A corrosion-resistant component configured for use with a semiconductor processing reactor, the corrosion-resistant component comprising: a) a ceramic insulating substrate; and, b) a white corrosion-resistant non-porous outer layer associated with the ceramic insulating substrate, the white corrosion-resistant non-porous outer layer having a thickness of at least 50 μm, a porosity of at most 1%, and a composition comprising at least 15% by weight of a rare earth compound based on total weight of the corrosion-resistant non-porous layer; and, c) an L* value of at least 90 as measured on a planar surface of the white corrosion-resistant non-porous outer layer. Methods of making are also disclosed.

A composite member may include an inorganic porous layer on a surface of metal. The inorganic porous layer may include ceramic fibers. The inorganic porous layer may be constituted of 15 mass % or more of an alumina constituent and 45 mass % or more of a titania constituent.

A sintered material comprises cubic boron nitride and a first material that is a partially stabilized ZrO.sub.2 with Al.sub.2O.sub.3 dispersed therein at crystal grain boundaries and/or in crystal grains, the sintered material comprising 20% by volume or more and 80% by volume or less of the cubic boron nitride, the sintered material comprising 0.001% by mass or more and 1% by mass or less of nitrogen in the first material when the first material is measured through secondary ion mass spectrometry.

The present invention relates to the field of MAX-phase ceramic-based composites, specifically to a short-fiber-reinforced oriented MAX-phase ceramic-based composite and a preparation method therefor. By using a new process with a fiber, a nano lamellar MAX-phase ceramic powder, other additives, etc., for preparing a fiber-reinforced MAX-phase ceramic-based composite, a novel ternary composite is prepared, wherein a matrix is composed of a highly oriented lamellar MAX-phase ceramic, the fiber is distributed parallel to the lamellar MAX-phase ceramic in an axial direction, and a granulate ceramic phase enhancement phase is dispersed in the matrix. Thus, the problems of a MAX-phase ceramic-based composite matrix material prepared by an existing method, such as coarse grains, multiple internal defects and a low strength, and a poor fracture toughness; and a reaction sintering temperature being too high such that fibers are chemically and physically damaged in a substrate, resulting in performance degradation, are solved. Fibers prepared by the method are suitable for large-scale industrial preparation and have properties that are far superior to those of any existing known fiber MAX-phase composite.

Provided are a piezoelectric ceramics which does not contain lead, has small temperature dependence of a piezoelectric constant within an operating temperature range, and has high density, a high mechanical quality factor, a satisfactory piezoelectric constant, and a small surface roughness, and a method of manufacturing the piezoelectric ceramics. The method of manufacturing a piezoelectric ceramics is characterized by including: sintering a compact containing a raw material at 1,000° C. or more to obtain a sintered compact; abrading the sintered compact; and annealing the abraded sintered compact at a temperature of 800° C. or more and less than 1,000° C.

A highly oriented nanometer MAX phase ceramic and a preparation method for a MAX phase in-situ autogenous oxide nanocomposite ceramic. The raw materials comprise a MAX phase ceramic nano-lamellar powder body or a blank body formed by the nano-lamellar powder body, wherein MAX phase ceramic nano-lamellar particles in the powder body or the blank meet the particle size being between 20-400 nm, and the oxygen content is between 0.0001%-20% by mass; MAX phase grains in the ceramic obtained after the raw materials are sintered are lamellar or spindle-shaped, the lamellar structure having a high degree of orientation. Utilizing special properties of the nano-lamellar MAX powder body, orientation occurs during compression and deformation to obtain a lamellar structure similar to that in a natural pearl shell, and such a structure has a high bearing capacity and resistance to external loads and crack propagation, just like a brick used in a building.

Embodiments disclosed herein are related to polycrystalline textured materials exhibiting heterogeneous templated grain growth, methods of forming such materials, and related systems. An example of a method of forming a polycrystalline textured material exhibiting heterogeneous templated grain growth includes providing a plurality of seeds. The method also includes aligning at least some of the plurality of seeds (e.g., single-crystal seeds) so that a selected crystallographic orientation of at least some of the plurality of seeds are substantially aligned with each other. Additionally, the method includes positioning the plurality of seeds in a powder matrix. The method then includes pressing the plurality of seeds and the powdered matrix to form a green body. Further, the method includes sintering the green body at a temperature that is sufficient to grow a plurality of grains from corresponding ones of the plurality of seeds to form the polycrystalline textured material.

Set forth herein are garnet material compositions, e.g., lithium-stuffed garnets and lithium-stuffed garnets doped with alumina, which are suitable for use as electrolytes and catholytes in solid state battery applications. Also set forth herein are lithium-stuffed garnet thin films having fine grains therein. Disclosed herein are novel and inventive methods of making and using lithium-stuffed garnets as catholytes, electrolytes and/or anolytes for all solid state lithium rechargeable batteries. Also disclosed herein are novel electrochemical devices which incorporate these garnet catholytes, electrolytes and/or anolytes. Also set forth herein are methods for preparing novel structures, including dense thin (<50 um) free standing membranes of an ionically conducting material for use as a catholyte, electrolyte, and, or, anolyte, in an electrochemical device, a battery component (positive or negative electrode materials), or a complete solid state electrochemical energy storage device. Also, the methods set forth herein disclose novel sintering techniques, e.g., for heating and/or field assisted (FAST) sintering, for solid state energy storage devices and the components thereof.

A complex according to the present disclosure contains a β-eucryptite crystal phase and a lithium tantalate crystal phase. In a temperature range of 0 to 50° C., a coefficient of thermal expansion calculated for each 1° C. is within 0±1 ppm/K. Calcium is contained in the lithium tantalate crystal phase. The volume ratio of the β-eucryptite crystal phase to the lithium tantalate crystal phase is from 90:10 to 99.5:0.5.

A method of producing polycrystalline Y.sub.3Ba.sub.5Cu.sub.8O.sub.y (Y-358) whereby powders of yttrium (III) oxide, a barium (II) salt, and copper (II) oxide are pelletized, calcined at 850 to 950° C. for 8 to 16 hours, ball milled under controlled conditions, pelletized again and sintered in an oxygen atmosphere at 900 to 1000° C. for up to 72 hours. The polycrystalline Y.sub.3Ba.sub.5Cu.sub.8O.sub.y thus produced is in the form of elongated crystals having an average length of 2 to 10 μm and an average width of 1 to 2 μm, and embedded with spherical nanoparticles of yttrium deficient Y.sub.3Ba.sub.5Cu.sub.8O.sub.y having an average diameter of 5 to 20 nm. The spherical nanoparticles are present as agglomerates having flower-like morphology with an average particles size of 30 to 60 nm. The ball milled polycrystalline Y.sub.3Ba.sub.5Cu.sub.8O.sub.y prepared under controlled conditions shows significant enhancement of superconducting and flux pinning properties.