Patent classifications
C04B35/62897
Method for producing a consolidated fiber preform
A method for producing a consolidated fiber preform intended for the manufacture of a part made of composite material, includes shaping a fiber texture in a heated metal mold, the texture being pre-impregnated with a transient or fugitive material, or shaping a fiber texture in a metal mold and injecting a transient or fugitive material into the fiber texture held in shape in the metal mold, cooling the mold, removing the set fiber preform from the mold, coating the fiber preform with a slurry containing a powder of ceramic or carbon particles, heat-treating the coated fiber preform so as to form a porous shell around the fiber preform by consolidation of the slurry and so as to remove the transient or fugitive material present in the fiber preform, consolidating the fiber preform by gas-phase chemical infiltration.
Method of fabricating a ceramic matrix composite for resistance against silicon attack
A method of making a ceramic matrix composite (CMC) that may show improved resistance to chemical attack from molten silicon along with excellent mechanical strength is described. The method includes forming an interphase coating on one or more silicon carbide fibers, depositing a matrix layer comprising silicon carbide on the interphase coating, oxidizing the matrix layer to form an oxidized film comprising silicon oxide, depositing a wetting layer comprising silicon carbide on the oxidized film. After depositing the wetting layer, a fiber preform containing the silicon carbide fibers is heat treated. After the heat treatment, the fiber preform is infiltrated with a slurry. After infiltration with the slurry, the fiber preform is infiltrated with a melt containing silicon, and then the melt is cooled to form a ceramic matrix composite.
PERFORMANCE OF TECHNICAL CERAMICS
Disclosed herein is a ceramic particle comprising a core substrate chosen from yttria-stabilized zirconia, partially stabilized zirconia, zirconium oxide, aluminum nitride, silicon nitride, silicon carbide, and cerium oxide, and a conformal coating of a sintering aid film having a thickness of less than three nanometers and covering the core substrate, and methods for producing the ceramic particle.
Production method for composite material
A production method for a composite material, which includes a porous substrate and a silicon carbide film formed on a surface of a material forming the porous substrate, includes causing a silicon source containing a silicon atom, a chlorine source containing a chlorine atom, and a carbon source containing a carbon atom to react with each other to form the silicon carbide film on the surface of the material forming the porous substrate.
Nano particle agglomerate reduction to primary particle
A nanoparticle cluster reduction method yields a new composition of matter including a large percentage (e.g., 75% or higher percentage) of primary nanoparticles in the new composition of matter. The particle reduction method reduces the size of nanoparticle clusters in material of the new composition of matter, allows particle reduction of specific nanoparticle cluster sizes, and allows particle reduction to primary nanoparticles. This new composition of matter can include a high permittivity and high resistivity dielectric compound. This new composition of matter, according to certain examples, has high permittivity, high resistivity, and low leakage current. In certain examples, the new composition of matter constitutes a dielectric energy storage device that is a battery with very high energy density, high operating voltage per cell, and an extended battery life cycle. An example method can include a controlled gas evolution reaction to reduce the size of nanoparticle clusters.
FIBER HAVING INTEGRAL WEAK INTERFACE COATING, METHOD OF MAKING AND COMPOSITE INCORPORATING THE FIBER
Disclosed is a method of coating a high temperature fiber including depositing a base material on the high temperature fiber using atomic layer deposition, depositing an intermediate material precursor on the base material using molecular layer deposition, depositing a top material on the intermediate material precursor or the intermediate layer using atomic layer deposition, and heat treating the intermediate precursor. The intermediate material in the final coating includes a structural defect, has lower density than the top material or a combination thereof. Also disclosed are the coated high temperature fiber and a composite including the high temperature fiber.
Lithium-mixed oxide particles encapsulated in aluminum oxide and titanium dioxide, and method for using same
Process for producing coated mixed lithium oxide particles, in which mixed lithium oxide particles and a mixture comprising aluminium oxide and titanium dioxide are subjected to dry mixing by means of a mixing unit having a specific power of 0.1-1 kW per kg of mixed lithium oxide particles and mixture used, in total, under shearing conditions. Coated mixed lithium oxide particles comprising a mixture of aluminium oxide and titanium dioxide as coating material, wherein the aluminium oxide and the titanium dioxide are in the form of aggregated primary particles and the weight ratio of aluminium oxide to titanium dioxide is 10:90-90:10. Battery cell comprising the coated mixed lithium oxide particles.
Ceramic matrix composite component with modified thermal expansion and method for producing the same
A ceramic matrix composite (CMC) material component is provided that includes a CMC material and an environmental barrier coating (EBC). The CMC material includes first fibers, a matrix, and at least one coefficient of thermal expansion (CTE) increasing additive. The first fibers include a first material having a first CTE value. The matrix includes a second material having a second CTE value. The at least one CTE increasing additive has a third CTE value. The EBC is disposed on at least one exposed surface of the CMC material and has a fourth CTE value. The third CTE value is greater than the first CTE value and the second CTE value, and the at least one CTE increasing additive is present within the CMC material in an amount that elevates a CTE value of the CMC material above the first CTE value or the second CTE value.
Method of fabricating high-permittivity dielectric material
Nano-sized particles of barium-titanate are heated as a gas mixture of 25% hydrogen and 75% nitrogen is passed there through yielding particles of barium-titanate having oxygen vacancies therein. The particles of barium-titanate having oxygen vacancies therein are coated with silica yielding silica-coated particles having a silica coating thickness in a range of 2-5 nanometers. The silica-coated particles are sintered by application of pressure in a range of 35-50 megapascals and temperature in a range of 950-1050° C. The sintered quantity of material is cooled at a cooling rate in a range of 1-3° C. per minute at least until the temperature thereof is less than 120° C.
OXIDATION-INDUCED SHAPE MEMORY FIBER AND PREPARATION METHOD AND APPLICATION THEREOF
The present disclosure relates to an oxidation-induced shape memory fiber comprising a tension-bearing core material and/or a tension-bearing core material coated with an antioxidative coating, and an oxidizable pressure-bearing coating. The oxidizable pressure-bearing coating is coated outside the tension-bearing core material and/or the tension-bearing core material coated with an antioxidative coating; the oxidizable pressure-bearing coating is in compressive stress state and/or the tension-bearing core material coated with an antioxidative coating and the oxidizable pressure-bearing coating are in tension-compression balance state. The disclosure also relates to preparation and application thereof, the preparation is: reserving anchoring end, exerting tension force on tension-bearing core material and/or tension-bearing core material coated with an antioxidative coating, followed by coating oxidizable pressure-bearing coating thereon. The oxidation-induced shape memory fiber is applicable to high temperature oxidation environment.