C04B41/5009

ZIRCONIA MILL BLANK HAVING deltaCtotal OF ZIRCONIA 5.0 OR LESS AND PREPARING METHOD THEREOF
20240270654 · 2024-08-15 · ·

To provide a preparing method of a zirconia mill blank for dental cutting and machining having any one or more of translucency gradation, color gradation and strength gradation after perfect sintering by impregnating a zirconia calcined body with a plurality of impregnating solutions, which can suppress deterioration of the fitting property of a dental prosthesis device prepared from the zirconia mill blank for dental cutting and machining and a zirconia mill blank for dental cutting and machining having any one or more of translucency gradation, color gradation and strength gradation after perfect sintering and suppressing deterioration of the fitting property of a dental prosthesis device prepared from the zirconia mill blank for dental cutting and machining.

To porovide a zirconia mill blank for dental cutting and machining of the present invention is a preparing method of a zirconia mill blank for dental cutting and machining having any one or more of translucency gradation, color gradation and strength gradation after perfect sintering, comprising a step of impregnating a zirconia calcined body with at least two types of impregnating solutions, wherein at least one of the impregnating liquids contains a zirconium component, and in a case in which the total of metal ion concentrations (mass %) contained in each impregnating liquid is defined as C.sub.total, the difference ?C.sub.total which is a difference between C.sub.total of each impregnating liquid is 5.0 or less.

ZIRCONIA MILL BLANK HAVING MAXIMUM VALUE OF deltaSP(m) OF STABILIZER CONCENTRATION LESS THAN 0.5
20240261070 · 2024-08-08 · ·

To provide a zirconia mill blank for dental cutting and machining that can impart translucency gradation and color gradation similar to a natural tooth to a zirconia perfect sintered body without the need for special equipment.

To provide a zirconia mill blank for dental cutting and machining comprising two opposing surfaces and a side surface between the two opposing surfaces, wherein the side surface has a rectangular shape in a side view of the zirconia mill blank for dental cutting and machining, and in a case in which one of the two opposing surfaces is defined as surface A, the other surface of the two opposing surfaces is defined as surface B, a surface which is parallel to the surface A and is located at a position of 1.0 mm to 1.5 mm from the surface A toward the surface B in a direction parallel to the side surface is defined as surface C, points which are set to having 0.5 mm of distance on the straight line in the direction parallel to the side surface from the surface C toward the surface B in the area from the surface C to the surface B are defined as point P(1), point P(2), to point P(n) in the order from the surface C, a stabilizer concentration (mol %) at each point is defined as SP(1), SP(2), to SP(n) (n?((shortest distance (mm) between the surface C and the surface B)?2)/0.5), the maximum value of the stabilizer concentration (mol %) is defined as SPmax, the minimum value of the stabilizer concentration (mol %) is defined as SPmin, and the maximum value of ASP(m) defined by the following formula is defined as ?SPmax, the zirconia mill blank for dental cutting and machining has a portion where the value of SPmax?Spmin which is a difference between the SPmax and the SPmin is 0.3 or more, and the ?SPmax is less than 0.5.

[00001] ? SP ( m ) = .Math. "\[LeftBracketingBar]" SP ( m ) - SP ( m + 1 ) .Math. "\[RightBracketingBar]" ( m = 1 , 2 , .Math. n - 1 )<

ZIRCONIA MILL BLANK HAVING MAXIMUM VALUE OF deltaSP(m) OF STABILIZER CONCENTRATION LESS THAN 0.5
20240261070 · 2024-08-08 · ·

To provide a zirconia mill blank for dental cutting and machining that can impart translucency gradation and color gradation similar to a natural tooth to a zirconia perfect sintered body without the need for special equipment.

To provide a zirconia mill blank for dental cutting and machining comprising two opposing surfaces and a side surface between the two opposing surfaces, wherein the side surface has a rectangular shape in a side view of the zirconia mill blank for dental cutting and machining, and in a case in which one of the two opposing surfaces is defined as surface A, the other surface of the two opposing surfaces is defined as surface B, a surface which is parallel to the surface A and is located at a position of 1.0 mm to 1.5 mm from the surface A toward the surface B in a direction parallel to the side surface is defined as surface C, points which are set to having 0.5 mm of distance on the straight line in the direction parallel to the side surface from the surface C toward the surface B in the area from the surface C to the surface B are defined as point P(1), point P(2), to point P(n) in the order from the surface C, a stabilizer concentration (mol %) at each point is defined as SP(1), SP(2), to SP(n) (n?((shortest distance (mm) between the surface C and the surface B)?2)/0.5), the maximum value of the stabilizer concentration (mol %) is defined as SPmax, the minimum value of the stabilizer concentration (mol %) is defined as SPmin, and the maximum value of ASP(m) defined by the following formula is defined as ?SPmax, the zirconia mill blank for dental cutting and machining has a portion where the value of SPmax?Spmin which is a difference between the SPmax and the SPmin is 0.3 or more, and the ?SPmax is less than 0.5.

[00001] ? SP ( m ) = .Math. "\[LeftBracketingBar]" SP ( m ) - SP ( m + 1 ) .Math. "\[RightBracketingBar]" ( m = 1 , 2 , .Math. n - 1 )<

ALUMINUM NITRIDE CERAMIC, AND PREPARATION METHOD THEREOF
20240316538 · 2024-09-26 ·

An Aluminum nitride ceramic and preparation method thereof. The aluminum nitride ceramic comprises a porous aluminum nitride matrix. A ferrite is loaded on the pore surface of the porous aluminum nitride matrix; and nano nickel particles are loaded on the surface of the ferrite. The preparation method of the aluminum nitride ceramic comprises steps: sintering the aluminum nitride ceramic by pressureless sintering method, depositing the ferrite on pore surface of porous aluminum nitride matrix by hydrothermal method, and loading nano nickel particles on the surface of the ferrite by reduction method. A micro-reactor is provided. So that the technical problems: the preheating time of the micro-reactor prepared is too long, nickel particles fall off from the surface of matrix, and nano nickel particles grow up due to quick and direct temperature rise can be solved.

ALUMINUM NITRIDE CERAMIC, AND PREPARATION METHOD THEREOF
20240316538 · 2024-09-26 ·

An Aluminum nitride ceramic and preparation method thereof. The aluminum nitride ceramic comprises a porous aluminum nitride matrix. A ferrite is loaded on the pore surface of the porous aluminum nitride matrix; and nano nickel particles are loaded on the surface of the ferrite. The preparation method of the aluminum nitride ceramic comprises steps: sintering the aluminum nitride ceramic by pressureless sintering method, depositing the ferrite on pore surface of porous aluminum nitride matrix by hydrothermal method, and loading nano nickel particles on the surface of the ferrite by reduction method. A micro-reactor is provided. So that the technical problems: the preheating time of the micro-reactor prepared is too long, nickel particles fall off from the surface of matrix, and nano nickel particles grow up due to quick and direct temperature rise can be solved.

Method of making glass sheets with vehicle pretreatment of refractory

A method of making a glass sheet includes treating a refractory block material comprising at least one multivalent component with a vehicle comprising at least one redox altering component or precursor. The method also includes flowing molten glass over the refractory block material, wherein the treatment of the refractory block material with the vehicle comprising at least one redox altering component or precursor reduces the amount of oxygen production resulting from interaction between the at least one multivalent component and the molten glass.

COATING INSPECTION METHOD

Provided herein are methods and compositions which allow for efficient inspection, maintenance and repair of ceramic coatings.

COMPOSITE BRAKE DISKS WITH AN INTEGRATED HEAT SINK, METHODS FOR MANUFACTURING THE SAME, AND METHODS FOR PRODUCING ENCAPSULATED HEAT SINK MATERIAL

Brake disks with integrated heat sink are provided. Brake disk includes a fiber-reinforced composite material and an encapsulated heat sink material impregnated into the fiber-reinforced composite material. The encapsulated heat sink material comprises a heat sink material encapsulated within a silicon-containing encapsulation layer. Methods for manufacturing the brake disk with integrated heat sink and methods for producing the encapsulated heat sink material are also provided.

COMPOSITE BRAKE DISKS WITH AN INTEGRATED HEAT SINK, METHODS FOR MANUFACTURING THE SAME, AND METHODS FOR PRODUCING ENCAPSULATED HEAT SINK MATERIAL

Brake disks with integrated heat sink are provided. Brake disk includes a fiber-reinforced composite material and an encapsulated heat sink material impregnated into the fiber-reinforced composite material. The encapsulated heat sink material comprises a heat sink material encapsulated within a silicon-containing encapsulation layer. Methods for manufacturing the brake disk with integrated heat sink and methods for producing the encapsulated heat sink material are also provided.

CMAS-Protective Coating Infiltrants

A method for protecting a coated substrate having a porous ceramic barrier coating includes applying a molten salt to the ceramic barrier coating. The salt is selected from the group consisting of one or more acetates and/or nitrates. The molten salt is infiltrated into porosity of the ceramic barrier coating. The infiltrated molten salt is solidified. The solidified salt is sintered.