinforcement structure and a ceramic matrix within pores of the porous reinforcement structure. The ceramic matrix composite includes a surface zone comprised of an exterior surface of the ceramic matrix composite and pores that extend from the exterior surface into the ceramic matrix composite. A glaze material seals the surface zone within the pores of the surface zone and on the exterior surface of the surface zone as an exterior glaze layer on the ceramic matrix composite. The glaze material is a glass or glass-ceramic material. The ceramic matrix composite includes an interior zone under the surface zone, and the interior zone is free of any of the glaze material and has a greater porosity than the surface zone.