C04B2235/5276

METHOD OF FABRICATING A CERAMIC COMPOSITE
20210053881 · 2021-02-25 ·

A method of making a ceramic composite component includes providing a fibrous preform or a plurality of fibers, providing a first plurality of particles, coating the first plurality of particles with a coating to produce a first plurality of coated particles, delivering the first plurality of coated particles to the fibrous preform or to an outer surface of the plurality of fibers, and converting the first plurality of coated particles into refractory compounds. The first plurality of particles or the coating comprises a refractory metal.

Composite airfoil assembly for an interdigitated rotor
10941665 · 2021-03-09 · ·

Rotor assemblies and methods for manufacturing airfoils for rotor assemblies are provided. For example, a rotor assembly comprises a rotary structure extending circumferentially about an axial centerline of a gas turbine engine and an airfoil having a root and a tip. The root is coupled to the rotary structure and has a bulbous shape. The airfoil is formed from a plurality of composite plies, a portion of which defines at the root first and second end surfaces, which are in contact with the rotary structure and together define a chisel-shaped end of the root. In another embodiment, a rotor assembly comprises an outer rotor extending circumferentially about an axial centerline of a gas turbine engine and a composite outer rotor blade having a root and a tip. The blade root is coupled to the outer rotor and extends inward along a radial direction toward the axial centerline.

COMPRESSIBLE COATING REINFORCEMENTS FOR CERAMIC MATRIX COMPOSITES, AND METHODS OF MAKING THE SAME
20230416160 · 2023-12-28 ·

Some variations provide a pre-ceramic matrix composite comprising: a precursor pre-ceramic matrix; reinforcing elements disposed within the precursor pre-ceramic matrix; and a compressible material disposed on the surface of the reinforcing elements and interposed between the reinforcing elements and the precursor pre-ceramic matrix. Other variations provide a ceramic matrix composite comprising: a ceramic matrix; reinforcing elements disposed within the ceramic matrix; and a compressed material disposed on the surface of the reinforcing elements and interposed between the reinforcing elements and the matrix. The coating of compressible material prevents cracking during processing because the coating absorbs stresses associated with volumetric shrinkage of the ceramic matrix during densification, thereby reducing the stresses at the interface between the reinforcing elements and the ceramic matrix. Methods of fabricating ceramic matrix composites using the principles of the invention are disclosed. Methods include pyrolysis of pre-ceramic polymers, sintering of pre-ceramic materials, and sol-gel processing.

Anti-corrosion and anti-coking ceramic coating with easy state identification for coal-fired boiler and preparation method thereof

Disclosed are an anti-corrosion and anti-coking ceramic coating with easy state identification for a coal-fired boiler and a preparation method thereof. The ceramic coating is formed by compounding a bottom coating layer and a surface coating layer, wherein the bottom coating layer is prepared from raw materials comprising sodium silicate, lanthanum oxide, niobium pentoxide, aluminum oxide, bismuth oxide, boron oxide, zinc oxide, silicon oxide, titanium dioxide, nano whisker, titanium nitride, and graphite fluoride, and the surface coating layer is prepared from raw materials comprising sodium silicate, lanthanum oxide, niobium pentoxide, chromium oxide, aluminum oxide, bismuth oxide, boron oxide, zinc oxide, silicon oxide, graphite fluoride, titanium nitride, silicon carbide, nano whisker, and cobalt green. An operating state of the ceramic coating is rapidly identified by a color difference between the bottom coating layer and the surface coating layer, which is beneficial to efficient maintenance of the ceramic coating during inspection.

BARRIER COATINGS
20210024424 · 2021-01-28 ·

An example article includes a substrate and a barrier coating on the substrate extending from an inner interface facing the substrate to an outer surface opposite the inner interface. The barrier coating includes a bulk matrix and a plurality of discrete plugs inset within the bulk matrix and dispersed across the outer surface of the barrier coating. An example technique includes forming the barrier coating on the substrate of a component.

LOW-SHRINKAGE, HIGH-STRENGTH, AND LARGE CERAMIC PLATE AND MANUFACTURING METHOD THEREOF

Disclosed are a low-shrinkage, high-strength, and large ceramic plate and a manufacturing method thereof. The method comprises the following steps: (1) preparing a ceramic raw material powder; (2) subjecting an acicular wollastonite to surface coating with a silane coupling agent and to pre-dispersion with a fumed silica to obtain a pre-treated acicular wollastonite; and (3) thoroughly mixing the ceramic raw material powder and the pre-treated acicular wollastonite and granulating the resulting mixture, the amount of the pre-treated acicular wollastonite added being 10 wt % to 30 wt % of the ceramic raw material powder, and subjecting the resulting granules to dry pressing and sintering to obtain the large ceramic plate. The acicular wollastonite is incorporated into the manufacturing of the large ceramic plate to take full advantage of the reinforcing effect and low sintering shrinkage characteristics of the acicular wollastonite. The invention reduces sintering shrinkage and increases product strength.

Method of densifying a ceramic matrix composite using a filled tackifier

A method of producing an enhanced ceramic matrix composite includes applying a tackifier compound to a fiber preform. The tackifier compound includes inorganic filler particles. The method further includes modifying the tackifier compound such that the inorganic filler particles remain interspersed throughout the fiber preform, and occupy pores of fiber preform.

Method of fabricating a ceramic composite

A method of making a ceramic composite component includes providing a fibrous preform or a plurality of fibers, providing a first plurality of particles, coating the first plurality of particles with a coating to produce a first plurality of coated particles, delivering the first plurality of coated particles to the fibrous preform or to an outer surface of the plurality of fibers, and converting the first plurality of coated particles into refractory compounds. The first plurality of particles or the coating comprises a refractory metal.

MAGNESIUM ALUMINATE SPINEL REINFORCED MAGNESIUM OXIDE-BASED FOAM CERAMIC FILTER SYNTHESIZED IN SITU FROM MAGNESIUM OXIDE WHISKER, AND PREPARATION METHOD THEREFOR
20200316505 · 2020-10-08 ·

The present invention provides A magnesium oxide whisker in-situ formed MA spinel-reinforced magnesium oxide-based ceramic foam filter and a method for preparing the same. The method comprising: 1) preparing a ceramic slurry having a solid content of 60%-70% by dosing 15%-25% by mass of a nanometer alumina sol, 0.8%-1.5% by mass of a rheological agent, and the balance magnesium oxide ceramic powder comprising magnesium oxide whiskers, and then adding deionized water and ball milling to mix until uniform, and then vacuum degassing the mixture; 2) soaking a polyurethane foam template into the ceramic slurry, squeezing by a roller press the polyurethane foam template to remove redundant slurry therein to make a biscuit, and drying the biscuit by heating it to 80 C.-1200 C.; 3) putting the dried biscuit into a sintering furnace, elevating the temperature to 1400 C.-1600 C. and performing a high temperature sintering, cooling to the room temperature with the furnace to obtain the magnesium oxide-based ceramic foam filter.

Slurry Mixtures for 3-D Slurry Extrusion of Artifacts
20200308062 · 2020-10-01 ·

A slurry composition for forming an article using additive manufacturing is provided. The slurry composition comprises a carrier having a viscosity of at least 0.001 cP at normal temperature and pressure. The carrier is adapted to be flowable through a nozzle. The slurry composition further comprises a material selected from the group of a metal-containing material, a ceramic-containing material, an inorganic carbon-containing material, a silica-containing material, and combinations thereof.